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首页> 外文期刊>JOM >Structural and Electrical Analysis of Microwave Processed YSZ Electrolytes for SOFC Prepared by Co-precipitation Method
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Structural and Electrical Analysis of Microwave Processed YSZ Electrolytes for SOFC Prepared by Co-precipitation Method

机译:通过共沉淀法制备微波加工YSZ电解质的结构和电气分析

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AbstractThe aim of the present study is to investigate the effect of microwave energy on the structural and electrical properties of yttria-stabilized zirconia (YSZ) electrolyte for solid oxide fuel cells (SOFC). Five different compositions of Zr1?xYxO2?x/2(x?=?0.06–0.14) were prepared by a co-precipitation method and were then sintered by microwave as well as conventional heating at 1400°C for 20?min and 240?min, respectively. The structural and electrical properties of the samples sintered by both the methods were compared. The x-ray diffraction (XRD) results revealed that YSZ samples sintered by both methods had either a tetragonal crystal structure or a cubic structure depending on its composition. Almost the same degree of densification as well as conductivity of same order was found from impedance analysis for both microwave- and conventionally sintered YSZ products, which showed that microwave sintering is the better alternative for material processing in terms of saving energy and time without compromising the product quality.]]>
机译:<![cdata [ <标题>抽象 ara id =“par1”>目前研究的目的是调查效果微波能量对固体氧化物燃料电池(SOFC)的氧化钇稳定氧化锆(YSZ)电解质结构和电性能的影响。五种不同的Zr <下标> 1?<重点类型=“斜体”> x y <重点类型=“斜体”> x o <下标> 2?<重点类型=“斜体”> x / 2 (<重点类型=“斜体”> x ?=?0.06-0.14)由共同制备沉淀方法,然后通过微波烧结,以及在1400℃下常规加热20≤min,分别为240≤min。比较了两种方法烧结的样品的结构和电性能。 X射线衍射(XRD)结果表明,通过两种方法烧结的YSZ样品具有四边形晶体结构或根据其组成的立方结构。从微波和常规烧结的YSZ产品的阻抗分析中发现了几乎相同的致密化以及相同顺序的电导率,这表明微波烧结是在节省能量和时间方面更好的材料处理替代方案,而不会损害产品质量。 ]]>

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