The Effects of Aniline Stabilizers on Nitrocellulose Based on Isothermal Thermal Decomposition

Luo Liqiong; Jin Bo; Chai Zuohu; Huang Qiong; Chu Shijin; Peng Rufang

摘要

Abstract > The effects of various aniline stabilizers on the thermal stability of nitrocellulose (NC) were investigated via isothermal thermal decomposition dynamics. The pressure‐time curves of NC/stabilizer composites were found to have a distinct inflection point, which was not observed on the pressure‐time curves of NC. The effects of stabilizers on the isothermal thermal decomposition kinetics of NC were evaluated using Arrhenius equation and model‐fitting method, and the effect of stabilizers on the storage time of NC was estimated using Berthelot equation. Results showed that the activation energy of NC/MNA, NC/ENA, NC/ i ‐PNA, and NC/ n ‐BNA before the inflection point were 162.9, 153.3, 147.4, and 150.6?kJ?mol ?1 , respectively, which were significantly increased compared with that of pure NC (144.7?kJ?mol ?1 ). Furthermore, the time required for the decomposition extent of NC/MNA, NC/ENA, NC/ i ‐PNA, and NC/ n ‐BNA to reach 0.1?% were 24.9, 11.2, 16.7, and 11.2?years, respectively, at 298.15?K, which was longer than that required of NC (10.6?years). UV‐vis revealed that the stabilizers were almost consumed when the NC/stabilizer thermal decomposition pressure‐time curve reached the inflection point. Based on the above results, the stability order was MNA i ‐PNAENA n ‐BNA as the criterion for time of the inflection point. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 通过等温热分解动力学研究各种苯胺稳定剂对硝化纤维素（NC）的热稳定性的影响。发现Nc /稳定剂复合材料的压力 - 时间曲线具有明显的拐点，在NC的压力 - 时间曲线上未观察到这一点。使用Arhenius方程和模型配合方法评估稳定剂对Nc等温热分解动力学的影响，使用Berthelot方程估计稳定器对NC储存时间的影响。结果表明，NC / MNA，NC / ENA，NC /的激活能量/ 我</ i> -PNA和NC / n </ i> -BNA之前拐点为162.9,153.3,147.4和150.6？KJ？摩尔？1 </ sup> 分别与纯NC相比显着增加（144.7 kj？mol ？1 </ sup> ）。此外，NC / MNA，NC / ENA，NC /的分解程度所需的时间我</ i> -PNA和NC / n </ i> -BNA达到0.1？％分别为24.9,11.2,16.7和11.2？多年，分别为298.15？K，这比NC（10.6？年）长。 UV-Vis显示，当NC /稳定剂热分解压力 - 时间曲线达到拐点时，稳定剂几乎消耗。基于上述结果，稳定性顺序是MNA＆我</ i> -PNA＆ ena＆ n </ i> -BNA作为拐点的时间准则。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29946/'>《Propellants, Explosives, Pyrotechnics》</a> <b style="margin: 0 2px;">|</b><span>2020年第6期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Luo Liqiong&option=202" target="_blank" rel="nofollow">Luo Liqiong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jin Bo&option=202" target="_blank" rel="nofollow">Jin Bo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chai Zuohu&option=202" target="_blank" rel="nofollow">Chai Zuohu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Huang Qiong&option=202" target="_blank" rel="nofollow">Huang Qiong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chu Shijin&option=202" target="_blank" rel="nofollow">Chu Shijin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Peng Rufang&option=202" target="_blank" rel="nofollow">Peng Rufang;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>State Key Laboratory of Environment-friendly Energy MaterialsSouthwest University of Science and TechnologySichuan Mianyang 621010 China;</p> <p>State Key Laboratory of Environment-friendly Energy MaterialsSouthwest University of Science and TechnologySichuan Mianyang 621010 China;</p> <p>State Key Laboratory of Environment-friendly Energy MaterialsSouthwest University of Science and TechnologySichuan Mianyang 621010 China;</p> <p>State Key Laboratory of Environment-friendly Energy MaterialsSouthwest University of Science and TechnologySichuan Mianyang 621010 China;</p> <p>State Key Laboratory of Environment-friendly Energy MaterialsSouthwest University of Science and TechnologySichuan Mianyang 621010 China;</p> <p>State Key Laboratory of Environment-friendly Energy MaterialsSouthwest University of Science and TechnologySichuan Mianyang 621010 China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1837.html" title="爆炸物工业、火柴工业">爆炸物工业、火柴工业;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nitrocellulose&option=203" rel="nofollow">Nitrocellulose;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Stabilizer&option=203" rel="nofollow">Stabilizer;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aniline&option=203" rel="nofollow">Aniline;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Isothermal thermal decomposition&option=203" rel="nofollow">Isothermal thermal decomposition;</a> </p> <div class="translation"> 机译：硝酸纤维素;稳定剂;苯胺;等温热分解; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" 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</span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020315143019.html">三唑酮及其盐的合成、结构、热分解机理、非等温热分解反应动力学及理论研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=马海霞&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 马海霞</a> <span> . 2004</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/061204564534.html">基于二苯胺和杂环二苯胺衍生物的高效磷稳定剂</a> <b>[P]</b> . <span> 中国专利： CN110573566B </span> <span> . 2021.07.30</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120101614939.html">基于二苯胺和杂环二苯胺衍生物的高效磷稳定剂</a> <b>[P]</b> . <span> 中国专利： CN110573566A </span> <span> . 2019-12-13</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130419435612.html">ISOTHERMAL/NON-ISOTHERMAL THERMOGRAVIMETRIC ANALYZER CAPABLE OF PRECISELY 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