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首页> 外文期刊>Journal of Physical Organic Chemistry >Demonstration of NC(sp 2 ) NC(sp 22 ) ‐centered stereofluctuations in a guanidine derivative and its cation
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Demonstration of NC(sp 2 ) NC(sp 22 ) ‐centered stereofluctuations in a guanidine derivative and its cation

机译：在胍衍生物和阳离子中的 nc（sp 2 ） nc（sp 2 ）（sp 2 2） - 中晶体化及其阳离子

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Abstract > NMR line shapes and coalescences of pairs of diastereotopic reporter nuclei ( 1 H and 13 C) at suitable molecular positions were used to measure the stereofluctuation rate constants of an <fi>N</fi> ‐aryl cycloguanidine model compound of the type aryl—N═C[N(CH <sub>3</sub> )CH <sub>2</sub> ] <sub>2</sub> ( 7 in Scheme?[Scheme 1. 1 Scheme The model compounds 1 and 5 to ...]) in toluene and in CDCl <sub>3</sub> as the solvents. The key criterion is coincidence or noncoincidence of the rate constants, which revealed that both free N═C double‐bond rotation and free <fi>N</fi> —aryl single‐bond rotation occur much more slowly than in‐plane, lone‐electron pair inversion at nitrogen, which is fast even at ?99°C. The related cycloguanidinium model compound ( 6 in Scheme?[Scheme 1. 1 Scheme The model compounds 1 and 5 to ...]) cannot perform such an N‐inversion but simulates it at roughly 35°C in CDCl <sub>3</sub> and in Cl <sub>2</sub> CD—CDCl <sub>2</sub> through a less rapid N═C half‐rotation that is coupled with a correlated, counter‐sense <fi>N</fi> —aryl half‐rotation, whereas both free N═C double‐bond rotation and free <fi>N</fi> —aryl rotation are again significantly slower. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > NMR线形状和成对的双对抗报告核（ 1 </ sup在合适的分子位置以H和 13℃）用于测量芳基-n═c型芳基 - n═c的<fi> n-fi> -aryl环核素内模型化合物的立体电磁率常数[n （CH <sub> 3 </ sub>）ch <sub> 2 </ sub>] <sub> 2 </ sub>（方案中 7 </ b>）？[方案1. 1方案模型化合物在甲苯中和5至......]中的1和5至...]作为溶剂的甲苯和CdCl <sub> 3 </ sub>。关键标准是速率常数的巧合或非煅烧，这揭示了自由的N═C双键旋转和Free <Fi> N </ Fi> -Aryl单键旋转比在平面内更慢 - Electron对氮的反转，即使在α99℃下也快速。相关环核苷酸模型化合物（方案中的 6）化合物？[方案1. 1方案，模型化合物1和5-]）不能进行这种n倒数，但在大约35°C下模拟它在CDCL <Sub> 3 </ sub>和CL <sub> 2 </ sub> CD-CD-CDCL <SUB> 2 </ sub>通过较少的N═C半旋转，与相关的计数器相耦合-Sense <fi> n </ fi> - ralyl半旋转，而免费的n═c双键旋转和free <fi> n </ fi> -aryl旋转再次较慢。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35546/'>《Journal of Physical Organic Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2018年第8期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Knorr Rudolf&option=202" target="_blank" rel="nofollow">Knorr Rudolf;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=B?hrer Petra&option=202" target="_blank" rel="nofollow">B?hrer Petra;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department ChemieLudwig‐Maximilians‐Universit?t MünchenMunich Germany;</p> <p>Department ChemieLudwig‐Maximilians‐Universit?t MünchenMunich Germany;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4796.html" title="有机化学一般性问题">有机化学一般性问题;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=diastereotopomerization&option=203" rel="nofollow">diastereotopomerization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=internal rotation&option=203" rel="nofollow">internal rotation;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nitrogen inversion&option=203" rel="nofollow">nitrogen inversion;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=NMR line shapes&option=203" rel="nofollow">NMR line shapes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=stereolability&option=203" rel="nofollow">stereolability;</a> </p> <div class="translation"> 机译：非对称运动化;内部旋转;氮倒置;NMR系形状;立体性; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025793536.html">Demonstration of <fc > NC(sp 2 ) </fc> NC(sp <sup >22 ) ‐centered stereofluctuations in a guanidine derivative and its cation</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Knorr Rudolf&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Knorr Rudolf,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=B?hrer 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href="/academic-journal-cn_journal-clinical-pulmonary-medicine_thesis/0201277865225.html">特发性肺纤维化患者肺泡灌洗液和血清中Napsin A、KL-6、SP-A、SP-D表达的意义及与肺功能相关性</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈石&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 陈石</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈静&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陈静</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=魏瑜&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,魏瑜</a> <span> <a href="/journal-cn-5956/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 临床肺科杂志 </a> </span> <span> . 2020</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_advanced-textile-technology_thesis/020123791775.html">合成糊料SP在阳离子染料印花中的应用</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=袁近&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 袁近</a> <span> <a href="/journal-cn-9412/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 现代纺织技术 </a> </span> <span> . 2002</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-12752_thesis/02022722940.html">超音波對Chlorella sp.與Chodatella sp.之破壞及釋出各類有機物中螢光強度值之變化</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=趙升雲&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 趙升雲</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=何曉蓉&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,何曉蓉</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陳振正&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陳振正</a> <span> <a href="/conference-cn-12752/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第六届海峡两岸水质安全控制技术及管理研讨会 </a> <span> <span> . 2010</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020313134342.html">含咪唑啉阳离子的离子型铁(Ⅲ)配合物的合成、表征及其在sp3C−H键酯化反应中的应用</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=卢冰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 卢冰</a> <span> . 2017</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120206083016.html">Nc3015‑SP链传动弧形自动交换激光切割机</a> <b>[P]</b> . <span> 中国专利： CN206084153U </span> <span> . 2017-04-12</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120742895.html">确定移动SPS接收机视野中SPS卫星有序组的方法</a> <b>[P]</b> . <span> 中国专利： CN1429344B </span> <span> . 2011.05.11</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130414310419.html">KOMAGATAEIBACTER SP SFCB22-18 STRAIN AND PRODUCTION METHODS OF BATERIAL CELLULOSE BY USING SAME</a> <b>[P]</b> . <span> 外国专利： <!-- 韩国专利： --> KR20140130569A </span> <span> . 2014-11-11</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：KOMAGATAEIBACTER SP SFC 22-18菌株和使用相同方法生产纤维素的方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130415027765.html">Strain composition comprising: Stenotrophomonas sp strain 2L, 5L Stenotrophomonas sp strain, Stenotrophomonas sp strain 6L, Stenotrophomonas sp strain 3N, Achromobacter sp strain 4P, Arthrobacter sp strain 1N, 2N Brevundimonas sp strain, Brevundimonas sp strain 5N, 6N Brevuedimonas sp strain, Pseudomonas sp strain 3G, 4G strain Pseudomonas sp. deposited under - deposit number KKP 2041 p, bioremediation vaccine strains containing the composition, the use of vaccine bioremediation of soil to remove contaminants and soil purification method</a> <b>[P]</b> . <span> 外国专利： <!-- --> PL219151B1 </span> <span> . 2015-03-31</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：菌株组成包括：嗜麦芽单胞菌2L菌株，5L嗜麦芽单胞菌sp菌株，嗜麦芽单胞菌sp菌株6L，嗜麦芽单胞菌sp菌株3N，无色杆菌属菌株4P，节杆菌属菌株1N，短杆菌属菌株2N，短杆菌属菌株，短杆菌属菌株5N，短杆菌属菌株6N，短杆菌属sp菌株3G，4G菌株假单胞菌sp。保藏下保藏号为KKP 2041 p，包含生物修复疫苗菌株的成分，利用疫苗对土壤进行生物修复以去除污染物和土壤净化方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130417619429.html">Strain composition comprising: Stenotrophomonas sp strain 2L, 5L Stenotrophomonas sp strain, Stenotrophomonas sp strain 6L, Stenotrophomonas sp strain 3N, Achromobacter sp strain 4P, Arthrobacter sp strain 1N, 2N Brevundimonas sp strain, Brevundimonas sp strain 5N, 6N Brevuedimonas sp strain, Pseudomonas sp strain 3G, 4G strain Pseudomonas sp. deposited under - deposit number KKP 2041 p, bioremediation vaccine strains containing the composition, the use of vaccine bioremediation of soil to remove contaminants and soil purification method</a> <b>[P]</b> . <span> 外国专利： <!-- --> PL399388A1 </span> <span> . 2013-12-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：菌株组成包括：嗜麦芽单胞菌2L菌株，5L嗜麦芽单胞菌sp菌株，嗜麦芽单胞菌sp菌株6L，嗜麦芽单胞菌sp菌株3N，无色杆菌属菌株4P，节杆菌属菌株1N，短杆菌属菌株2N，短杆菌属菌株，短杆菌属菌株5N，短杆菌属菌株6N，短杆菌属sp菌株3G，4G菌株假单胞菌sp。保藏下保藏号为KKP 2041 p，包含生物修复疫苗菌株的成分，利用疫苗对土壤进行生物修复以去除污染物和土壤净化方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" 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