Time‐Lapsing Evaluation of the Retardation Behaviour of Polypropylene Homo‐ and Copolymers using the Stepped Isothermal Method based on Depth‐Sensing Macroindentation

Krolopp Tobias; Lach Ralf; Sch?ne Jan; Mecklenburg Thomas; Langer Beate; Grellmann Wolfgang

摘要

Summary <section xml:id="masy201600137-sec-0001"> >The Stepped Isothermal Method (SIM) is a relatively new method for accelerated determination of the creep behaviour of polymers. The need for such a new method arises from the fact that for modern plastic components such as pipe systems minimum lifetimes of 50 years and more are achieved. The analysis of creep applying conventional methods of testing over such long periods of time is not reasonable from an economic point of view. This forms the basis for the development of accelerated procedures such as SIM. Plastic components can exhibit creep characteristics to be a function of the position due to processing. Such position‐dependent creep behaviour cannot be imaged by volume‐sensitive creep tests such as SIM under uniaxial tensile load. Therefore, SIM was implemented by means of recording macroindentation to characterize the local long‐time creep behaviour and the expressiveness of this method for different polypropylene materials was shown in this study. </section> </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <标题类型=“main”>摘要</ title> <第XML：ID =“Masy201600137-SEC-0001”> 阶梯式等温法（SIM）是一种相对较新的方法，用于加速聚合物的蠕变行为的测定。对于这种新方法的需求产生的是，对于现代塑料部件，例如管材系统的最小寿命，实现了50岁以上。在长时间施用常规测试方法的蠕变分析与经济的观点来说不合理。这构成了发展加速程序，如SIM。由于加工，塑料部件可以表现出蠕变特性以成为位置的函数。这种位置依赖性蠕变行为不能通过单轴拉伸载荷如SIM等体积敏感的蠕变试验成像。因此，通过记录宏观晶体来实现SIM，以表征局部长时间蠕变行为，本研究显示了这种不同聚丙烯材料方法的表达性。</ p> </部分> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-24298/'>《Macromolecular symposia》</a> <b style="margin: 0 2px;">|</b><span>2017年第1期</span><b style="margin: 0 2px;">|</b><span>共1页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Krolopp Tobias&option=202" target="_blank" rel="nofollow">Krolopp Tobias;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lach Ralf&option=202" target="_blank" rel="nofollow">Lach Ralf;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sch?ne Jan&option=202" target="_blank" rel="nofollow">Sch?ne Jan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mecklenburg Thomas&option=202" target="_blank" rel="nofollow">Mecklenburg Thomas;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Langer Beate&option=202" target="_blank" rel="nofollow">Langer Beate;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Grellmann Wolfgang&option=202" target="_blank" rel="nofollow">Grellmann Wolfgang;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Akademie Mitteldeutsche Kunststoffinnovation (AMK)Eberhard‐Leibnitz‐Stra?e 206217 Merseburg Germany;</p> <p>Polymer Service GmbH MerseburgEberhard‐Leibnitz‐Stra?e 206217 Merseburg Germany;</p> <p>Polymer Service GmbH MerseburgEberhard‐Leibnitz‐Stra?e 206217 Merseburg Germany;</p> <p>Basell Polyolefine GmbH a lyondellbasell company PP compounds Europe PADIndustrial Area H?chst/Building C65765926 Frankfurt Germany;</p> <p>Polymer Service GmbH MerseburgEberhard‐Leibnitz‐Stra?e 206217 Merseburg Germany;</p> <p>Akademie Mitteldeutsche Kunststoffinnovation (AMK)Eberhard‐Leibnitz‐Stra?e 206217 Merseburg Germany;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1185.html" title="高分子化学（高聚物）">高分子化学（高聚物）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=creep&option=203" rel="nofollow">creep;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=depth‐sensing macro‐indentation&option=203" rel="nofollow">depth‐sensing macro‐indentation;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=poly(propylene) (PP)&option=203" rel="nofollow">poly(propylene) (PP);</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=retardation behaviour&option=203" rel="nofollow">retardation behaviour;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=time‐lapsing&option=203" rel="nofollow">time‐lapsing;</a> </p> <div class="translation"> 机译：蠕变;深度感测宏压缩进;聚（丙烯）（pp）;延迟行为;时间过去; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> 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sensory evaluation method</a> <b>[P]</b> . <span> 外国专利：  JP6859010B2 </span> <span> . 2021-04-14</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：延时感觉评估系统和延时感觉评估方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130458929623.html">METHOD FOR PRODUCING PURE POLYPROPYLENE IN BETA-CRYSTALL FORM USING ISOTACTIC POLYPROPYLENE HOMO OR COPOLYMERS OPTIONALLY CONTAINING UP TO 40 POLYETHYLENE</a> <b>[P]</b> . <span> 外国专利：  HU209132B </span> <span> . 1995-07-28</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用异丙基最多含40％聚乙烯的等位聚丙烯均聚物或共聚物生产呈β-结晶形式的纯聚丙烯的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130408520261.html">METHOD AND APPARATUS FOR IMPLEMENTATION OF ACCESS TO THE SYSTEM BASED ON WIRELESS LAN CLMSS EC ofCLMTXT 1. A method for performing medium access by stations (STA) in a wireless communication system, the method comprising the steps of: CLMTXT - taking a frame element comprising a set of parameters (RPS) for limited access window (RAW); CLMTXT - check field RAW-destination RPS-member; and CLMTXT - performing access based on the RAW initial time when the STA corresponds RAW-group associated with the field RAW-destination, CLMTXT - wherein the RAW start time is obtained based on starting time indicator subfield, CLMTXT - wherein the start time indicator subfield indicates whether or not included subfield RAW initial time indicating the start time RAW, RAW-in destination field. CLMTXT 2. A method according to Claim. 1, wherein, when the RAW-destination field is not a destination field in the first RAW RPS-member and subfield di</a> <b>[P]</b> . <span> 外国专利：  RU2015147909A </span> <span> . 2017-05-16</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：基于无线局域网<CLMTXT>的<CLMSS EC>实现对系统的访问的方法和装置1.一种用于在无线通信系统中由站（STA）执行媒体访问的方法，该方法包括以下步骤：<CLMTXT --取帧元素，包括用于受限访问窗口（RAW）的一组参数（RPS）; <CLMTXT>-检查字段RAW目标RPS成员;和<CLMTXT>-当STA对应于与字段RAW目的地相关联的RAW组时，基于RAW初始时间进行访问，<CLMTXT>-其中，基于开始时间指示符子字段<CLMTXT>获得RAW开始时间-其中，开始时间指示符子字段指示包括的子字段RAW初始时间是否指示开始时间RAW，RAW输入目的地字段。 <CLMTXT> 2.根据权利要求1的方法。参照图1，其中，当RAW目的地字段不是第一RAW RPS成员中的目的地字段和子字段di时 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div 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