Influence of Anion and Crosslink Density on the Ionic Conductivity of 1,2,3‐Triazolium‐Based Poly(ionic liquid) Polyester Networks

Nguyen Anh; Rhoades Taylor C.; Johnson R. Daniel; Miller Kevin M.

摘要

Abstract > Covalently crosslinked, 1,2,3‐triazolium‐containing poly(ionic liquid) networks are prepared using Michael addition polymerization. Crosslink density and counteranion are varied in order to decipher the relationships between poly(ionic liquid) (PIL) structure and their thermal, mechanical, and conductive properties. An increase in acrylate concentration leads to a higher crosslink density, as reflected by an increase in the differential scanning calorimetry T <sub>g</sub> , dynamic mechanical analyzer E ′, and a decrease in the ionic conductivity. Most notable with variable counteranion PILs is that analysis of the ionic conductivity curves reveals a common “crossover” point at ≈85 °C (same acrylate:acetoacetate ratio). Below this crossover temperature, the ionic conductivity appears to be more dependent upon network/polymer chain dynamics. Above 85 °C, the conductivity correlates best with the size of the counteranion. All of the PILs reported here exhibit good ionic conductivities (10 ?6 to 10 ?8 S cm ?1 @25 °C, 30% RH), supporting the notion that 1,2,3‐triazolium‐containing PILs represent a vastly underrated electroactive material platform. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> >共价交联，使用迈克尔加成聚合制备含有1,2,3-三唑鎓的聚（离子液体）网络。改变交联密度和对抗以破译聚（离子液体）（Pil）结构与其热，机械和导电性能之间的关系。丙烯酸酯浓度的增加导致更高的交联密度，如差分扫描量热法的增加反射，如差示扫描量热率 t </ i> <sub> g </ sub>，动态机械分析仪 e </ i> '，并降低离子电导率。可变对抗桩最值得注意的是，离子电导率曲线的分析显示≈85℃（相同的丙烯酸酯：乙酰乙酸酯比例）的常见“交叉”点。低于该交叉温度，离子电导率似乎更依赖于网络/聚合物链动力学。在85°C以上，电导率最佳地与抵抗的大小相关。这里报道的所有含量表现出良好的离子电导率（10 β6</ sup>至10 β8</ sup> s cm 1 </ sup> @ 25°C，30％ RH），支持含1,2,3-三唑粒的Pils代表巨大低低得低得出的电活性材料平台的观念。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" > 著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-24310/'>《Macromolecular chemistry and physics 》</a> <b style="margin: 0 2px;">|</b><span>2017年第21期</span><b style="margin: 0 2px;">|</b> <span>共1页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nguyen Anh&option=202" target="_blank" rel="nofollow">Nguyen Anh;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rhoades Taylor C.&option=202" target="_blank" rel="nofollow">Rhoades Taylor C.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Johnson R. Daniel&option=202" target="_blank" rel="nofollow">Johnson R. Daniel;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Miller Kevin M.&option=202" target="_blank" rel="nofollow">Miller Kevin M.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>1201 Jesse D. Jones HallMurray State UniversityMurray KY 42071 USA;</p> <p>1201 Jesse D. Jones HallMurray State UniversityMurray KY 42071 USA;</p> <p>1201 Jesse D. Jones HallMurray State UniversityMurray KY 42071 USA;</p> <p>1201 Jesse D. Jones HallMurray State UniversityMurray KY 42071 USA;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li> <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span> <a href="https://www.zhangqiaokeyan.com/clc/1185.html" title="高分子化学（高聚物）">高分子化学（高聚物） ;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=1&option=203" rel="nofollow">1;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=2&option=203" rel="nofollow">2;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=3‐triazolium&option=203" rel="nofollow">3‐triazolium;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ionic conductivity&option=203" rel="nofollow">ionic conductivity;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Michael addition&option=203" rel="nofollow">Michael addition;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=poly(ionic liquid)&option=203" rel="nofollow">poly(ionic liquid);</a> </p> <div class="translation"> 机译：1;2;3-三唑鎓;离子电导率;迈克尔加成;聚（离子液体）; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704023544941.html">Influence of Anion and Crosslink Density on the Ionic Conductivity of 1,2,3‐Triazolium‐Based Poly(ionic liquid) Polyester Networks</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nguyen Anh&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Nguyen Anh,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rhoades Taylor C.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Rhoades Taylor C.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Johnson R. 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class="enjiyixqcontent" href="/patent-detail/06120102587332.html">2-(1,2,3-三唑-2-基)苯甲酰胺及3-(1,2,3-三唑-2-基)吡啶酰胺衍生物</a> <b>[P]</b> . <span> 中国专利： CN103917538A </span> <span> . 2014-07-09</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130422033260.html">3-METHYL-1,4-SUBSTITUTED 1,2,3-TRIAZOLIUM-BASED IONIC LIQUID AND A METHOD FOR MANUFACTURING THE SAME</a> <b>[P]</b> . <span> 外国专利：  KR20120067257A </span> <span> . 2012-06-25</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：3-甲基-1,4-取代的1,2,3-三唑基离子液体及其制造方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130415220928.html">1,2,3-triazolium ionic liquids</a> <b>[P]</b> . <span> 外国专利：  US8907105B1 </span> <span> . 2014-12-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：1,2,3-三唑鎓离子液体 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130415223788.html">Method of purifying a gas stream using 1,2,3-triazolium ionic liquids</a> <b>[P]</b> . <span> 外国专利：  US8906135B1 </span> <span> . 2014-12-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用1,2,3-三唑鎓离子液体净化气流的方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704023544941','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div 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