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Rapid Green Synthesis and Characterization of Silver Nanoparticles Arbitrated by Curcumin in an Alkaline Medium

机译:碱性介质中丙烃仲裁银纳米颗粒的快速绿色合成及表征

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Green synthesis of silver nanoparticles is desirable practice. It is not only the required technique for industrial and biomedical purposes but also a promising research area. The aim of this study was to synthesize green curcumin silver nanoparticles (C-Ag NPs). The synthesis of C-Ag NPs was achieved by reduction of the silver nitrate (AgNO3) in an alkaline medium. The characterizations of the prepared samples were conducted by ultraviolet visible (UV-vis) spectroscopy, powder X-ray diffraction (PXRD), field emission scanning electron microscopy (FESEM), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED) and zeta potential (ZP) analyses. The formation of C-Ag NPs was evaluated by the dark color of the colloidal solutions and UV-vis spectra, with 445 nm as the maximum. The size of the crystalline nanoparticles, recorded as 12.6 +/- 3.8nm, was confirmed by HRTEM, while the face-centered cubic (fcc) crystallographic structure was confirmed by PXRD and SAED. It is assumed that green synthesized curcumin silver nanoparticles (C-Ag NPs) can be efficiently utilized as a strong antimicrobial substance for food and meat preservation due to their homogeneous nature and small size.
机译:银纳米粒子的绿色合成是理想的实践。它不仅是工业和生物医学目的所需的技术,而且是一个有前途的研究区。本研究的目的是合成绿色姜黄素银纳米颗粒(C-Ag NPS)。通过在碱性培养基中还原硝酸银(AgNO 3)来实现C-Ag NP的合成。制备样品的特征是通过紫外线可见(UV-VI)光谱,粉末X射线衍射(PXRD),场发射扫描电子显微镜(FESEM),高分辨率透射电子显微镜(HRTEM),选定区域电子衍射,粉末X射线衍射(PXRD)进行。 (SAED)和Zeta潜力(ZP)分析。通过胶体溶液和UV-Vis光谱的暗颜色评估C-Ag NP的形成,最大445nm。通过HRTEM确认记录为12.6 +/- 3.8nm的结晶纳米颗粒的尺寸,同时通过PXRD确认朝向立方(FCC)晶体结构并落下。假设绿色合成姜黄素银纳米颗粒(C-Ag NPS)可以有效地用作由于其均匀性质和体积小而有效地用作食物和肉类保存的强抗微生物物质。

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