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Molybdenum Schiff base complex supported on MNPs as an efficient and easily recyclable catalyst in three-component Strecker reaction for synthesis of alpha-aminonitrile derivatives

机译:MNPS中的钼席氏孢子基综合体在三分 - 氨基腈衍生物的三分球反应中得到高效且可回收的催化剂,用于合成α-氨基腈衍生物

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摘要

An efficient and straight procedure has been described for one-pot multi-component synthesis of alpha-aminonitrile derivatives in the presence of a molybdenum Schiff base complex supported on magnetite nanoparticles as a heterogeneous catalyst. The synthesized catalyst was characterized by Fourier transform infrared, X-ray powder diffraction, vibrating sample magnetometry, scanning electron microscopy, energy dispersive X-ray and inductively coupled plasma atomic emission spectroscopy. The extensive substrate scopes, easy recoverability of the magnetite catalyst, solvent-free conditions, short reaction time and high yields of products make this protocol environmentally friendly, practical and economically attractive.
机译:已经在作为非均相催化剂上支持的磁铁矿纳米颗粒上负载的钼Schiff碱基络合物存在下进行一锅多组分合成α-氨基腈衍生物的一种有效和直接的程序。 合成催化剂的特征在于傅里叶变换红外,X射线粉末衍射,振动样品磁力学,扫描电子显微镜,能量分散X射线和电感耦合等离子体原子发射光谱。 广泛的基材范围,磁铁催化剂的易恢复性,无溶剂条件,短的反应时间和高产率的产品使得该方案环境友好,实用,经济上有吸引力。

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