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Voltammetric Detection of Catecholamine Metabolites Using Tr?ger's Base Modified Electrode

机译：使用TRαGER的基础改性电极伏安检测儿茶酚胺代谢物

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Abstract > The advantage of surface modification of voltammetric sensor for determination of catecholamine metabolites such as vanillyl mandelic acid (VMA) and homovanillic acid (HVA) is discussed. The amino‐substituted coumarin derivative of Tr?ger's base was deposi‐ted on a graphite screen‐printed electrode (poly(CTB)/G/SPE) cycling the electrode potential between 0 and 1.2?V in 5 mL CH <sub>2</sub> Cl <sub>2</sub> containing 1×10 ?3 ?mol?L ?1 tetrabutylammonium tetrafluoroborate and 20?μL 0.1?mol?L ?1 HCl. The poly(CTB) functions as both a selective recognition and pre‐concentrator agent for catecholamine metabolites. The high sensitivity of the voltammetric sensor coated by a poly(CTB) film toward VMA was achieved despite the high structural similarity between the two tested metabolites. We presume the voltammetric detection of these species is based on selective binding by a poly(CTB) film supported by its good adherence to the electrode substrate. The voltammetric signals of VMA were observable in the concentration range 10–100?μmol?L ?1 (LOD=0.2?μmol?L ?1 ) and 20–60?μmol?L ?1 (LOD=10?μmol?L ?1 ) in the model and synthethic urine samples, respectively. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</标题> >伏安传感器的表面改性的优势，用于测定vanillyl mendelic acid等儿茶酚胺代谢物（讨论了VMA）和同种烷酸（HVA）。 TrαGER碱的氨基取代的香豆素衍生物在石墨丝网印刷电极（聚（CTB）/ G / SPE）上循环循环在5mL CH <sub> 2中的电极电位之间的电极电位。含有1×10 α3</ sup>αmolα1α1α1α1α1/ sup>四氟铵四氟硼酸铵和20≤μl0.1Ω·摩尔？？1 </ sup> hcl。聚（CTB）用作儿茶酚胺代谢物的选择性识别和预浓缩剂代理。尽管两种测试的代谢物之间的结构相似性高，但是通过聚（CTB）膜涂覆的伏安传感器对VMA的高灵敏度。我们假设这些物种的伏安检测基于由其良好粘附到电极基板的聚（CTB）膜的选择性结合。 VMA的伏安信号在浓度范围内可观察到10-100Ωμmolα1 1（LOD =0.2≤μmol≤1）和20-60？ μmolα1α1/ sup>（LOD = 10？μmol？l β1</ sup>）分别在模型和合成尿液样本中。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2018年第4期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shishkanova Tatiana V.&option=202" target="_blank" rel="nofollow">Shishkanova Tatiana V.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Broncová Gabriela&option=202" target="_blank" rel="nofollow">Broncová Gabriela;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fitl P?emysl&option=202" target="_blank" rel="nofollow">Fitl P?emysl;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Král Vladimír&option=202" target="_blank" rel="nofollow">Král Vladimír;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Barek Ji?í&option=202" target="_blank" rel="nofollow">Barek Ji?í;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Analytical ChemistryUniversity of Chemistry and Technology Prague166 28 Prague 6 Technická 5 Czech Republic;</p> <p>Department of Analytical ChemistryUniversity of Chemistry and Technology Prague166 28 Prague 6 Technická 5 Czech Republic;</p> <p>Department of Physics and MeasurementsUniversity of Chemistry and Technology Prague166 28 Prague 6 Technická 5 Czech Republic;</p> <p>Department of Analytical ChemistryUniversity of Chemistry and Technology Prague166 28 Prague 6 Technická 5 Czech Republic;</p> <p>Charles University Faculty of Science Department of Analytical Chemistry UNESCO Laboratory of environmental electrochemistry128 43 Prague 2 Hlavova 2030 Czech Republic;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polymeric Tr?ger's base&option=203" rel="nofollow">polymeric Tr?ger's base;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=voltammetric sensor&option=203" rel="nofollow">voltammetric sensor;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=vanillyl mandelic acid&option=203" rel="nofollow">vanillyl mandelic acid;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=homovanillic acid&option=203" rel="nofollow">homovanillic acid;</a> </p> <div class="translation"> 机译：聚合物TR？GER的基础;伏安传感器;vanillyl弱甲酸;己酰胺酸; 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