Reaction 5-(Arylmethylidene)-2,4,6-pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Phenylhydrazones in the Presence of Sodium N-Chlorobenzenesulfonamide

Tyrkov A. G.; Yurtaeva E. A.; Rsaeva O. B.

首页> 外文期刊>Russian Journal of Organic Chemistry >Reaction 5-(Arylmethylidene)-2,4,6-pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Phenylhydrazones in the Presence of Sodium N-Chlorobenzenesulfonamide

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Reaction 5-(Arylmethylidene)-2,4,6-pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Phenylhydrazones in the Presence of Sodium N-Chlorobenzenesulfonamide

机译：反应5-（芳基甲基）-2,4,6-嘧啶-2,4,6（1H，3H，5H） - 在N-氯苯磺酰胺存在下与亚癸酰甲醛苯基缺水剂

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The reactions of 5-(arylmethylidene)-2,4,6-pyrimidine-2,4,6(1H,3H,5H)-triones with arenecarbaldehyde phenylhydrazones in the presence of sodium N-chlorobenzenesulfonamide give 2,3,7,9-tetraasaspiro-[4.5]dec-1-ene-6,8,10-triones in yields of 30-45%.

机译：在N-氯苯磺酰胺钠存在下，用仲二甲醛苯基缺水的5-（芳基甲基）-2,4,6-嘧啶-2,4,6（1H，3H，5H）-2,4,6（1H，3H，5H）的反应给予2,3,7,9 -tetraasaspiro-[4.5] 12-1-eNE-6,8,10-10-产量为30-45％。

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来源
《Russian Journal of Organic Chemistry》 |2019年第2期|共4页
作者
Tyrkov A. G.; Yurtaeva E. A.; Rsaeva O. B.;
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作者单位

Astrakhan State Univ Pl Shaumyana 1 Astrakhan 414000 Russia;

Minist Hlth Russian Federat Inst Leprosy Res Per N Ostrovskogo 3 Astrakhan 414057 Russia;

Astrakhan State Univ Pl Shaumyana 1 Astrakhan 414000 Russia;

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正文语种 eng
中图分类有机化学;
关键词
5-(arylmethylidene)-2; 4; 6-pyrimidine-2; 4; 6(1H; 3H; 5H)-triones; arenecarbaldehyde phenylhydrazones; sodium N-chlorobenzenesulfonamide; 1; 3-dipolar cycloaddition; 2; 3; 7; 9-tetraazaspiro4.5dec1ene6; 8; 10-triones;

机译：5-（芳基甲基）-2;4;6-嘧啶-2;4;6（1H;3H;5H） - 甲苯磺酸苯肼;N-氯苯磺酰胺;1;3-偶极环形加法;2;3;7;9-tetraazaspiro [4.5] DEC1ENE6;8;10-TRIONES;

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1. Reaction 5-(Arylmethylidene)-2,4,6-pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Phenylhydrazones in the Presence of Sodium N-Chlorobenzenesulfonamide [J] . Tyrkov A. G., Yurtaeva E. A., Rsaeva O. B. Russian Journal of Organic Chemistry . 2019,第2期

机译：反应5-（芳基甲基）-2,4,6-嘧啶-2,4,6（1H，3H，5H） - 在N-氯苯磺酰胺存在下与亚癸酰甲醛苯基缺水剂
2. Synthesis and Antimycobacterial Activity of 5-(Hetarylmethylidene)-2,4,6-Pyrimidine-2,4,6(1H,3H,5H )-Triones And 5-(2-Chloropropylidene)-2,4,6-Pyrimidine-2,4,6(1H,3H,5H )-Triones [J] . Yushin M. Yu, Tyrkov A. G., Saroyants L. V, Pharmaceutical Chemistry Journal . 2020,第2期

机译：5-（hetarylmethylynylynylynidine-2,4,6（1H，3H，5H） - 十字和5-（2-氯丙烯）-2,4,6-嘧啶 - 的合成和抗致细胞活性 - 2,4,6（1h，3h，5h） - 轴
3. 5-(Arylmethylidene)-2,4,6-pyrimidine-2,4,6(1H,3H,5H)-triones in Reaction with p-Phenacyl- and p-Acetonylisoquinolinium bromides [J] . Tyrkov A. G., Nosachev S. B., Vladimirova T. S. Russian Journal of Organic Chemistry . 2016,第5期

机译：5-（芳基亚甲基）-2,4,6-嘧啶-2,4,6（1H，3H，5H）-三酮与对乙酰基和对乙酰基异喹啉溴化物反应
4. Glassy 2-(1-benzyl-2-styryl-6-methylpyridin-4(1-H)-ylidene) fragment containing 1H-indene-1,3(2H)-dione and pyrimidine-2,4,6(1H,3H,5H)-trione derivatives with light-emitting and amplified spontaneous emission properties [C] . Elmars Zarins, Julija Pervenecka, Elina Misina, Conference on Fiber Lasers and Glass Photonics: Materials through Applications . 2020

机译：含1H-茚-1,3（2H）-二酮和嘧啶-2,4,6（1H）的玻璃状2-（1-苄基-2-苯乙烯基-6-甲基吡啶-4（1-H）-亚烷基）片段具有发光和放大的自发发射特性的3H，5H）-三酮衍生物
5. Novel substituted (Z)-5-((N-benzyl-1H-indol-3-yl)methylene)imidazolidine-2,4-diones and 5-((N-benzyl-1H-indol-3-yl)methylene)pyrimidine-2,4,6(1H,3H,5H)-triones as potent radio-sensitizing agents [O] . Y. Thirupathi Reddy, Konjeti R. Sekhar, Nidhish Sasi, 2010

机译：新型取代（Z）-5 - （（N-苄基-1H-吲哚-3-基）亚甲基）咪唑烷-2,4-二乙酯和5-（（N-苄基-1H-吲哚-3-基）亚甲基）嘧啶-2,4,6（1H，3H，5H） - 标纹作为有效的无线电敏化剂
6. Results of a Local Lymph Node Assay in Mice (LLNA/IMDS) with Toluene Diisocyanate based adduct in Organic Solvent (TDI Trimer) 1,3,5-Triazine- 2,4,6(1H,3H,5H)-trione, 1,3,5-tris(3-isocya natomethylphenyl). [R] . 2011

机译：基于甲苯二异氰酸酯的有机溶剂加成物（TDI三聚体）1,3,5-三嗪-2,4,6（1H，3H，5H） - 三酮，1小鼠局部淋巴结检测结果（LLNa / ImDs），3,5-三（3-isocya natomethylphenyl）。

Reaction 5-(Arylmethylidene)-2,4,6-pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Phenylhydrazones in the Presence of Sodium N-Chlorobenzenesulfonamide

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