Highly thermal conductive benzoxazine‐epoxy interpenetrating polymer networks containing liquid crystalline structures

Liu Ying; Chen Jiming; Zhang Yaoheng; Gao Sheng; Lu Zaijun; Xue Qingbin

摘要

ABSTRACT > A diamine‐based benzoxazine monomer (Bz) and a liquid crystalline epoxy monomer (LCE) are synthesized, respectively. Subsequently, a benzoxazine‐epoxy interpenetrating polymer network (PBEI) containing liquid crystalline structures is obtained by sequential curing of the LCE and the Bz in the presence of imidazole. The results show that the preferential curing of LCE plays a key role in the formation mechanism of liquid crystalline phase. Due to the introduction of liquid crystalline structures, the thermal conductivity of PBEI increases with increasing content of LCE. When the content of LCE is 80 wt %, the thermal conductivity reaches 0.32 W m ?1 K ?1 . Additionally, the heat‐resistance of PBEI is superior to liquid crystalline epoxy resin. Among them, PBEI55 containing equal weight of Bz and LCE has better comprehensive performance. Its thermal conductivity, glass transition temperature, and the 5 % weight loss temperature are 0.28 W m ?1 K ?1 , 160 °C, and 339 °C, respectively. By introducing boron nitride (BN) fillers into PBEI55, a composite of PBEI/BN with the highest thermal conductivity of 3.00 W m ?1 K ?1 is obtained. ? 2017 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2017 , 55 , 1813–1821 </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”> <title type =“main”>抽象</ title> >基于二胺的苯并恶嗪单体（BZ）和液晶环氧单体（LCE）分别合成。随后，通过在咪唑的存在下通过连续固化LCE和BZ而获得含有液晶结构的苯并恶嗪 - 环氧互持聚合物网络（PBEI）。结果表明，LCE的优先固化在液晶相的形成机制中起着关键作用。由于引入液晶结构，普博的导热率随着LCE的增加而增加。当LCE的含量为80wt％时，导热率达到0.32w m Δ1</ sup> k Δ1</ sup>。另外，普博的耐热性优于液晶环氧树脂。其中，含有平等的BZ和LCE的PBEI55具有更好的全面性能。其导热率，玻璃化转变温度和5％重量损失温度分别为0.28WM 1 / sop>，160℃和339℃。通过将氮化硼（BN）填料引入PBEI55中，获得了具有3.00Wm α1</ sup> k α1</ sup>的最高导热率的pbei / bn的复合物。还2017年Wiley期刊，Inc.J.Minon。 SCI。，B部分：聚合物。物理。 2017 </ b>， 55 </ i>，1813-1821 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35627/'>《Journal of Polymer Science, Part B. Polymer Physics》</a> <b style="margin: 0 2px;">|</b><span>2017年第24期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Ying&option=202" target="_blank" rel="nofollow">Liu Ying;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Jiming&option=202" target="_blank" rel="nofollow">Chen Jiming;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Yaoheng&option=202" target="_blank" rel="nofollow">Zhang Yaoheng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gao Sheng&option=202" target="_blank" rel="nofollow">Gao Sheng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lu Zaijun&option=202" target="_blank" rel="nofollow">Lu Zaijun;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xue Qingbin&option=202" target="_blank" rel="nofollow">Xue Qingbin;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Key Laboratory for Special Functional Aggregated Materials of Ministry of Education School of Chemistry and Chemical Engineering Shandong UniversityJinan 250100 People's Republic of China;</p> <p>Institute of Lanzhou Petrochemical Company PetroChinaLanzhou 730060 People's Republic of China;</p> <p>Institute of Lanzhou Petrochemical Company PetroChinaLanzhou 730060 People's Republic of China;</p> <p>Key Laboratory for Special Functional Aggregated Materials of Ministry of Education School of Chemistry and Chemical Engineering Shandong UniversityJinan 250100 People's Republic of China;</p> <p>Key Laboratory for Special Functional Aggregated Materials of Ministry of Education School of Chemistry and Chemical Engineering Shandong UniversityJinan 250100 People's Republic of China;</p> <p>Key Laboratory for Special Functional Aggregated Materials of Ministry of Education School of Chemistry and Chemical Engineering Shandong UniversityJinan 250100 People's Republic of China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1185.html" title="高分子化学（高聚物）">高分子化学（高聚物）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=interpenetrating polymer networks&option=203" rel="nofollow">interpenetrating polymer networks;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=liquid crystals&option=203" rel="nofollow">liquid crystals;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polybenzoxazines&option=203" rel="nofollow">polybenzoxazines;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thermal conductivity&option=203" rel="nofollow">thermal conductivity;</a> </p> <div class="translation"> 机译：互穿聚合物网络;液晶;聚苯肼;导热率; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025810981.html">Highly thermal conductive benzoxazine‐epoxy interpenetrating polymer networks containing liquid crystalline structures</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Ying&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Liu Ying,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Jiming&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Chen Jiming,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Yaoheng&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zhang Yaoheng,</a> <a href="/journal-foreign-35627/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of Polymer Science, Part B. 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