Synthesis and structure of potassium 2-(pyridin-2-yl)-1H-benzo[d]imidazolate and preparation of related bis(diimine) ligands

Ilicheva A. I.; Baranov E. V.; Begantsova Yu. E.; Varvarin A. E.; Bochkarev L. N.

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Synthesis and structure of potassium 2-(pyridin-2-yl)-1H-benzo[d]imidazolate and preparation of related bis(diimine) ligands

机译：钾的合成与结构2-（吡啶-2-基）-1H-苯并[D]咪唑酸酯和相关双（二氰）配体的制备

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摘要

A potassium derivative of 2-(pyridin-2-yl)-1H-benzo[d]imidazole (BenzimidK) is synthesized and structurally characterized (DIF file CCDC no. 1478559). The complex is used for the preparation of new bis(diimine) ligands containing different diimine fragments linked by the bridging (CH2)(4) group.

机译：合成和结构表征的2-（吡啶-2-基）-1H-苯并[d]咪唑（Benzimidk）的钾衍生物（D <倒置感叹号>如果文件CCDC NO。1478559）。该复合物用于制备含有由桥接（CH2）（4）组连接的不同二氰基片段的新BIS（二氰）配体。

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来源
《Russian Journal of Coordination Chemistry》 |2017年第2期|共7页
作者
Ilicheva A. I.; Baranov E. V.; Begantsova Yu. E.; Varvarin A. E.; Bochkarev L. N.;
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作者单位

Russian Acad Sci Razuvaev Inst Organometall Chem Nizhnii Novgorod Russia;

Russian Acad Sci Razuvaev Inst Organometall Chem Nizhnii Novgorod Russia;

Russian Acad Sci Razuvaev Inst Organometall Chem Nizhnii Novgorod Russia;

Russian Acad Sci Razuvaev Inst Organometall Chem Nizhnii Novgorod Russia;

Russian Acad Sci Razuvaev Inst Organometall Chem Nizhnii Novgorod Russia;

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正文语种 eng
中图分类化学;
关键词
potassium; benzimidazole; coordination polymers; diimine ligands;

机译：钾;苯并咪唑;配位聚合物;二亚胺配体;

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1. Synthesis and structure of potassium 2-(pyridin-2-yl)-1H-benzo[d]imidazolate and preparation of related bis(diimine) ligands [J] . Ilicheva A. I., Baranov E. V., Begantsova Yu. E., Russian Journal of Coordination Chemistry . 2017,第2期

机译：钾的合成与结构2-（吡啶-2-基）-1H-苯并[D]咪唑酸酯和相关双（二氰）配体的制备
2. Synthesis and crystal structure of a novel multimodal ligand, 6,6'-bis(2-(di(pyridin-2-yl)methylene)-1-methylhydrazinyl)-2,2'-bipyridine, and its copper(I) complex, {[Cu_3L_2](PF_6)_3° 3H_2O} (1) [J] . ?A?LAR A?A?, ?SMA?L YILMAZ, ABDURRAHMAN ?ENGüL, Turkish journal of chemistry . 2010,第5期

机译：新型多峰配体6,6'-双（2-（二（吡啶-2-基）亚甲基）-1-甲基肼基）-2,2'-联吡啶及其铜（I）配合物的合成和晶体结构，{[Cu_3L_2]（PF_6）_3°3H_2O}（1）
3. Crystal structures of bis-[2-(pyridin-2-yl)phenyl-κ2N,C1]rhodium(III) complexes containing an aceto-nitrile or monodentate thyminate(1?) ligand [J] . Sakate M., Hosoda H., Suzuki T. Acta Crystallographica Section E: Crystallographic Communications . 2016,第4期

机译：含乙腈或单齿胸苷（1？）配体的双-[2-（吡啶-2-基）苯基-κ2N，C1]铑（III）配合物的晶体结构
4. Synthesis of Titanium(IV) Complexes that Contain the Bis(silylamide) Ligand of the Type 1,8-C_(10)H_6(NR)_2~(2-) (R = SiMe_3, Si~tBuMe_2, Si~iPr_3), and Olefin Polymerization Catalyzed by the 1,8-C_(10)H_6(NR)_2 TiX_2(X = Cl, Br)-cocatalyst Syste [C] . Kazuo Takaoki, Kotohiro Nomura, Naofumi Naga, Tokyo conference on advanced catalytic science and technology . 1999

机译：含有双（甲硅烷酰亚胺）配体的钛（IV）配合物的合成1,8-C_（10）H_6（NR）_2〜（2-）（R = SIME_3，SI〜TBUME_2，SI〜IPR_3 ）和烯烃聚合由1,8-C_（10）H_6（NR）_2 Tix_2（x = Cl，Br） - 催化剂系统催化
5. Elucidating photophysical attributes of alpha,alpha'-diimine ligands, rhodium(III) dicyano-bis (alpha,alpha'-diimine) and tris(alpha,alpha'-diimine) complexes via ab inition and density-functional calculations. [D] . Matz, Phillip Daniel. 2002

机译：阐明了α，α'-二亚胺配体，铑（III）二氰基双（α，α'-二亚胺）和三（α，α'-二亚胺）配合物的光物理属性，方法是通过原子和密度函数计算。
6. Crystal structures of bis2-(pyridin-2-yl)phenyl-κ2NC1rhodium(III) complexes containing an acetonitrile or monodentate thyminate(1−) ligand [O] . Mika Sakate, Haruka Hosoda, Takayoshi Suzuki 2016

机译：双 2-（吡啶-2-基）苯基-κ2的晶体结构碳氮1含乙腈或单齿胸苷（1-）配体的铑（III）配合物
7. Crystal structures of bis[2-(pyridin-2-yl)phenyl-κ2N,C1]rhodium(III) complexes containing an acetonitrile or monodentate thyminate(1−) ligand [O] . Mika Sakate, Haruka Hosoda, Takayoshi Suzuki 2016

机译：含有乙腈或单齿盐酸盐（1-）配体的双[2-（吡啶-2-基）苯基-κ2N，C1]铑（III）配合物的晶体结构

Synthesis and structure of potassium 2-(pyridin-2-yl)-1H-benzo[d]imidazolate and preparation of related bis(diimine) ligands

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