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Development of a technique for the on line determination of Uranium in solution by gamma ray spectrometry

机译:γ射线光谱法在线测定溶液中铀的技术开发

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摘要

A technique based on gamma ray spectrometry has been developed for the continuous monitoring of uranium in the solution form. Simulated container and support system was designed and fabricated for the development of an efficiency calibration curve and to find the detection limit for the estimation of uranium using 185.7 keV (~(235)U) gamma ray. The system was calibrated for its counting efficiency using HPGe detector system, in a standard source mount to detector geometry. The sensitivity of the detection system and counting time for low-level estimation of uranium has also been established. The detectioa limit of the monitor is approx 10 mg of Uranium per litre of the solution. In order to correct for the density variation of the solution, experiment was carried to study the variation of count rate of 185.7 keV gamma ray of ~(235)U as a function of the density of the solution. This report gives the details of the development of a continuous monitor for the determination of uranium in the solution streams.
机译:已经开发出一种基于伽马射线能谱的技术,用于连续监测溶液形式的铀。设计并制造了模拟的容器和支撑系统,以绘制效率校准曲线,并找到使用185.7 keV(〜(235)U)γ射线估算铀的检测极限。使用HPGe检测器系统对系统的计数效率进行校准,并安装在检测器几何体的标准光源中。还建立了检测系统的灵敏度和铀低含量估算的计数时间。监测仪的检出限约为每升溶液10毫克铀。为了校正溶液的密度变化,进行了实验以研究〜(235)U的185.7 keV伽马射线计数率随溶液密度的变化。该报告详细介绍了开发连续监测仪以确定溶液流中铀的方法。

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