Benzocyclobutene organosiloxane resins prepared by alcoholysis of BCB functionalized chlorosilane for highly crosslinked low-k thermosets

Yuanrong Cheng; Shichang Tian; Yunfei Shi; Wenhao Chen; Zhuo Li; Tangwei Zhu; Ziyu Zhang

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Benzocyclobutene organosiloxane resins prepared by alcoholysis of BCB functionalized chlorosilane for highly crosslinked low-k thermosets

机译：通过BCB官能化氯硅烷的醇解制备的苯并环丁烯有机氧氧氧氧氧氧氧氧氧氧杂环氧烷用于高度交联的低k热固性件

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?Highly crosslinked BCB siloxane resins with three different linkage group prepared.

?Good thermostaiblity: Td5above 450°C.

?Low-k: low dielectric constant as 2.69 and low dissipation loss as 1.5?10?3.

?Relationship of chemical structure and properties of the cured resins discussed.

Abstract

In this paper, highly crosslinked benzocyclobutene (BCB) organosiloxane intrinsic low-k thermosets with high thermal stability were prepared by thermal-curing of BCB organosiloxane resins, which were synthesized by alcoholysis

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？高度交联的BCB硅氧烷树脂，制备三种不同的连杆组。

？良好的恒温力：T D5 上面450°C。

？低k：低介电常数为2.69，低耗散损耗为1.5？10 ？3 。 < / ce：list-item> ？化学结构的关系讨论的固化树脂的性质。

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在本文中，通过BCB的热固化制备高度交联的苯并环丁烯（BCB）有机硅氧烷具有高热稳定性的高k热固性有机硅氧烷树脂，由醇解合成

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来源
《European Polymer Journal》 |2017年第2017期|共8页
作者
Yuanrong Cheng; Shichang Tian; Yunfei Shi; Wenhao Chen; Zhuo Li; Tangwei Zhu; Ziyu Zhang;
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作者单位

Department of Materials Science Fudan University;

Department of Materials Science Fudan University;

Department of Materials Science Fudan University;

Department of Materials Science Fudan University;

Department of Materials Science Fudan University;

Department of Materials Science Fudan University;

Department of Materials Science Fudan University;

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原文格式 PDF
正文语种 eng
中图分类有机化学;
关键词
Benzocyclobutene; Organosiloxane; Alcoholysis; Thermal stability; Low-k;

机译：苯并丁烯;有机硅氧烷;醇解;热稳定性;低k;

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专利

1. Benzocyclobutene organosiloxane resins prepared by alcoholysis of BCB functionalized chlorosilane for highly crosslinked low-k thermosets [J] . Yuanrong Cheng, Shichang Tian, Yunfei Shi, European Polymer Journal . 2017,第期

机译：通过BCB官能化氯硅烷的醇解制备的苯并环丁烯有机氧氧氧氧氧氧氧氧氧氧杂环氧烷用于高度交联的低k热固性件
2. Multi-benzocyclobutene functionalized siloxane monomers prepared by Piers-Rubinsztajn reaction for low-k materials [J] . Li Junyi, Zhang Ziyu, Zhu Tangwei, European Polymer Journal . 2020,第1期

机译：多苯并丁烯官能化硅氧烷单体由Piers-RubinsZtajn反应用于低K材料制备
3. Highly cross-linked thermosetting resin of maleimidobenzoxazine functionalized with benzocyclobutene [J] . Cheng Y., Qi T., Jin Y., Polymer: The International Journal for the Science and Technology of Polymers . 2013,第1期

机译：苯并环丁烯官能化的马来酰亚胺苯并恶嗪的高度交联的热固性树脂
4. Study of benzocyclobutene-functionalized siloxane thermoset with a cyclic structure [C] . Yang Jun, Sun Mingfei, Cheng Yuanrong, 2011 12th International Conference on Electronic Packaging Technology High Density Packaging . 2011

机译：环状结构热固性苯并环丁烯官能化硅氧烷的研究
5. Highly Functionalized Thermosets from Renewables for Composites and Coatings Applications [D] . Yu, Arvin Zillion. 2017

机译：复合材料和涂料应用中可再生能源的高官能化热固性
6. Correction: Hydrolysis and condensation of a benzocyclobutene-functionalized precursor for the synthesis of high performance low-K polymers [O] . Yuanrong Cheng, Wenhao Chen, Zhuo Li, 2017

机译：校正：苯并环丁烯官能化前体的水解和缩合，用于合成高效低钾聚合物

Benzocyclobutene organosiloxane resins prepared by alcoholysis of BCB functionalized chlorosilane for highly crosslinked low-k thermosets

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