Evaluation of the catocene/graphene oxide nanocomposite catalytic activity on ammonium perchlorate thermal decomposition

Saat Maryam; Yarmohammadi Masoud; Zamani Pedram Mona; Shahidzadeh Mansour; Amini‐Fazl Mohammad Sadegh

摘要

Abstract > A novel nanocomposite catalyst for thermal degradation of the ammonium perchlorate (AP) has been synthesized, and its effect on the thermal behavior of AP has been investigated. Preparation of the catalyst was carried out via functionalization of the graphene oxide with phenyl isocyanate and its noncovalent bonding to catocene. The catalytic activity of the catalyst was studied by thermal gravimetric analysis/differential scanning calorimetry at various heating rates. In addition, the effect of the catalyst on the AP thermal decomposition has been investigated by Kissinger and Friedman methods as two model‐free methods for calculation of the activation energy parameter. According to the Kissinger method calculations, the E <sub>a</sub> of AP decomposition reduced about 151?kJ?mol ?1 lower than the reported value for pure AP in the presence of the catalyst. Calculation of the E <sub>a</sub> value for various reaction conversion rates by the Friedman method also confirmed the Kissinger method results. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 已经合成了用于热氯酸铵（AP）的热劣化的新型纳米复合催化剂，研究了对AP的热行为的影响。通过用苯基异氰酸酯的石墨烯氧化物的官能化和其非共价键与甲胶烯来进行催化剂的制备。通过以各种加热速率进行热重分析/差示扫描量热法研究催化剂的催化活性。此外，通过基辛格和弗里德曼方法研究了催化剂对AP热分解的影响，作为用于计算激活能量参数的两个模型方法。根据基辛格方法计算， E. <sub> a </ sub> </ i> AP分解减少约151？KJ？摩尔？1 </ sup> 在催化剂存在下低于纯AP的报道值。计算的计算 E. <sub> a </ sub> </ i> 弗里德曼方法的各种反应转化率的价值也证实了基辛格方法结果。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-20953/'>《International Journal of Chemical Kinetics》</a> <b style="margin: 0 2px;">|</b><span>2019年第5期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Saat Maryam&option=202" target="_blank" rel="nofollow">Saat Maryam;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yarmohammadi Masoud&option=202" target="_blank" rel="nofollow">Yarmohammadi Masoud;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zamani Pedram Mona&option=202" target="_blank" rel="nofollow">Zamani Pedram Mona;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shahidzadeh Mansour&option=202" target="_blank" rel="nofollow">Shahidzadeh Mansour;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Amini‐Fazl Mohammad Sadegh&option=202" target="_blank" rel="nofollow">Amini‐Fazl Mohammad Sadegh;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Chemical EngineeringIslamic Azad UniversityTehran Iran;</p> <p>Young Researchers and Elite ClubIslamic Azad UniversityTehran Iran;</p> <p>Faculty of Mechanical Engineering‐Energy DivisionK. N. Toosi University of TechnologyTehran Iran;</p> <p>Department of Chemical EngineeringIslamic Azad UniversityTehran Iran;</p> <p>Research Laboratory of Advanced Polymer MaterialUniversity of TabrizTabriz Iran;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ammonium perchlorate&option=203" rel="nofollow">ammonium perchlorate;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=catocene&option=203" rel="nofollow">catocene;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=graphene oxide&option=203" rel="nofollow">graphene oxide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanocomposite catalyst&option=203" rel="nofollow">nanocomposite catalyst;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thermal decomposition&option=203" rel="nofollow">thermal decomposition;</a> </p> <div class="translation"> 机译：高氯酸铵;树胶;石墨烯;纳米复合催化剂;热分解; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022991927.html">Evaluation of the catocene/graphene oxide nanocomposite catalytic activity on ammonium perchlorate thermal decomposition</a> <b>[J]</b> . <span> <a 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<b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_detail_thesis/0201295578693.html">Ag修饰N-石墨烯/TiO_2纳米复合材料的光催化活性</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=周民杰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 周民杰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=付碧松&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,付碧松</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张娜&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,张娜</a> <span> <a href="/journal-cn-56955/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 人工晶体学报 </a> </span> <span> . 2015</span><span>,第6期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-8330_thesis/020222119166.html">通过减少石墨烯的缺陷和增加界面接触提高石墨烯-TiO2复合材料的光催化活性</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张燕辉&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 张燕辉</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=徐艺军&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,徐艺军</a> <span> <a href="/conference-cn-8330/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十三届全国太阳能光化学与光催化学术会议 </a> <span> <span> . 2012</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314609959.html">石墨相氮化碳及其纳米复合材料的制备与其在催化高氯酸铵热分解中的应用研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李奇&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 李奇</a> <span> . 2016</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120113040690.html">一种催化高氯酸铵热分解的ZnO/石墨烯催化剂的制备方法</a> <b>[P]</b> . <span> 中国专利： CN113070055A </span> <span> . 2021-07-06</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/061204400388.html">电催化活性纳米复合材料及其生产方法</a> <b>[P]</b> . <span> 中国专利： CN107851803B </span> <span> . 2021.05.11</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130500004702.html">REDUCED GRAPHENE OXIDE/MANGANESE(IV) OXIDE NANOCOMPOSITE AND ELECTRODE COMPRISING SAME, METHOD OF MANUFACTURE OF VARIOUS GRAPHENE MATERIAL/METAL OXIDE NANOCOMPOSITES</a> <b>[P]</b> . <span> 外国专利：  US2021159490A1 </span> <span> . 2021-05-27</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：还原氧化物/锰（IV）氧化物纳米复合材料和电极，其包括该氧化物纳米复合材料，制造各种石墨烯材料/金属氧化物纳米复合材料的方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130421733950.html">Apparatus useful for decomposing nitrous oxide, comprises at least a reactor that includes a catalyst for catalytically decomposing nitrous oxide, where the reactor is surrounded at least partially by thermally insulating expanded glass</a> <b>[P]</b> . <span> 外国专利：  DE102011118789A1 </span> <span> . 2012-06-21</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于分解一氧化二氮的设备至少包括反应器，该反应器包括用于催化分解一氧化二氮的催化剂，其中该反应器至少部分地被热绝缘的膨胀玻璃包围。 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130500811755.html">- - MEHTOD FOR MANUFACTURING GRAPHENE-TIN OXIDE NANOCOMPOSITES AND GRAPHENE-TIN OXIDE NANOCOMPOSITES</a> <b>[P]</b> . <span> 外国专利：  KR102311971B1 </span> <span> . 2021-10-12</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：- - 制造石墨烯 - 氧化锡纳米复合材料和石墨烯氧化锡纳米复合材料的方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704022991927','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="关闭" onclick="$('.journalsub-pop-up').hide()"> <p class="pardon">抱歉，该期刊暂不可订阅，敬请期待！</p> <p class="current">目前支持订阅全部北京大学中文核心（2020）期刊目录。</p> <div style="display: 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