Spectral decomposition of        <fc xmlns='http://www.wiley.com/namespaces/wiley'>R</fc>R        aman spectra of mixed‐phase        <fc xmlns='http://www.wiley.com/namespaces/wiley'>          TiO          <sub>2</sub>        </fc>          TiO          <sub xmlns='http://www.wiley.com/namespaces/wiley'>2</sub>2                thin films on        <fc xmlns='http://www.wiley.com/namespaces/wiley'>Si</fc>Si        and silicate substrates

Schipporeit Sebastian; Mergel Dieter

摘要

Abstract > We present a method to fit Raman spectra of TiO <sub>2</sub> thin films on silicon wafers, fused silica, and crown glass with adjustable model spectra of the different components of the substrate and the thin film. With reasonable restrictions of the fitting parameters, the method developed in this paper allows a simultaneous fit to the measured spectra. The TiO <sub>2</sub> thin film spectrum is split into one spectrum for the amorphous phase and spectra for each crystalline phase (anatase, rutile, and brookite) being divided into first‐order scattering and a phase background (including second‐order scattering). Moreover, if the substrate is luminescent, the substrate spectrum is split into luminescence and Raman spectra. All decisions on parameters are made by the fitting procedure within a simultaneous fit of a series of spectral models to the observed Raman spectrum. The main strategies for preparing such models are pointed out in a way that they should be applicable to other materials. > TiO <sub>2</sub> is a promising and flexible material for photocatalytic applications with rapidly growing interest in mixed‐phase TiO <sub>2</sub> as nanostructured material or thin film. For the analysis of such films, it is important to differentiate the signals of the various phases and to distinguish between signals from the substrate and the film. This provides a means to improve the quantitative evaluation of Raman spectra. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> >我们存在一种硅晶片，熔融二氧化硅和冠玻璃上TiO <sub> 2 </ sub>薄膜的拉曼光谱的方法，具有基板和薄膜的不同组分的可调节模型光谱。具有合理参数的合理限制，本文开发的方法允许同时适合测量的光谱。将TiO <sub> 2 </ sub>薄膜光谱分成为无定形相的一种光谱，用于每个结晶相（锐钛矿，金红石和布鲁克钛矿）分为一阶散射和相位背景（包括第二个-Order散射）。此外，如果基板被发光，则基板谱被分成发光和拉曼光谱。关于参数的所有决定都是由拟合程序在同时适合一系列光谱模型到观察到的拉曼光谱。准备这些模型的主要策略是指他们应该适用于其他材料的方式。 </ p> TiO <sub> 2 </ sub>是光催化应用的有希望的和柔韧的材料，具有在混合相TiO <sub> 2 </ sub>作为纳米结构材料或薄膜中的快速生长感兴趣的应用。为了分析这种薄膜，重要的是要区分各个相的信号并区分来自基板和膜的信号。这提供了改善拉曼光谱的定量评估的方法。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35645/'>《Journal of Raman Spectroscopy: An International Journal for Original Work in All Aspects of Raman Spectroscopy, Including Higher Order Processes, and Also Brillouin- and Rayleigh Scattering》</a> <b style="margin: 0 2px;">|</b><span>2018年第7期</span><b style="margin: 0 2px;">|</b><span>共13页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Schipporeit Sebastian&option=202" target="_blank" rel="nofollow">Schipporeit Sebastian;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mergel Dieter&option=202" target="_blank" rel="nofollow">Mergel Dieter;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Faculty of PhysicsUniversity of Duisburg‐EssenDuisburg Germany;</p> <p>Faculty of PhysicsUniversity of Duisburg‐EssenDuisburg Germany;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4724.html" title="光谱学">光谱学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=amorphous phase&option=203" rel="nofollow">amorphous phase;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=decomposition of R aman spectra&option=203" rel="nofollow">decomposition of R aman spectra;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=mixed‐phase TiO 2&option=203" rel="nofollow">mixed‐phase TiO 2;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=second‐order scattering&option=203" rel="nofollow">second‐order scattering;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thin films&option=203" rel="nofollow">thin films;</a> </p> <div class="translation"> 机译：非晶相;RAMAN Spectra的分解;混合相TiO 2;二阶散射;薄膜; 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href="/patent-detail/06130435141101.html">METHOD OF IMPROVING OF THE COST/EFFICIENCY INDEX OF ANTI-HELICOBACTER THERAPY OF DUODENUM PEPTIC ULCER http://www.google.com/url?sa=tamp;ct=resamp;cd=2amp;url=http3A2F2Fwww.ncbi.nlm.nih.gov2Fentrez2Fquery.fcgi3Fcmd3DRetrieve26db3DPubMed26list_uids3D1523004326dopt3DAbstractamp;ei=jGe7Ru2NIJXi-AKT3aTMDgamp;usg=AFQjCNG9isUJ2GUaghb1bYtqUhP8D-Pkwwamp;sig2=-9nJyqkyxKjGoDz_gysIbg</a> <b>[P]</b> . <span> 外国专利：  UA24972U </span> <span> . 2007-07-25</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：改善十二指肠胃溃疡抗幽门螺杆菌治疗成本/效率指数的方法<http://www.google.com/url?sa=t&ct=res&cd=2&url=http%3A%2F%2Fwww.ncbi.nlm .nih.gov％2Fentrez％2Fquery.fcgi％3Fcmd％3DRetrieve％26db％3DPubMed％26list_uids％3D15230043％26dopt％3DAbstract＆ei = jGe7Ru2NIJXi-AKT3aTMDg＆usg = AFQjCngyyKykYyKJyk_DwKhYD_KwhDkWyDJKyKwhDwDkWyDJWyKJwKDtWhWhWhYKYK2DQWhDW </span> </p> </li> 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Spectral decomposition of RR aman spectra of mixed‐phase TiO 2 TiO 22 thin films on SiSi and silicate substrates

摘要

Spectral decomposition of RR aman spectra of mixed‐phase TiO ₂ TiO ₂2 thin films on SiSi and silicate substrates