Theoretical studies and antibacterial activity for Schiff base complexes

机译：席夫碱基复合物的理论研究和抗菌活性

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Abstract > New ligand 4‐((2‐Hydroxy1‐naphthyl) methylene amino)‐1.5‐dimethyl‐2‐phenyl‐1H‐pyrazol‐3(2H)‐one (HL) was synthesized from the reaction of 2‐hydroxy‐1‐naphthaldehyde and 4‐aminophenaz one. A complexes of this ligand [VO(II)(HL)(SO <sub>4</sub> )], [Pt(IV)(L)Cl <sub>3</sub> ], [Re(V)(L)Cl <sub>3</sub> ]Cl, and [M(II)(L)Cl] (M═Pd(II), Ni(II), Cu(II)) were synthesized. The resulted compounds were characterized by IR, NMR ( 1 H and 13 C), mass spectrometry, element analysis, and UV‐Vis spectroscopy. Additionally, the spectroscopic studies revealed octahedral geometries for the Re(V), Pt(IV) complexes, and square pyramidal for VO(II), square planar for Pd(II) complex, and tetrahedral for the Ni(II) and Cu(II) complexes. Thermodynamic parameters (ΔE * , ΔH * , ΔS * , ΔG * , and K) were calculated using from the TGA curve Coats‐Red fern method. Therefore, hyper Chem‐8 program has been used to predict structural geometries of compounds in the gas phase. Finally, the synthesized Schiff base and its metal complexes were screened for their biological activity against bacterial species, 2 Gram‐positive bacteria ( Bacillus subtilis and <fc> <fi>Staphylococcus aureus</fi> </fc> ) and 2 Gram‐negative bacteria ( <fc> <fi>Escherichia coli</fi> </fc> and Pseudomonas aeruginosa ). </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</标题> >新配体4 - （（2-羟基1-萘基）亚甲氨基）-1.5-二甲基-2-苯基-1H-吡唑-3（2H） - 从2-羟基-1-萘醛和4-氨基苯基的反应中合成了-ONE（HL）。该配体的复合物[VO（II）（HL）（SO <sub> 4 </ sub>）]，[Pt（IV）（L）C1 <sub> 3 </ sub>]，[Re（v）（L）Cl <亚> 3 </ sub>] Cl，和[M（II）（L）Cl]（M 3 S（II），Ni（II），Ni（II），Cu（II））。通过IR，NMR（ 1 h和 13℃），质谱，元素分析和UV-Vis光谱表征所得化合物。另外，光谱研究揭示了Re（V），Pt（IV）复合物和VO（II）的方形金字塔，Pd（II）复合物的方形平面，以及用于Ni（II）和Cu的四面体（ II）复合物。使用来自的热力学参数（ΔE * </ sup>，Δh * </ sup>，Δg * </ sup>和k）使用TGA曲线涂层 - 红色蕨类植物方法。因此，HEAD CHEM-8程序已被用于预测气相中化合物的结构几何形状。最后，筛选合成的席夫碱及其金属配合物，用于对细菌物种的生物活性，2革氏阳性细菌（枯草芽孢杆菌和<fc> <fi>金黄色葡萄球菌</ fi> </ Fc>）和2克阴性细菌（<Fc> <Fi>大肠杆菌</ Fi> </ Fc>和假单胞菌铜绿假单胞菌）。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35546/'>《Journal of Physical Organic Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2017年第12期</span><b style="margin: 0 2px;">|</b><span>共12页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Al Zoubi Wail&option=202" target="_blank" rel="nofollow">Al Zoubi Wail;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Al‐Hamdani Abbas Ali Salih&option=202" target="_blank" rel="nofollow">Al‐Hamdani Abbas Ali Salih;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Putu Widiantara I&option=202" target="_blank" rel="nofollow">Putu Widiantara I;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hamoodah Rehab Ghalib&option=202" target="_blank" rel="nofollow">Hamoodah Rehab Ghalib;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ko Young Gun&option=202" target="_blank" rel="nofollow">Ko Young Gun;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of Materials Science and EngineeringYeungnam UniversityGyeongsan 38541 Republic of Korea;</p> <p>Department of Chemistry College of Science for WomenUniversity of BaghdadBaghdad Iraq;</p> <p>School of Materials Science and EngineeringYeungnam UniversityGyeongsan 38541 Republic of Korea;</p> <p>Department of Chemistry College of Science for WomenUniversity of BaghdadBaghdad Iraq;</p> <p>School of Materials Science and EngineeringYeungnam UniversityGyeongsan 38541 Republic of Korea;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4796.html" title="有机化学一般性问题">有机化学一般性问题;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=2‐hydroxy‐1‐naphthaldehyde&option=203" rel="nofollow">2‐hydroxy‐1‐naphthaldehyde;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=theoretical studies&option=203" rel="nofollow">theoretical studies;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thermal analysis&option=203" rel="nofollow">thermal analysis;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=transition metal complexes&option=203" rel="nofollow">transition metal complexes;</a> </p> <div class="translation"> 机译：2-羟基-1-萘醛;理论研究;热分析;过渡金属配合物; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> 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