Synthesis of a 16-Membered P4N2 Macrocycle with Pyridyl-Substituted Phosphorus Atoms

Wittmann T. I.; Musina E. I.; Litvinov I. A.; Karasik A. A.; Sinyashin O. G.

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Synthesis of a 16-Membered P4N2 Macrocycle with Pyridyl-Substituted Phosphorus Atoms

机译：用吡啶基取代的磷原子合成16元P4N2大环缩合

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摘要

The first example of 16-membered aminomethylphosphines with pyridyl substituents on the phosphorus atom was synthesized as an RSSR isomer by covalent self-assembly in the system 1,3-bis[(pyridin-2-yl)phosphino]propane-formaldehyde-isopropylamine.

机译：通过在体系1,3-双[（吡啶-2-基）磷基丙烷 - 甲醛 - 异丙胺中，通过共价自组装合成具有磷原子上的吡啶基取代基的16-元氨基甲基膦的第一实例作为RSSR异构体。

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来源
《Russian Journal of General Chemistry》 |2018年第11期|共4页
作者
Wittmann T. I.; Musina E. I.; Litvinov I. A.; Karasik A. A.; Sinyashin O. G.;
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作者单位

Russian Acad Sci FRC Kazan Sci Ctr AE Arbuzov Inst Organ &

Phys Chem Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

Russian Acad Sci FRC Kazan Sci Ctr AE Arbuzov Inst Organ &

Phys Chem Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

Russian Acad Sci FRC Kazan Sci Ctr AE Arbuzov Inst Organ &

Phys Chem Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

Russian Acad Sci FRC Kazan Sci Ctr AE Arbuzov Inst Organ &

Phys Chem Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

Russian Acad Sci FRC Kazan Sci Ctr AE Arbuzov Inst Organ &

Phys Chem Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
macrocycle; corand; aminomethylphosphine; covalent self-assembly;

机译：宏循环;符合氨基甲基膦;共价自组装;

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专利

1. Synthesis of a 16-Membered P4N2 Macrocycle with Pyridyl-Substituted Phosphorus Atoms [J] . Wittmann T. I., Musina E. I., Litvinov I. A., Russian Journal of General Chemistry . 2018,第11期

机译：用吡啶基取代的磷原子合成16元P4N2大环缩合
2. Dinitrogen Reduction by a Chromium(0) Complex Supported by a 16-Membered Phosphorus Macrocycle [J] . Michael T.Mock, Shentan Chen, Molly OHagan, Journal of the American Chemical Society . 2013,第31期

机译：铬（0）配合物由一个十六元的磷大环化合物支持的二氮还原
3. Synthesis and characterization of metal-free phthalocyanine containing 16-membered N2S2-donor macrocycles linked to a 2-pyridinyl methyl moiety [J] . Nilgiin Kabay, Yasar Gok Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2013,第31期

机译：包含与2-吡啶基甲基部分连接的16元N2S2-供体大环的无金属酞菁的合成与表征
4. Novel Phosphorus Containing Macrocycles [C] . Journal of Tsinghua University: science and technology . 2001

机译：新型含大环磷
5. Molecular recognition and sensing by macrocycles: Synthesis and applications of macrocycles with convergent functionalities. [D] . Choi, Kihang. 2003

机译：大环化合物的分子识别和传感：具有聚合功能的大环化合物的合成和应用。
6. Synthesis and Characterizationof a Click-Assembled18-Atom Macrocycle That Displays Selective AXL Kinase Inhibitory Activity [O] . Olga Cruz-López, Carolin Temps, Beatrice Longo, 2019

机译：合成与表征点击组装的显示选择性AXL激酶抑制活性的18原子大环。
7. A New, Convenient Synthesis of the Linear Phosphazene Salt Cl3PdNdPCl3Cl: Preparation of Higher Linear Homologues Cl3PdN-(PCl2dN)xdPCl3Cl (x = 1-3) and the 16-Membered Macrocycle NCCl(NPCl2)32 [O] . -1

机译：一种新的，方便地合成线性磷腈盐Cl3PDNDPCl3Cl：较高线性同源物的制备Cl 3PDN-（PCL2DN）XDPCl3Cl（X = 1-3）和16-元宏晶的NCCl（NPCL2）32
8. Controlled Synthesis of Organic-Inorganic Polymers that Possess a Backbone of Phosphorus and Nitrogen Atoms [R] . Allcock, H. R. 1981

机译：具有磷和氮原子骨架的有机 - 无机聚合物的可控合成

Synthesis of a 16-Membered P4N2 Macrocycle with Pyridyl-Substituted Phosphorus Atoms

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