Cathodized Gold Nanoparticle‐Modified Graphite Pencil Electrode for Non‐Enzymatic Sensitive Voltammetric Detection of Glucose

Kawde Abdel‐Nasser; Aziz Md. Abdul; El‐Zohri Manal; Baig Nadeem; Odewunmi Nurudeen

摘要

Abstract > A highly sensitive enzymeless electrochemical glucose sensor has been developed based on the simply prepared cathodized gold nanoparticle‐modified graphite pencil electrode (AuNP‐GPE). Cyclic voltammetry (CV) experiments show that AuNP‐GPE is able to oxidize glucose partially at low potential (around ?0.27) whereas the bare GPE cannot oxidize glucose in the entire tested potential windows. Besides, fructose and sucrose cannot be oxidized at potential lower than +0.1?V at AuNP‐GPE. As a result, the glucose oxidation peak at around ?0.27?V is suitable enough for selective detection of glucose in the presence of fructose and sucrose. Cathodization of AuNP‐GPE under optimum condition (‐1.0?V for 30?s) in the same glucose solution before voltammetric measurement enhanced glucose oxidation peak current around ?0.27?V to achieve an efficient electrochemical sensor for glucose with a detection limit of 12 μM and dynamic range between 0.05 to 5.0?mM with a good linearity (R 2 = 0.999). Almost no interference effect was observed for sensing of glucose in the presence of ascorbic acid, alanine, phenylalanine, fructose, sucrose, and NaCl. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> > a高度已经基于简称制备的阴极金纳米颗粒改性石墨铅笔电极（AUNP-GPE）开发了敏感酶促电化学葡萄糖传感器。循环伏安法（CV）实验表明，AUNP-GPE能够在低电位（周围0.27）处部分地氧化葡萄糖（周围α07），而裸GPE不能在整个测试的潜在窗口中氧化葡萄糖。此外，在AUNP-GPE下，果糖和蔗糖不能在低于+0.1〜v的电位下氧化。结果，葡萄糖氧化峰在周围α0.27≤v是足以在果糖和蔗糖存在下选择性检测葡萄糖。在伏安测量的相同葡萄糖溶液中在相同的葡萄糖溶液中在相同的葡萄糖溶液中的最佳条件（-1.0〜v持续30μl）的阴极化增强了葡萄糖氧化峰值电流的葡萄糖氧化峰值电流，以实现具有12的有效电化学传感器的葡萄糖。 μm和动态范围在0.05至5.0Ωmm之间，线性良好（R 2 </ sup> = 0.999）。对于在抗坏血酸，丙氨酸，苯丙氨酸，果糖，蔗糖和NaCl存在下，观察到对葡萄糖感测的几乎没有干扰效果。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" > 著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis 》</a> <b style="margin: 0 2px;">|</b><span>2017年第5期</span><b style="margin: 0 2px;">|</b> <span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kawde Abdel‐Nasser&option=202" target="_blank" rel="nofollow">Kawde Abdel‐Nasser;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aziz Md. Abdul&option=202" target="_blank" rel="nofollow">Aziz Md. Abdul;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=El‐Zohri Manal&option=202" target="_blank" rel="nofollow">El‐Zohri Manal;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Baig Nadeem&option=202" target="_blank" rel="nofollow">Baig Nadeem;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Odewunmi Nurudeen&option=202" target="_blank" rel="nofollow">Odewunmi Nurudeen;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Chemistry DepartmentKing Fahd University of Petroleum and MineralsDhahran 31261 Kingdom of Saudi Arabia;</p> <p>Center of Excellence of NanotechnologyKing Fahd University of Petroleum and MineralsDhahran 31261 Kingdom of Saudi Arabia.;</p> <p>Botany &</p> <p>Microbiology DepartmentFaculty of Science Assiut UniversityAssiut 71516 Egypt.;</p> <p>Chemistry DepartmentKing Fahd University of Petroleum and MineralsDhahran 31261 Kingdom of Saudi Arabia;</p> <p>Chemistry DepartmentKing Fahd University of Petroleum and MineralsDhahran 31261 Kingdom of Saudi Arabia;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li> <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span> <a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学 ;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Graphite pencil electrode&option=203" rel="nofollow">Graphite pencil electrode;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gold nanoparticles&option=203" rel="nofollow">Gold nanoparticles;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cathodization&option=203" rel="nofollow">Cathodization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Glucose sensor&option=203" rel="nofollow">Glucose sensor;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Voltammetry&option=203" rel="nofollow">Voltammetry;</a> </p> <div class="translation"> 机译：石墨铅笔电极;金纳米颗粒;阴极化;葡萄糖传感器;伏安法; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704023174597.html">Cathodized Gold Nanoparticle‐Modified Graphite Pencil Electrode for Non‐Enzymatic Sensitive Voltammetric Detection of Glucose</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kawde Abdel‐Nasser&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Kawde Abdel‐Nasser,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aziz Md. 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