Arylamine polymers prepared via facile paraldehyde addition condensation: an effective hole‐transporting material for perovskite solar cells

Suwa Koki; Tanaka Suguru; Oyaizu Kenichi; Nishide Hiroyuki

摘要

Abstract > Arylamine polymers were prepared via the facile one‐step addition condensation of <fi>N</fi> , <fi>N</fi> ′‐diphenyl‐ <fi>N</fi> , <fi>N</fi> ′‐bis(4‐methylphenyl)‐1,4‐phenylenediamine and 4‐methoxytriphenylamine with paraldehyde. The polymers were highly soluble in common organic solvents. The non‐conjugated arylamine polymer structure was characterized and found to form tough, homogeneous, amorphous layers with a glass transition temperature above 200?°C on a substrate by a simple spin‐coating process. The polymer layers exhibited a hole mobility of the order of 10 ?5 ?cm 2 ?V ?1 ?s ?1 , which was comparable with those of previously reported arylamine polymers, and a highest occupied molecular orbital level of ?5.38?eV appropriate for the hole‐transporting layer of perovskite solar cells. The perovskite cells fabricated with the polymers gave a photovoltaic conversion efficiency of 16.0%. ? 2018 Society of Chemical Industry </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <标题类型=“main”>抽象</ title> > 通过容易的一步添加凝结制备芳基胺聚合物 <fi> n </ fi> 那 <fi> n </ fi> '-联苯- <fi> n </ fi> 那 <fi> n </ fi> '-bis（4-甲基苯基）-1,4-苯二胺和4-甲氧基苯胺与仲醛。聚合物高度可溶于普通的有机溶剂。特征和发现非缀合的芳基胺聚合物结构，并发现通过简单的旋涂工艺在底物上以高于200℃的玻璃化转变温度的坚韧，均匀的无定形层。聚合物层表现出10级的空穴迁移率10 ？5 </ sup> ？厘米 2 </ sup> ？V. ？1 </ sup> ？S. ？1 </ sup> ，与先前报道的芳基胺聚合物的那些相当，以及最高占用的分子轨道水平的α.5.38？适用于钙钛矿太阳能电池的空穴传输层。用聚合物制造的钙钛矿细胞使光伏转化效率为16.0％。还2018年化学工业学会 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29710/'>《Polymer international》</a> <b style="margin: 0 2px;">|</b><span>2018年第6期</span><b style="margin: 0 2px;">|</b><span>共5页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Suwa Koki&option=202" target="_blank" rel="nofollow">Suwa Koki;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tanaka Suguru&option=202" target="_blank" rel="nofollow">Tanaka Suguru;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Oyaizu Kenichi&option=202" target="_blank" rel="nofollow">Oyaizu Kenichi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nishide Hiroyuki&option=202" target="_blank" rel="nofollow">Nishide Hiroyuki;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Applied ChemistryWaseda UniversityTokyo Japan;</p> <p>Department of Applied ChemistryWaseda UniversityTokyo Japan;</p> <p>Department of Applied ChemistryWaseda UniversityTokyo Japan;</p> <p>Department of Applied ChemistryWaseda UniversityTokyo Japan;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1185.html" title="高分子化学（高聚物）">高分子化学（高聚物）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=arylamine polymer&option=203" rel="nofollow">arylamine polymer;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=addition condensation&option=203" rel="nofollow">addition condensation;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hole‐transporting material&option=203" rel="nofollow">hole‐transporting material;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=perovskite solar cell&option=203" rel="nofollow">perovskite solar cell;</a> </p> <div class="translation"> 机译：芳基胺聚合物;添加冷凝;空穴传输材料;钙钛矿太阳能电池; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" 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