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Preparation and Characterization of Highly Fluorescent TGA-CdTe Quantum Dot-Hyamine 1622 Additive Composite

机译:高荧光TGA-CDTE量子点型1622添加剂复合材料的制备与表征

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Objective: The aim of the present study was to prepare highly luminescent additive composite polymer with hyamine 1622 and Thioglycolic Acid (TGA) coated CdTe Quantum Dots (QDs). Methods: The additive nano-composite was synthesized by the colloid synthesis method for the first time. The properties like particle size, fluorescence efficiency, fluorescence imaging, self-assembling, quantum dots, encapsulation, etc. were characterized by the employing of instrumental techniques such as ~1H and ~(13)C NMR, Fourier Transform Infrared spectroscopy (FT-IR), BAB image analysis system spectroscopy, Atomic Force Microscopy (AFM), Transmission Electron Microscopy (TEM) and Energy Dispersive X-Ray Spectroscopy (EDS). Results: CdTe quantum dots were stabilized successfully in the solid phase by hydrophobic conversion with hyamine 1622 as the cationic surfactant. The experimental results show that the prepared composite is ideal for various applications, easily synthesized, safe, and maintain good fluorescence properties. Conclusion: The newly prepared additive nanocomposite having sharp and narrow excitation/emission properties is expected to be applicable in biomedical/analytical systems.
机译:目的:本研究的目的是制备高发光的添加剂复合聚合物,用红霉素1622和巯基乙酸(TGA)涂覆的CdTe量子点(QDS)。方法:第一次通过胶体合成方法合成添加剂纳米复合物。通过采用仪器技术,如〜1H和〜(13)C NMR,傅里叶变换红外光谱(FT- IR),BAB图像分析系统光谱,原子力显微镜(AFM),透射电子显微镜(TEM)和能量分散X射线光谱(EDS)。结果:通过用Hyamine 1622作为阳离子表面活性剂,通过疏水转化成功稳定CdTe量子点。实验结果表明,制备的复合材料是各种应用的理想选择,易于合成,安全,保持良好的荧光性能。结论:预期具有尖锐窄的激发/排放性能的新制备的添加剂纳米复合材料适用于生物医学/分析系统。

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