Synchrotron Based Measurement of the Temperature Dependent Thermal Expansion Coefficient of Ammonium Perchlorate

Kellogg Robert; Lapidus Saul; Hedman Trevor; Kalman Joseph

摘要

Abstract > Ammonium perchlorate is commonly used as an oxidizer in solid rocket propellant. Having a knowledge of its thermal expansion properties is essential for its application in different environments. Knowledge of thermal expansion properties is also useful for the prediction of propellant mechanical properties and response of propellant slow cook off applications. X‐ray diffraction analysis was performed on ammonium perchlorate at temperatures ranging from 260?K to 500?K. From there, Bragg peaks were indexed by fitting theoretical values of 2θ to the 2θ values of peaks obtained from the experiment. The Miller indices along with the 2θ values were then used to solve for the lattice parameters at each temperature. The lattice parameters, in nanometers, range from 0.9201 to 0.9373, 0.5805 to 0.5865, and 0.7439 to 0.7535 for a , b , and c , respectively. The measurement of the lattice parameter expansion leads to the determination of the temperature dependent thermal expansion coefficients within the temperature range. The lattice parameter values also lead to the determination of strain and stress on the ammonium perchlorate crystal. Direct measurement of the strain within the crystal lattice provides a more accurate measurement method over traditional optical‐based techniques. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 高氯酸铵通常用作固体火箭推进剂的氧化剂。了解其热膨胀性能对于其在不同环境中的应用至关重要。热膨胀性能知识对于预测推进剂机械性能和推进剂缓慢烹饪脱离应用的反应也是有用的。在从260Ωk至500℃的温度下对高氯酸铵进行X射线衍射分析。从那里，通过拟合理论值来编制布拉格峰 2θ</ i> 到了 2θ</ i> 从实验中获得的峰值值。米勒指数以及 2θ</ i> 然后用于在每个温度下求解晶格参数的值。纳米，纳米，范围为0.9201至0.9373，0.5805至0.5865，0.7439至0.7535 a </ i> 那 b </ i> ，和 c </ i> ，分别。晶格参数膨胀的测量导致温度范围内的温度相关的热膨胀系数的确定。晶格参数值也导致测定高氯酸铵晶体上的应变和应力。晶格内的应变的直接测量为传统的光学技术提供更准确的测量方法。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29946/'>《Propellants, Explosives, Pyrotechnics》</a> <b style="margin: 0 2px;">|</b><span>2020年第3期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kellogg Robert&option=202" target="_blank" rel="nofollow">Kellogg Robert;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lapidus Saul&option=202" target="_blank" rel="nofollow">Lapidus Saul;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hedman Trevor&option=202" target="_blank" rel="nofollow">Hedman Trevor;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kalman Joseph&option=202" target="_blank" rel="nofollow">Kalman Joseph;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Mechanical and Aerospace EngineeringCalifornia State University Long BeachLong Beach CA USA;</p> <p>X-ray Science DivisionArgonne National LaboratoryLemont IL USA;</p> <p>Combustion Science and Propulsion Research BranchNaval Air Warfare Center-Weapons DivisionChina Lake CA USA;</p> <p>Mechanical and Aerospace EngineeringCalifornia State University Long BeachLong Beach CA USA;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1837.html" title="爆炸物工业、火柴工业">爆炸物工业、火柴工业;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ammonium Perchlorate&option=203" rel="nofollow">Ammonium Perchlorate;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Thermal Expansion&option=203" rel="nofollow">Thermal Expansion;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Synchrotron&option=203" rel="nofollow">Synchrotron;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Propellant&option=203" rel="nofollow">Propellant;</a> </p> <div class="translation"> 机译：高氯酸铵;热膨胀;同步;推进剂; 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