Effect of Morphology for Ammonium Dinitramide on the Mechanical and Combustion Properties of Composite Propargyl‐terminated Copolyether Propellant

Gong Li; Li Yonghui; Guo Yanpei; Li Jianmin; Yang Rongjie

摘要

Abstract > Because the isocyanate‐crosslinked copolyether binder system has poor compatibility with ammonium dinitramide (ADN), the click‐chemistry propargyl‐terminated ethylene oxide‐tetrahydrofuran copolyether (PTPET) binder cured by multi‐functional azide is introduced. In the solid propellant, the effects of spherical ADN and flaky ADN on the mechanical and combustion properties of PTPET solid propellants were investigated. The results show that the mechanical properties of the propellant prepared with the ADN‐spherical were comprehensively better than those of the propellant prepared with the ADN‐flaky. The ? <sub>b</sub> /? <sub>m</sub> of the propellant with ADN‐spherical was obviously lower than that of the propellant with ADN‐flaky when the temperature at ?40?°C. There was a sharp peak around ?40?°C, followed by a broad peak, and a step rise near 40?°C about the DMA curves of both propellants. The burning rate measurement results showed that propellant prepared with flaky ADN had the higher burning rate at 3–17?MPa. The flame structures of both propellants showed stable combustion but the size of aluminum particles in flame zone for the propellant prepared with flaky ADN was larger. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 因为异氰酸酯交联的共聚醚粘合剂体系与二硝基酰胺（ADN）相容差，引入了通过多官能叠氮化物固化的咔哒化学炔丙基封端的环氧乙烷 - 四氢呋喃共解醚（PTPET）粘合剂。在固体推进剂中，研究了球形ADN和FLAKY ADN对PTPET固体推进剂的机械和燃烧性能的影响。结果表明，用ADN球形制备的推进剂的机械性能综合地优于用ADN-片状制备的推进剂的机械性能。这？ <sub> b </ sub> /？ <sub> m </ sub> 当温度在α4℃的温度时，具有AdN球形的推进剂显着低于adn-flaky的推进剂。周围有一个尖峰？40？°C，随后是一个宽峰，并且关于两个推进剂的DMA曲线近40°C的台阶上升。燃烧速率测量结果表明，用薄片ADN制备的推进剂在3-17℃下具有较高的燃烧速率。两种推进剂的火焰结构显示出稳定的燃烧，但用薄片ADN制备的推进剂的火焰区中的铝颗粒的尺寸较大。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29946/'>《Propellants, Explosives, Pyrotechnics》</a> <b style="margin: 0 2px;">|</b><span>2020年第6期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gong Li&option=202" target="_blank" rel="nofollow">Gong Li;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Yonghui&option=202" target="_blank" rel="nofollow">Li Yonghui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Guo Yanpei&option=202" target="_blank" rel="nofollow">Guo Yanpei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Jianmin&option=202" target="_blank" rel="nofollow">Li Jianmin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Rongjie&option=202" target="_blank" rel="nofollow">Yang Rongjie;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of Materials Science and Engineering Key Laboratory for Ministry of Education of High Energy Density MaterialBeijing Institute of TechnologyBeijing People's Republic of China;</p> <p>School of Materials Science and Engineering Key Laboratory for Ministry of Education of High Energy Density MaterialBeijing Institute of TechnologyBeijing People's Republic of China;</p> <p>School of Materials Science and Engineering Key Laboratory for Ministry of Education of High Energy Density MaterialBeijing Institute of TechnologyBeijing People's Republic of China;</p> <p>School of Materials Science and Engineering Key Laboratory for Ministry of Education of High Energy Density MaterialBeijing Institute of TechnologyBeijing People's Republic of China;</p> <p>School of Materials Science and Engineering Key Laboratory for Ministry of Education of High Energy Density MaterialBeijing Institute of TechnologyBeijing People's Republic of China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1837.html" title="爆炸物工业、火柴工业">爆炸物工业、火柴工业;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ammonium dinitramide&option=203" rel="nofollow">Ammonium dinitramide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Morphology&option=203" rel="nofollow">Morphology;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mechanical property&option=203" rel="nofollow">Mechanical property;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Combustion property&option=203" rel="nofollow">Combustion property;</a> </p> <div class="translation"> 机译：二硝酰胺铵;形态;力学性质;燃烧性; 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