Facile fabrication of PbS/MoS<ce:inf loc='post'>2</ce:inf> nanocomposite photocatalyst with efficient photocatalytic activity under visible light
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Facile fabrication of PbS/MoS2 nanocomposite photocatalyst with efficient photocatalytic activity under visible light

机译:PBS / MOS 2> 2 纳米复合光催化剂,具有高效的光催化活性在可见光下

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摘要

Abstract A PbS/MoS2 nanocomposite was synthesized in different molar ratio of PbS 0.5%, 1.0% and 1.5% by precipitation – deposition method and successfully characterized by various instrumental techniques such as UV–visible diffuse reflectance spectra (DRS), X-ray diffraction (XRD), Scanning electron microscopy (SEM), Energy dispersive X-ray spectrometry (EDX), BET-surface area, photoluminescence (PL) spectroscopy. The photocatalytic activity was monitored via the degradation of methylene blue dye and the results revealed that 1% PbS/MoS2 shows better photocatalytic activity than that of 0.5%PbS/MoS2 and 1.5%PbS/MoS2. The effect of operational parameters such as pH and catalyst dosage on the photocatalytic activity was investigated. The PbS-MoS2 nanocomposite exhibit excellent photocatalytic degradation on methylene blue (MB) dye under visible light irradiation. Graphical abstract Display Omitted Highlights ? PbS- MoS2 nanocomposites were prepared by precipitation – deposition method. ? The degradation of methylene blue using PbS- MoS2 nanocomposites. ? PbS- MoS2 nanocomposites can act as an good photocatalytic activity. ]]>
机译:<![CDATA [ 抽象 PBS / MOS 2 纳米复合材料通过沉淀沉积方法的PBS 0.5%,1.0%和1.5%的不同摩尔比合成,并通过各种仪器技术成功表征,例如UV可见漫射反射谱(DRS),X射线衍射(XRD),扫描电子显微镜(SEM),能量分散X射线光谱法(EDX),BET表面积,光致发光(PL)光谱。通过亚甲基蓝染料的降解监测光催化活性,结果显示,1%PBS / MOS 2 显示出比0.5%PBS的更好的光催化活性/ MOS 2 和1.5%PBS / MOS 2 。研究了诸如pH和催化剂剂量的操作参数对光催化活性的影响。 PBS-MOS 2 纳米复合材料在可见光照射下在亚甲基蓝(MB)染料上表现出优异的光催化降解。 图形抽象 显示省略 突出显示 PBS-MOS 2 纳米复合材料通过沉淀沉积方法制备。 使用PBS-MOS的亚甲基蓝的劣化:inf loc =“post”> 2 纳米复合材料。 ?< / ce:标签> pbs-mos 2 纳米复合材料可以充当良好的光催化活性。< / ce:para> ] ]

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