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首页> 外文期刊>Luminescence: The journal of biological and chemical luminescence >Characterization of a highly Al 3+3+ ‐selective fluorescence probe based on naphthalimide‐Schiff base and its application to practical water samples
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Characterization of a highly Al 3+3+ ‐selective fluorescence probe based on naphthalimide‐Schiff base and its application to practical water samples

机译：基于萘硫代胺 - 席夫底座的高度Al 3 + / sup> 3+ - 选择性荧光探针及其在实用水样中的应用

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Abstract > A new fluorescent Al 3+ ‐probe, N ‐allyl‐4‐[3,3′‐((2‐aminoethyl)azanediyl)‐bis( N ′‐(2‐hydroxybenzylidene)propanehy‐drazide)]‐1,8‐naphthalimide ( L ), was designed and synthesized based on 1,8‐naphthalimide. The probe L contains 1,8‐naphthalimide moiety as the fluorophore and a Schiff base as the recognition group. The structure of L was determined by single crystal X‐ray. L emission at 526?nm increased on addition of Al 3+ under excitation wavelength at 350?nm. L exhibited high selectivity and sensitivity fluorescence emission towards to Al 3+ in ethanol/Tris–HCl buffer solution (1:1, v /v, pH?=?7.2) as compared with other tested metal ions. A good linearity with a correlation coefficient (R 2 ) of 0.99 was observed in the concentration range 2–10?μM. The binding constant and the detection limit of L for Al 3+ were calculated to 2.6?×?10 4 ?M ?1 and 0.34?μM, respectively. The results of experiments that including Job plot, ultraviolet–visible (UV–Vis) light titration, fluorescence titration, ESI‐MS and 1 H NMR titration, indicated a 1:1 stoichiometric complex between L and Al 3+ . L was highly effective in monitoring Al 3+ in real‐life Yellow River and tap water samples. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >一个新的荧光Al 3 + </ sup> -probe， n </ i> allyl-4- [3,3' - （（2-氨基乙基）偶氮二酯 - （ n / el>' - （2-羟基苄基）丙烷hy-drazide）] - 1，基于1,8-萘二亚胺设计和合成了8-萘酰亚胺（ L </ b>）。探针 l </ b>含有1,8-萘酰亚胺部分，作为荧光团和席克碱作为识别组。 <B> L </ B>的结构由单晶X射线测定。 <B> L </ B>在526℃下发射在激发波长下在350℃下加入Al <Sup> 3 + </ sup>。 <B> L </ B>在乙醇/三-HCl缓冲溶液中向Al <Sup> 3 + / sop>展示了高选择性和敏感性荧光发射（1：1， v </ i> / v与其他测试金属离子相比，pH？=β7.2）。在浓度范围内，观察到0.99的相关系数（R <SUP> 2 </ sup>）的良好线性度在2-10Ωμm。将Al 3 + </ sup>的粘合常数和检测限为2.6？×10 4 </ sup>Δm？1 </ sup>和0.34？μm。包括作业曲线，紫外 - 可见（UV-VIS）光滴定，荧光滴定，ESI-MS和 1 </ sup> H NMR滴定的实验结果表明之间的1：1化学计量复合物l </ b>和Al 3 + </ sup>。 l </ b>在现实生活中的al 3 + </ sup>中非常有效，在现实生活中的黄河和自来水样本中。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-26441/'>《Luminescence: The journal of biological and chemical luminescence》</a> <b style="margin: 0 2px;">|</b><span>2018年第1期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shen Kesheng&option=202" target="_blank" rel="nofollow">Shen Kesheng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mao Shanshan&option=202" target="_blank" rel="nofollow">Mao Shanshan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shi Xinkui&option=202" target="_blank" rel="nofollow">Shi Xinkui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Fei&option=202" target="_blank" rel="nofollow">Wang Fei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xu Yuling&option=202" target="_blank" rel="nofollow">Xu Yuling;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aderinto Stephen Opeyemi&option=202" target="_blank" rel="nofollow">Aderinto Stephen Opeyemi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wu Huilu&option=202" target="_blank" rel="nofollow">Wu Huilu;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of Chemical and Biological EngineeringLanzhou Jiaotong UniversityLanzhou Gansu People's Republic of China;</p> <p>School of Chemical and Biological EngineeringLanzhou Jiaotong UniversityLanzhou Gansu People's Republic of China;</p> <p>School of Chemical and Biological EngineeringLanzhou Jiaotong UniversityLanzhou Gansu People's Republic of China;</p> <p>School of Chemical and Biological EngineeringLanzhou Jiaotong UniversityLanzhou Gansu People's Republic of China;</p> <p>School of Chemical and Biological EngineeringLanzhou Jiaotong UniversityLanzhou Gansu People's Republic of China;</p> <p>School of Chemical and Biological EngineeringLanzhou Jiaotong UniversityLanzhou Gansu People's Republic of China;</p> <p>School of Chemical and Biological EngineeringLanzhou Jiaotong UniversityLanzhou Gansu People's Republic of China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1345.html" title="生物光学">生物光学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=aluminium&option=203" rel="nofollow">aluminium;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=fluorescence probe&option=203" rel="nofollow">fluorescence probe;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=naphthalimide&option=203" rel="nofollow">naphthalimide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=recognition&option=203" rel="nofollow">recognition;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Schiff base&option=203" rel="nofollow">Schiff base;</a> </p> <div class="translation"> 机译：铝;荧光探针;萘胺;识别;Schiff Base; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704023986412.html">Characterization of a highly Al <sup >3+3+ ‐selective fluorescence probe based on naphthalimide‐Schiff base and its application to practical water samples</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shen Kesheng&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Shen Kesheng,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mao 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