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5‐Phenyl‐1,3,4‐oxadiazole‐2‐thiol/polyamide‐montmorillonite microbicides nanocomposites as drug delivery system

机译：5-苯基-1,3,4-恶二唑-2-硫醇/聚酰胺 - 蒙脱石杀菌剂纳米复合材料作为药物递送系统

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Abstract > The preparation and structural characterization of polymeric microbicides consisting of 5‐phenyl‐1,3,4‐oxadiazole‐2‐thiol covalently bound to polyamide based on diethyl‐2,3‐dihydroxysuccinate and polyoxypropylenetriamine Jeffamine (T <sub>403</sub> ) are described. Two different mole ratios of 5‐phenyl‐1,3,4‐oxadiazole‐2‐thiol was reacted with chloroacetylated diethyl‐2,3‐dihydroxysuccinate followed by polycondensation with Jeffamine (T <sub>403</sub> ). The nanocomposites were prepared by modification of microbicide polyamides to yield polymers with phosphonium salt or amine hydrochloride salt followed by ion exchange process between the phosphonium salt or amine hydrochloride of the polyamides and the intermellar sodium cation of the clay mineral montmorillonite. The monomers were characterized by mass spectrum, proton nuclear magnetic resonance. The polymers showed good or moderate antimicrobial activities. Nanocomposites were characterized by Fourier transformed infrared spectroscopy, X‐ray diffraction, thermal gravimetric analysis, and transmission electron microscope. The swelling behavior and release of 5‐phenyl‐1,3,4‐oxadiazole‐2‐thiol in different pH values (2.3, 5.8, and 7.4) were studied. A slow release, ranging from 12% to 28% after 50?hours was recorded from nanocomposites. However, the release profile reached almost 70% from polyamides. The antimicrobial activity of the polyamides was studied against gram‐negative bacteria, gram‐positive bacteria, yeast, and the filamentous fungi by well diffusion method. The polyamides showed better antimicrobial activities than 5‐phenyl‐1,3,4‐oxadiazole‐2‐thiol. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</标题> >由5-苯基-1,3,4组成的聚合物微生物胶剂的制备和结构表征 - 基于二乙基-2,3-二羟基琥珀酸盐和聚氧丙基三胺jeffamine（T <sub> 403 </ sub>）共价结合至聚酰胺的聚酰胺唑-2-硫醇。两种不同的5-苯基-1,3,4-二氧化胺的摩尔比与氯乙酰化二乙基-2,3-二羟基琥珀酸盐反应，然后用jeffamine缩聚（t <sub> 403 </ sub>）。通过改性微生物剂聚酰胺制备纳米复合材料，得到具有鏻盐或盐酸胺的聚合物，然后在聚酰胺的鏻盐或盐酸胺之间的离子交换过程和粘土矿物蒙脱石的蛋白质钠阳离子之间。单体的特征在于质谱，质子核磁共振。聚合物显示出良好或中等的抗微生物活性。纳米复合材料的特征在于傅里叶变化的红外光谱，X射线衍射，热重分析和透射电子显微镜。研究了不同pH值（2.3,5.8和7.4）中的溶胀行为和5-苯基-1,3,4-二氧化胺-2-巯基二醇。从纳米复合材料记录50℃后，慢速释放，从12％到28％。然而，释放型材从聚酰胺达到近70％。通过良好的扩散方法对聚酰胺的抗微生物活性针对革兰氏阴性细菌，革兰氏阳性细菌，丝状真菌进行研究。聚酰胺显示比5-苯基-1,3,4-恶二唑-2-硫醇更好的抗微生物活性。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35546/'>《Journal of Physical Organic Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2018年第7期</span><b style="margin: 0 2px;">|</b><span>共12页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Salahuddin Nehal&option=202" target="_blank" rel="nofollow">Salahuddin Nehal;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Elbarbary Ahmed&option=202" target="_blank" rel="nofollow">Elbarbary Ahmed;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Allam Nanis G.&option=202" target="_blank" rel="nofollow">Allam Nanis G.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hashim Ayat F.&option=202" target="_blank" rel="nofollow">Hashim Ayat F.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Chemistry Faculty of ScienceTanta UniversityTanta Egypt;</p> <p>Department of Chemistry Faculty of ScienceTanta UniversityTanta Egypt;</p> <p>Department of Botany Faculty of ScienceTanta UniversityTanta Egypt;</p> <p>Food Industries and Nutrition DivisionNational Research Center (NRC)Giza Egypt;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4796.html" title="有机化学一般性问题">有机化学一般性问题;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=1&option=203" rel="nofollow">1;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=3&option=203" rel="nofollow">3;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=4‐oxadiazole&option=203" rel="nofollow">4‐oxadiazole;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=drug release system&option=203" rel="nofollow">drug release system;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=microbicides&option=203" rel="nofollow">microbicides;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanocomposites&option=203" rel="nofollow">nanocomposites;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polyamides&option=203" rel="nofollow">polyamides;</a> </p> <div class="translation"> 机译：1;3;4-氧代唑;药物释放系统;杀微生物剂;纳米复合物;聚酰胺; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025793746.html">5‐Phenyl‐1,3,4‐oxadiazole‐2‐thiol/polyamide‐montmorillonite microbicides nanocomposites as drug delivery system</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Salahuddin Nehal&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Salahuddin Nehal,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Elbarbary Ahmed&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Elbarbary Ahmed,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Allam Nanis G.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Allam Nanis G.,</a> <a href="/journal-foreign-35546/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of Physical Organic Chemistry .</a> <span>2018</span><span>,第7期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：5-苯基-1,3,4-恶二唑-2-硫醇/聚酰胺 - 蒙脱石杀菌剂纳米复合材料作为药物递送系统</span> </p> </li> <li> <div> <b>2. </b><a 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translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：蒙脱土/胰岛素/ TiO_2杂化纳米复合材料作为新型口服给药系统的研究</span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704010341175.html">Preparation of Novel pH-Sensitive Nanocomposites Based on Ionic-Liquid Modified Montmorillonite for Colon Specific Drug Delivery System</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mahkam Mehrdad&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Mahkam Mehrdad,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rafi Abdolrahim Abbaszad&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Rafi Abdolrahim Abbaszad,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gheshlaghi Leila Mohammadzadeh&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Gheshlaghi Leila Mohammadzadeh </a> <a href="/journal-foreign-29566/" target="_blank" rel="nofollow" class="tuijian_authcolor">Polymer Composites .</a> <span>2016</span><span>,第1期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：基于离子液体修饰的蒙脱土的新型pH敏感纳米复合材料的结肠特异性给药系统的制备</span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-conference-foreign_meeting-277153_thesis/0705017319089.html">Study on the Interaction of fluorescent probe 2-(2'-Chloro phenyl)-5-(2'- hydroxyl phenyl)1,3,4-oxadiazole with DNA</a> <b>[C]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ding Mei&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Ding Mei,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lei Yingjie&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Lei Yingjie,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xu Fang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Xu Fang,</a> <a href="/conference-foreign-277153/" target="_blank" rel="nofollow" class="tuijian_authcolor">International Conference on Advanced Engineering Materials and Technology .</a> <span>2011</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：荧光探针2-（2'-氯苯基）-5-（2'-羟基苯基）1,3,4-二氧化氮与DNA的相互作用研究</span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-degree-foreign_mphd_thesis/02061402844.html">Polyamide-imide and montmorillonite nanocomposites.</a> <b>[D] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ranade, Ajit Jagdish.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Ranade, Ajit Jagdish. </a> <span>2001</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：聚酰胺酰亚胺和蒙脱土纳米复合材料。</span> </p> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-journal-foreign-pmc_acta-crystallographica-section-e-crystallographic-communications_thesis/040004309061.html">5,5′-Di-4-pyridyl-2,2′-(p-phenylene)di-1,3,4-oxadiazole</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rui-Sha Zhou&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Rui-Sha Zhou,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jiang-Feng Song&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Jiang-Feng Song </a> <span>2016</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：5,5'-二-4-吡啶基-2.2'-（对亚苯基）二-1,3,4-恶二唑</span> </p> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/open-access_resources_thesis/01000129416826.html">3,3′-carbonylbis5-phenyl-1,3,4-oxadiazole-2(3H)-thione: A Novel, Reactive, and Versatile Condensing Agent for Amide, Ester, Thiol Ester, Urea, Carbonate, Polyamide, and Polyurea Syntheses</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yasuo Saegusa&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Yasuo Saegusa,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tatsushi Watanabe&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Tatsushi Watanabe,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shigeo Nakamura&option=202" target="_blank" rel="nofollow" class="tuijian_auth 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=晁淑军&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 晁淑军</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李硕&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李硕</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=惠新平&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,惠新平</a> <span> <a href="/journal-cn-6565/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 新乡医学院学报 </a> </span> <span> . 2006</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_world-pesticides_thesis/0201248119071.html">5-（2-芳酰基）-芳氧甲基-2-苯基-1，3，4-恶二唑的合成及对黍霜霉病的防治活性</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈锦露&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 陈锦露</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张芝平&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,张芝平</a> <span> <a href="/journal-cn-9193/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 世界农药 </a> </span> <span> . 2005</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-33950_thesis/02022994051.html">含毗陛环的双杂环化合物研究Ⅱ.2-取代苯氧乙硫基-5-吡唑基-1,3,4-恶二唑和双(5-吡唑基-1,3,4-恶二唑-2-)二硫代烷烃的合成及生物活性</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈寒松&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 陈寒松</a> <span> <a href="/conference-cn-33950/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国化工学会农药专业委员会第九届年会 </a> <span> <span> . 1998</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314742371.html">N-(5-烷基-1,3,4-噻二唑-2-基)-S-(5-取代-4-N-邻羟苯基亚胺基-1,2,4-三唑-3-基)-α-硫代乙酰胺的合成及活性研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=高海燕&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 高海燕</a> <span> . 2012</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120102862946.html">1-(5-(2-氨基苯并d恶唑-5-基)-1,3,4-噻二唑-2-基)-3-(2-氟-5-甲基苯基)脲的合成及其用途</a> <b>[P]</b> . <span> 中国专利： CN104250245A </span> <span> . 2014-12-31</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120100862362.html">含5-苯基-1,3,4-恶二唑-2-硫酮的金（I）膦配合物及其制备方法与应用</a> <b>[P]</b> . <span> 中国专利： CN110054640A </span> <span> . 2019-07-26</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130448243453.html">DERIVATIVES OF 5-PHENYL-3-(PIPERIDINE-4-YL)-1,3,4-OXADIAZOLE- -2(3H)-ONE, METHOD OF THEIR SYNTHESIS, PHARMACEUTICAL COMPOSITION BASED ON THEREOF AND DRUG</a> <b>[P]</b> . <span> 外国专利：  RU2167160C2 </span> <span> . 2001-05-20</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：5-苯基-3-（哌啶丁-4-基）-1,3,4-恶二唑--2（3H）-的衍生物，其合成方法，基于其的药物组成和药物 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130476760954.html">ALKYL- AND CYCLOALKYL-SUBSTITUTED 2-(2-(2- HYDROXY-3-T-BUTYLAMINO-PROPOXY)-5-ACYLAMINO- PHENYL)-1,3,4-OXADIAZOLE, MANUFACTURE AND DRUG CONTAINING SAME</a> <b>[P]</b> . <span> 外国专利：  JPS5759878A </span> <span> . 1982-04-10</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：烷基和环烷基取代的2-（2-（2-羟基-3-T-丁氨酯-丙基）-5-酰基氨基苯）-1,3,4-恶二唑，制造和药物含量相同 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130481876932.html">1,3,4 -THIADIAZOLE, 1,3,4-OXADIAZOLE AND 1,2,4 TRIAZOLE - 5 THIOLS</a> <b>[P]</b> . <span> 外国专利：  AU1244376A </span> <span> . 1977-10-06</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：1,3,4-噻二唑，1,3,4-恶二唑和1,2,4三唑-5硫醇 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" 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