Surface, interface and electronic properties of F8:F8BT  polymeric thin films used for organic light‐emitting diode applications

Borges Bruno GAL; Veiga Amanda G; Gioti Maria; Laskarakis Argiris; Tzounis Lazaros; Logothetidis Stergios; Rocco Maria Luiza M

摘要

Abstract > Ultrathin polymeric films consisting of poly(9,9‐di‐ <fi>n</fi> ‐octylfluorenyl‐2,7‐diyl) (F8) blended with poly(9,9‐dioctylfluorene‐ <fi>alt</fi> ‐benzothiadiazole) (F8BT) grown onto PEDOT:PSS/ITO/PET were investigated by X‐ray photoelectron spectroscopy (XPS), depth‐profiling XPS, reflection electron energy loss spectroscopy (REELS) and angle‐dependent X‐ray absorption spectroscopy (XAS) to gain information on the films' electronic, order and interface properties. AFM studies provide valuable information on the films' nanotopographical properties and homogeneity. Spectroscopic ellipsometry and photoluminescence spectroscopy were used also to obtain information on the optoelectronic properties. Well‐ordered films were observed from the XAS analysis, measured at the sulfur K absorption edge. XPS measurements demonstrated that the surface composition of the polymer thin films prepared by a spin‐coating wet‐chemical deposition method matches the expected F8:F8BT blend stoichiometry. The interfacial properties were studied through an argon ion sputtering process coupled to the XPS acquisition, showing an enhancement of oxygen components at the interface. The films' inhomogeneity was verified by AFM images and analysis. We obtained a value of 3.1 eV as the electronic bandgap of the F8:F8BT film from REELS data, whereas analysis of the spectroscopic ellipsometry spectra revealed that the optical bandgap of F8:F8BT has a value of 2.4 eV. A strong green emission was obtained for the produced films, which is in agreement with the expected emission due to the 1:19 ratio of the F8 and F8BT blended polymers. ? 2018 Society of Chemical Industry </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <标题类型=“main”>抽象</ title> > 超薄聚合物膜组成的聚（9,9-二 - <fi> n </ fi> - 与聚（9,9-二辛基氟烯 - <fi> alt </ fi> Benzothiadozole）（F8BT）生长在PEDOT上：通过X射线光电子能谱（XPS），深度分析XPS，反射电子能损光谱（REELS）和角度依赖性X射线吸收光谱（ XAS）获取有关电影电子，秩序和接口属性的信息。 AFM研究提供了有关薄膜的纳米模式和均匀性的有价值的信息。使用光谱椭圆形和光致发光光谱法也用于获得有关光电性质的信息。从XAS分析中观察到良好的薄膜，在硫磺K吸收边缘测量。 XPS测量表明，通过旋涂湿化学沉积方法制备的聚合物薄膜的表面组成与预期的F8：F8BT混合化学计量相匹配。通过耦合到XPS采集的氩离子溅射工艺研究界面性质，显示界面处的氧部件的增强。通过AFM图像和分析验证了膜的不均匀性。我们获得了从卷轴数据的F8：F8BT膜的电子带隙的值为3.1eV，而光谱椭圆形光谱的分析表明F8：F8BT的光学带隙具有2.4eV的值。由于F8和F8BT共混聚合物的1:19比例，所生产的薄膜获得强大的绿色发射，这是与预期发射的预期发射。还2018年化学工业学会 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29710/'>《Polymer international》</a> <b style="margin: 0 2px;">|</b><span>2018年第6期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Borges Bruno GAL&option=202" target="_blank" rel="nofollow">Borges Bruno GAL;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Veiga Amanda G&option=202" target="_blank" rel="nofollow">Veiga Amanda G;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gioti Maria&option=202" target="_blank" rel="nofollow">Gioti Maria;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Laskarakis Argiris&option=202" target="_blank" rel="nofollow">Laskarakis Argiris;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tzounis Lazaros&option=202" target="_blank" rel="nofollow">Tzounis Lazaros;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Logothetidis Stergios&option=202" target="_blank" rel="nofollow">Logothetidis Stergios;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rocco Maria Luiza M&option=202" target="_blank" rel="nofollow">Rocco Maria Luiza M;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Institute of ChemistryFederal University of Rio de JaneiroRio de Janeiro RJ Brazil;</p> <p>Institute of ChemistryFederal University of Rio de JaneiroRio de Janeiro RJ Brazil;</p> <p>Laboratory for Thin Films Nanobiomaterials?–?Nanosystems and Nanometrology (LTFN) Physics DepartmentAristotle University of ThessalonikiThessaloniki Greece;</p> <p>Laboratory for Thin Films Nanobiomaterials?–?Nanosystems and Nanometrology (LTFN) Physics DepartmentAristotle University of ThessalonikiThessaloniki Greece;</p> <p>Laboratory for Thin Films Nanobiomaterials?–?Nanosystems and Nanometrology (LTFN) Physics DepartmentAristotle University of ThessalonikiThessaloniki Greece;</p> <p>Laboratory for Thin Films Nanobiomaterials?–?Nanosystems and Nanometrology (LTFN) Physics DepartmentAristotle University of ThessalonikiThessaloniki Greece;</p> <p>Institute of ChemistryFederal University of Rio de JaneiroRio de Janeiro RJ Brazil;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1185.html" title="高分子化学（高聚物）">高分子化学（高聚物）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=conjugated polymers&option=203" rel="nofollow">conjugated polymers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thin films&option=203" rel="nofollow">thin films;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electronic properties&option=203" rel="nofollow">electronic properties;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=photoemission&option=203" rel="nofollow">photoemission;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=OLEDs&option=203" rel="nofollow">OLEDs;</a> </p> <div class="translation"> 机译：共轭聚合物;薄膜;电子特性;光曝光;OLEDS; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704023604550.html">Surface, interface and electronic properties of F8:F8BT polymeric thin films used for organic light-emitting diode applications</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Borges Bruno G. 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