Catalytic Activity of Ferrates (NiFe2O4, ZnFe2O4 and CoFe2O4) on the Thermal Decomposition of Ammonium Perchlorate

Zhang Ming; Zhao Fengqi; Yang Yanjing; An Ting; Qu Wengang; Li Hui; Zhang Jiankan; Li Na

摘要

Abstract > Three kinds of ferrates (NiFe <sub>2</sub> O <sub>4</sub> , ZnFe <sub>2</sub> O <sub>4</sub> and CoFe <sub>2</sub> O <sub>4</sub> ) were prepared via the facile solvothermal method and characterized using SEM, TEM, XRD, XPS, FT‐IR and BET instruments. The NiFe <sub>2</sub> O <sub>4</sub> , CoFe <sub>2</sub> O <sub>4</sub> and ZnFe <sub>2</sub> O <sub>4</sub> particles possess hollow structure with average particle size of 70, 220 and 360?nm, respectively. The catalytic performance of the ferrates for AP thermal decomposition were studied using DSC and TG‐DTG methods, and the decomposition mechanism of AP were suggested. The catalytic effects of different ferrates for AP thermal decomposition were significantly different. The CoFe <sub>2</sub> O <sub>4</sub> has the best catalytic activity, and the high thermal decomposition peak temperature ( T <sub>HDP</sub> ) and apparent activation energy ( E <sub>a</sub> ) of AP were decreased by 108.99?°C and 37.38?kJ?mol ?1 in the presence of CoFe <sub>2</sub> O <sub>4</sub> sample. Adding ferrates has no obvious influence on the gas‐phase decomposition products of AP, but has a great influence on the energy barrier of high temperature decomposition of AP. The excellent catalytic activity of CoFe <sub>2</sub> O <sub>4</sub> is mainly attributed to the synergistic interaction between Fe and Co, which is conducive to the thermal decomposition of AP. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 三种驯化剂（nife <sub> 2 </ sub> O. <sub> 4 </ sub> ，Znfe. <sub> 2 </ sub> O. <sub> 4 </ sub> 和cofe. <sub> 2 </ sub> O. <sub> 4 </ sub> ）通过容易的溶剂热法制备，并使用SEM，TEM，XRD，XPS，FT-IR和BET仪器进行了特征。 nife <sub> 2 </ sub> O. <sub> 4 </ sub> ，Cofe. <sub> 2 </ sub> O. <sub> 4 </ sub> 和Znfe. <sub> 2 </ sub> O. <sub> 4 </ sub> 颗粒分别具有平均粒径为70,220和360Ω·Nm的中空结构。使用DSC和TG-DTG方法研究了用于AP热分解的催化性能，并提出了AP的分解机制。不同丙酸酯对AP热分解的催化作用显着差异。 cofe. <sub> 2 </ sub> O. <sub> 4 </ sub> 具有最佳的催化活性，以及高热分解峰值温度（ t </ i> <sub> hdp </ sub> ）和明显的激活能量（ e </ i> <sub> a </ sub> ）AP的108.99°C和37.38？KJ？摩尔？1 </ sup> 在Cofe存在下 <sub> 2 </ sub> O. <sub> 4 </ sub> 样本。加入氢铁特对AP的气相分解产物没有明显影响，但对AP的高温分解的能量屏障具有很大影响。 CoFe的优异催化活性 <sub> 2 </ sub> O. <sub> 4 </ sub> 主要归因于FE和CO之间的协同相互作用，这有利于AP的热分解。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29946/'>《Propellants, Explosives, Pyrotechnics》</a> <b style="margin: 0 2px;">|</b><span>2020年第3期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Ming&option=202" target="_blank" rel="nofollow">Zhang Ming;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhao Fengqi&option=202" target="_blank" rel="nofollow">Zhao Fengqi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Yanjing&option=202" target="_blank" rel="nofollow">Yang Yanjing;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=An Ting&option=202" target="_blank" rel="nofollow">An Ting;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qu Wengang&option=202" target="_blank" rel="nofollow">Qu Wengang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Hui&option=202" target="_blank" rel="nofollow">Li Hui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Jiankan&option=202" target="_blank" rel="nofollow">Zhang Jiankan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Na&option=202" target="_blank" rel="nofollow">Li Na;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Science and Technology on Combustion and Explosion LaboratoryXi'an Modern Chemistry Research InstituteXi'an 710065 P. R. China;</p> <p>Science and Technology on Combustion and Explosion LaboratoryXi'an Modern Chemistry Research InstituteXi'an 710065 P. R. China;</p> <p>Science and Technology on Combustion and Explosion LaboratoryXi'an Modern Chemistry Research InstituteXi'an 710065 P. R. China;</p> <p>Science and Technology on Combustion and Explosion LaboratoryXi'an Modern Chemistry Research InstituteXi'an 710065 P. R. China;</p> <p>Science and Technology on Combustion and Explosion LaboratoryXi'an Modern Chemistry Research InstituteXi'an 710065 P. R. China;</p> <p>Science and Technology on Combustion and Explosion LaboratoryXi'an Modern Chemistry Research InstituteXi'an 710065 P. R. China;</p> <p>Science and Technology on Combustion and Explosion LaboratoryXi'an Modern Chemistry Research InstituteXi'an 710065 P. R. China;</p> <p>Science and Technology on Combustion and Explosion LaboratoryXi'an Modern Chemistry Research InstituteXi'an 710065 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1837.html" title="爆炸物工业、火柴工业">爆炸物工业、火柴工业;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solid propellant&option=203" rel="nofollow">solid propellant;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ferrate&option=203" rel="nofollow">ferrate;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thermal decomposition&option=203" rel="nofollow">thermal decomposition;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ammonium perchlorate&option=203" rel="nofollow">ammonium perchlorate;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=catalysis&option=203" rel="nofollow">catalysis;</a> </p> <div class="translation"> 机译：固体推进剂;加氢;热分解;高氯酸铵;催化作用; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024626646.html">Catalytic Activity of Ferrates (NiFe2O4, ZnFe2O4 and CoFe2O4) on the Thermal Decomposition of Ammonium 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WANG Tong</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王通&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王通</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ZHAO Ning-ning&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,ZHAO Ning-ning</a> <span> <a href="/conference-cn-40347/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 2015第十四届中国国际纳米科技（成都）研讨会 </a> <span> <span> . 2015</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314741696.html">光照下NiFe2O4/CoFe2O4分解二氧化碳为碳的研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杜婷&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 杜婷</a> <span> . 2013</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/061204729511.html">一种FeCo2O4材料在高氯酸铵热分解催化中的应用</a> <b>[P]</b> . <span> 中国专利： CN109529842B </span> <span> . 2021.10.22</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120113029416.html">一种ZnO/CB催化剂的制备方法及其催化高氯酸铵热分解的应用</a> <b>[P]</b> . <span> 中国专利： CN113058582A </span> <span> . 2021-07-02</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130487715701.html">AMMONIUM PERCHLORATE COMPOSITE PROPELLANT CONTAINING AN ORGANIC TRANSITIONAL METAL CHELATE CATALYTIC ADDITIVE</a> <b>[P]</b> . <span> 外国专利：  US3492176A </span> <span> . 1970-01-27</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包含有机过渡金属螯合物催化添加剂的高氯酸铵复合推进剂 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130484604255.html">CATALYTIC DECOMPOSITION OF AMMONIUM BISULFATE TO FORM AMMONIUM AND SULFUR DIOXIDE BISULFITE</a> <b>[P]</b> . <span> 外国专利：  US3835218A </span> <span> . 1974-09-10</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：硫酸氢铵催化分解成铵和二氧化硫亚硫酸氢盐 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130449123647.html">A process for preparing Zeolite Catalysts with AIPO4 acids combined with catalytic activity and / or hydrothermal stability improvedA process for improving the catalytic activity and hydrothermal stability of Zeolite Catalysts, a process for Cracking Hydrocarbon with a</a> <b>[P]</b> . <span> 外国专利：  AR014709A1 </span> <span> . 2001-03-28</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> 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