首页> 外文期刊>Journal of separation science. >Dispersive micro‐solid‐phase extraction combined with online preconcentration by capillary electrophoresis for the determination of glycopyrrolate stereoisomers in rat plasma

【24h】

Dispersive micro‐solid‐phase extraction combined with online preconcentration by capillary electrophoresis for the determination of glycopyrrolate stereoisomers in rat plasma

机译：分散微固相萃取通过毛细管电泳与在线前浓缩的含量测定大鼠等离子体中的甘吡咯醛晶体

获取原文

获取原文并翻译 | 示例

掌桥外文数据库（机构版） >>

开具论文收录证明 >>

文献代查 >>

页面导航

摘要
著录项
相似文献
相关主题

摘要

Abstract >A simple and sensitive analytical method for four isomers of glycopyrrolate in rat plasma was developed using cation‐selective exhaustive injection‐sweeping cyclodextrin‐modified electrokinetic chromatography (CSEI‐Sweeping‐CDEKC) for online enrichment combined with dispersive micro‐solid‐phase extraction pretreatment. The CSEI‐Sweeping‐CDEKC was conducted on an uncoated fused silica capillary (40.2?cm × 75 μm) with an applied voltage of –20?kV. The electrophoretic analysis was carried out in 30?mM phosphate solution at pH 2.0 containing 20?mg/mL sulfated‐β‐cyclodextrin and 5% acetonitrile. Under these optimized conditions, the detection limit for racemic glycopyrrolate was found to be 2.0?ng/mL and this method could increase 495‐fold detection sensitivity compared with the traditional injection method. Additionally, the parameters that affected the extraction efficiency of dispersive micro‐solid‐phase extraction were also examined systematically. The glycopyrrolate isomers in rat plasma samples as low as 0.0625?μg/mL were able to be separated and detected by capillary electrophoresis with the aid of CSEI‐sweeping. The findings of this study show that the dispersive micro‐solid‐phase extraction pretreatment coupled with CSEI‐Sweeping‐CDEKC is a rapid and convenient method for analyzing glycopyrrolate isomers in rat plasma. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</标题> >使用阳离子进行大鼠等离子体中甘瓶中四个异构体的简单敏感的分析方法 - 选择性详尽注射扫描环糊精改性电动色谱（CSEI-SHEEPY-CDEKC）用于在线富集结合分散微固相提取预处理。 CSEI-SWEEPING-CDEKC在未涂覆的熔融石英毛细管（40.2×cm×75μm）上，施加电压为-20 kV。在含有20μlmm/ ml硫酸化-β-环糊精和5％乙腈的pH 2.0的pH 2.0中在30·mm磷酸盐溶液中进行电泳分析。在这些优化的条件下，发现外消旋甘瓶的检测限为2.0？Ng / ml，与传统的注射方法相比，该方法可以增加495倍的检测灵敏度。另外，还系统地检查了影响分散微固相提取的提取效率的参数。大鼠等离子体样品中的丙吡咯烷异构体能够通过Csei-Sheeble借助于毛细管电泳分离和检测到0.0625Ω·μg/ mL的等离子体样品。该研究的发现表明，与Csei-Sheeping-Cdekc偶联的分散微固相提取预处理是一种快速而方便的方法，用于分析大鼠等离子体中的甘瓶异构体。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2018年第6期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Yongjing&option=202" target="_blank" rel="nofollow">Liu Yongjing;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yu Lishuang&option=202" target="_blank" rel="nofollow">Yu Lishuang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Hua&option=202" target="_blank" rel="nofollow">Zhang Hua;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Dawei&option=202" target="_blank" rel="nofollow">Chen Dawei;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Pharmacy CollegeFujian University of Traditional Chinese MedicineFuzhou People's Republic of China;</p> <p>Pharmacy CollegeFujian University of Traditional Chinese MedicineFuzhou People's Republic of China;</p> <p>Pharmacy CollegeFujian University of Traditional Chinese MedicineFuzhou People's Republic of China;</p> <p>Key Laboratory of Food Safety Risk AssessmentChina National Center for Food Safety Risk AssessmentBeijing People's Republic of China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=capillary electrophoresis&option=203" rel="nofollow">capillary electrophoresis;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=cation‐selective exhaustive injection&option=203" rel="nofollow">cation‐selective exhaustive injection;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=dispersive micro‐solid‐phase extraction&option=203" rel="nofollow">dispersive micro‐solid‐phase extraction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=enantioseparation&option=203" rel="nofollow">enantioseparation;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=glycopyrrolate&option=203" rel="nofollow">glycopyrrolate;</a> </p> <div class="translation"> 机译：毛细管电泳;阳离子选择性详尽注射;分散微固相萃取;对糖化剂;甘瓶; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846012.html">Dispersive micro‐solid‐phase extraction combined with online preconcentration by capillary electrophoresis for the determination of glycopyrrolate stereoisomers in rat plasma</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Yongjing&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Liu Yongjing,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yu Lishuang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Yu Lishuang,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Hua&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zhang Hua,</a> <a href="/journal-foreign-35800/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of separation science. .</a> <span>2018</span><span>,第6期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：分散微固相萃取通过毛细管电泳与在线前浓缩的含量测定大鼠等离子体中的甘吡咯醛晶体</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846689.html">Dispersive micro-solid-phase extraction using carbon-based adsorbents for the sensitive determination of verapamil in plasma samples coupled with capillary electrophoresis</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jouyban Abolghasem&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Jouyban Abolghasem,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hamidi Samin&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Hamidi Samin </a> <a href="/journal-foreign-35800/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of separation science. .</a> <span>2017</span><span>,第16期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：采用碳基吸附剂的分散微固相萃取，用于敏感测定血浆样品中的维拉帕米，含有毛细管电泳</span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024674272.html">Comparison between dispersive solid-phase and dispersive liquid-liquid microextraction combined with spectrophotometric determination of malachite green in water samples based on ultrasound-assisted and preconcentration under multi-variable experimental design optimization</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Dil Ebrahim Alipanahpour&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Dil Ebrahim Alipanahpour,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ghaedi Mehrorang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Ghaedi Mehrorang,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Asfaram Arash&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Asfaram Arash,</a> <a href="/journal-foreign-30134/" target="_blank" rel="nofollow" class="tuijian_authcolor">Ultrasonics sonochemistry .</a> <span>2017</span><span>,第期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：基于超声辅助和预浓缩的分光光度法分光光度法测定分散体固相和色散液体微萃取的比较</span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-conference-foreign_meeting-248298_thesis/070507666419.html">Capillary Electrophoresis with Amperometric Determination of Curcumin inChinese Herbal Medicine Pretreated by Solid Phase Semimicroextraction</a> <b>[C]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xiuhua Sun&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Xiuhua Sun </a> <a href="/conference-foreign-248298/" target="_blank" rel="nofollow" class="tuijian_authcolor">International seminar on electroanalytical chemistry .</a> <span>2001</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用固相半萃取物预处理毛细管电泳，含有水平测定的姜黄素雀巢草药预处理</span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-degree-foreign_mphd_thesis/02061188272.html">Molecularly imprinted solid phase extraction-pulsed elution and capillary electrophoresis for rapid screening of metformin in human plasma.</a> <b>[D] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Feng, Sherry Yu.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Feng, Sherry Yu. </a> <span>2005</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：分子印迹固相萃取脉冲洗脱和毛细管电泳，可快速筛选人血浆中的二甲双胍。</span> </p> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-journal-foreign-pmc_springer-open-choice_thesis/040004960272.html">Determination of fluorine in herbs and water samples by molecular absorption spectrometry after preconcentration on nano-TiO2 using ultrasound-assisted dispersive micro solid phase extraction</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Magdalena Krawczyk-Coda&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Magdalena Krawczyk-Coda,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ewa Stanisz&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Ewa Stanisz </a> <span>-1</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：超声辅助分散微固相萃取对纳米TiO2进行预浓缩后通过分子吸收光谱法测定草药和水样中的氟</span> </p> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/open-access_resources_thesis/0100096192610.html ">Preconcentration of uranium in water samples using dispersive liquid-liquid micro- extraction coupled with solid-phase extraction and determination with inductively coupled plasma-optical emission spectrometry</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=M. Rezaee,&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">M. Rezaee,,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=F. Khalilian&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">F. Khalilian </a> <span>2015</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：分散液 - 液微萃取结合固相萃取和电感耦合等离子体发射光谱法测定水样中的铀浓度</span> </p> </li> <li> <div> <b>8. </b><a class="enjiyixqcontent" href="/ntis-science-report_ad_thesis/02071690166.html">Sensitive Capillary Electrophoresis Microchip Determination of Trinitroaromatic Explosives in Nonaqueous Electrolyte Following Solid Phase Extraction</a> <b>[R] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lu, Q. &option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Lu, Q. ,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Collins, G. E. &option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Collins, G. E. ,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Smith, M. &option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Smith, M. ,</a> <span>2002</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：敏感毛细管电泳微萃取固相萃取法测定非水电解质中的三硝基芳烃炸药</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-pharmacological-bulletin_thesis/0201242268317.html">在线固相萃取-液质联用法定量分析生物基质中丁香醛及其在大鼠体内药代动力学研究中的应用</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王允吉&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王允吉</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王清清&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王清清</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨志晖&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,杨志晖</a> <span> <a href="/journal-cn-6427/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国药理学通报 </a> </span> <span> . 2012</span><span>,第007期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-analytical-chemistry_thesis/0201230557982.html">固相萃取-分散液液微萃取-柱前衍生法测定水样中痕量雌激素</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李鱼&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 李鱼</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘建林&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘建林</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张琛&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,张琛</a> <span> <a href="/journal-cn-10804/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 分析化学 </a> </span> <span> . 2012</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_natural-science-journal-hainan-university_thesis/0201270217224.html">微溶剂中通过硼氢化钠还原吡咯醛来制备新颖吡咯醇</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘彦飞&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 刘彦飞</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王智&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王智</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=丁俊熊&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,丁俊熊</a> <span> <a href="/journal-cn-4609/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 海南大学学报（自然科学版） </a> </span> <span> . 2018</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_journal-graduate-school-chinese-academy-sciences_thesis/0201279649515.html">分散固相萃取结合毛细管电泳-激光诱导荧光法测定血清中甲基化精氨酸</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=谢士杰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 谢士杰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨泽诚&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,杨泽诚</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=周洲&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,周洲</a> <span> <a href="/journal-cn-3816/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国科学院研究生院学报 </a> </span> <span> . 2020</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_journal-university-chinese-academy-sciences_thesis/0201281495011.html">分散固相萃取结合毛细管电泳-激光诱导荧光法测定血清中甲基化精氨酸</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=谢士杰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 谢士杰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨泽诚&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,杨泽诚</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=周洲&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,周洲</a> <span> <a href="/journal-cn-23987/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国科学院大学学报 </a> </span> <span> . 2020</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-1831_thesis/02022291670.html">分散固相萃取与分散相液液微萃取联用用于环境水样和底泥中痕量稀土元素的分析</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xueqin Guo&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . Xueqin Guo</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=郭雪勤&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,郭雪勤</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Man He&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Man He</a> <span> <a href="/conference-cn-1831/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十五届全国稀土分析化学学术研讨会 </a> <span> <span> . 2015</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020313424096.html">固相萃取与毛细管电泳在线联用同时测定尿液中的二甲双胍和格列苯脲</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王梦阳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王梦阳</a> <span> . 2016</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/061201386753.html">一种用于固相萃取-毛细管电泳在线联用的毛细管微柱的制备方法</a> <b>[P]</b> . <span> 中国专利： CN102680557B </span> <span> . 2014.06.04</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120107037350.html">一种用于固相萃取-毛细管电泳在线联用的毛细管微柱的制备方法</a> <b>[P]</b> . <span> 中国专利： CN102680557A </span> <span> . 2012-09-19</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130418020289.html">Sample stacking method using on-line automatic solid phase extraction coupled to nonaqueous capillary electrophoresis and interface structure between solid-phase preconcentration cartridge and capillary therefor</a> <b>[P]</b> . <span> 外国专利：  US8784630B2 </span> <span> . 2014-07-22</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：在线自动固相萃取结合非水毛细管电泳的样品堆积方法及固相预浓缩柱与毛细管之间的界面结构 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130430679563.html">SAMPLE STACKING METHOD USING ON-LINE AUTOMATIC SOLID PHASE EXTRACTION COUPLED TO NONAQUEOUS CAPILLARY ELECTROPHORESIS AND INTERFACE STRUCTURE BETWEEN SOLID-PHASE PRECONCENTRATION CARTRIDGE AND CAPILLARY THEREFOR</a> <b>[P]</b> . <span> 外国专利：  US2009084680A1 </span> <span> . 2009-04-02</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：固相富集色谱柱与毛细管之间耦合的非连续毛细管电泳和界面结构的在线自动固相萃取样品堆积方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130414284547.html">Stacking method using on-line automatic elution solid phase extraction combining nonaqueous capillary electrophoresis and interface structure between solid phase extractor and capillary therefor</a> <b>[P]</b> . <span> 外国专利：  KR101467561B1 </span> <span> . 2014-12-01</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：在线自动洗脱固相萃取结合非水毛细管电泳及其固相萃取器与毛细管之间的界面结构的堆叠方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704025846012','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="" onclick="$('.journalsub-pop-up').hide()"> <p class="pardon">抱歉，该期刊暂不可订阅，敬请期待！</p> <p class="current">目前支持订阅全部北京大学中文核心（2020）期刊目录。</p> <div style="display: flex;margin-top: 69px;justify-content: space-between;"> <div class="no-sub" onclick="$('.journalsub-pop-up').hide()">暂不订阅</div> <div class="other-sub" onclick="continueSub('from=pc-detail')">继续订阅其他期刊</div> </div> </div> </div> <div class="right_btn"> <ul> <li class="gouwuche">  </li> <li class="yijian"> <a href="javascript:void(0);" onclick="link_analysis('/mycenter/auth/complaint.html',this)">意见反馈</a> </li> <li class="top"> <a href="javascript:scrollTo(0,0);">回到顶部</a> </li> <li class="shouye"> <a href="/">回到首页</a> </li> </ul> </div> <div class="xllindexfooter"> <div class="xllindexfootercenter"> <div class="xllindexfooterleft left" > <div class="xllindexfooterleftli"> <ul> <li><a href="/about.html">关于掌桥</a></li> <li><a href="/help/helpmap.html">资源导航</a></li> <li><a href="/help/helpguide.html">新手指南</a></li> <li><a href="/help/helpcenter.html">常见问题</a></li> <li><a href="/sitemap.html">网站地图</a></li> <li><a href="/help/helpcenter.html?type=9">版权声明</a></li> </ul> </div> <div class="xllindexfooterleft"> <p class="xllindexfooterlefteamil">客服邮箱：kefu@zhangqiaokeyan.com</p> <div class="xllindexfooterlefttcp"> <div class="xllindexfooterpoliceiimg"></div> <div class="xllindexfooterpoliceispan"> <span>京公网安备：11010802029741号 </span> <span>ICP备案号：<a href="https://beian.miit.gov.cn" rel="nofollow" target="_blank">京ICP备15016152号-6</a></span> <span>六维联合信息科技 (北京) 有限公司©版权所有</span> </div> </div> </div> </div> <div class="xllindexfooterright left"> <ul> <li> <p style="font-weight: bold;">客服微信</p> <div></div> </li> <li> <p style="font-weight: bold;">服务号</p> <div></div> </li> </ul> </div> </div> </div> <span id="0704025846012down" data-source="7," data-out-id="MJ2VdBWNBdDi7QxDAJN5Qcm4K4lNRcvWnFS5NGxnTanV118mG+fIa/WIGIIPcM6n," data-f-source-id="7" data-title="Dispersive micro‐solid‐phase extraction combined with online preconcentration by capillary electrophoresis for the determination of glycopyrrolate stereoisomers in rat plasma" data-price="20" data-site-name="" data-transnum="24" style="display:none;"></span> <input type="hidden" value="4" id="sourcetype"> <input type="hidden" value="35800" id="journalid"> <input type="hidden" value="1" id="inyn_provide_service_level"> <input type="hidden" value="https://cdn.zhangqiaokeyan.com" id="imgcdn"> <input type="hidden" value="1" id="isdeatail"> <input type="hidden" value="" id="syyn_indexed_database"> <input type="hidden" value="" id="servicetype"> <input type="hidden" id="pagename" value="Dispersive micro‐solid‐phase extraction combined with online preconcentration by capillary electrophoresis for the determination of glycopyrrolate stereoisomers in rat plasma"/> <input type="hidden" value="thesis_get_original" id="pageIdentification"> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/jquery-1.12.4.js"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/common/lwlh_ajax.js"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/zq.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/common/common.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/jquery.cookie.js"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/top.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/common/tip.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/common/login.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/common/down.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/common/search.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/searchtype.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/user/regist.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/zxs_solor/detail.js?v=5.7.7"></script> <script type="text/javascript" src="https://www.zhangqiaokeyan.com/statistics/static/pagecollection.js"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/tj.js"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/pushbaidu.js"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/common/history.js"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/util/cookie.js?v=5.7.7"></script> <script type="text/javascript" src="https://cdn.zhangqiaokeyan.com/js/weipu/weipu.js?v=5.7.7"></script> </body> <script> $(function(){ var weiPuStatus = getCookie('WeiPuStatus'); if(weiPuStatus){ tipWeiPuStatus(weiPuStatus); delCookie('WeiPuStatus'); } getFacetKeywordVoInId(); var sourcetype = $("#sourcetype").val(); var inyn_provide_service_level = $("#inyn_provide_service_level").val(); if((sourcetype ==1||sourcetype==4)&&inyn_provide_service_level!=4){ getJournal(); } }) </script> </html>