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Formation of a Uniform Distribution of TiO_2 Nanotubes Array on Complex Geometry Samples

机译:复杂几何形状样品上TiO_2纳米管阵列均匀分布的形成

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We demonstrate that is possible to create a uniform distribution of TiO_2 nanotubes array on complex geometry samples, like a titanium screw commonly used as a dental implant, using a very simple experimental set-up. TiO_2 nanotubes array were synthesized by a potentiostatic anodization process, in H_3PO_4 and HF aqueous solution. During the anodization, the titanium implants were used as working electrode and platinum sheet as a counter electrode, in order to anodize the whole screw, a rotating device was used. The morphology of the porous layers is controlled by anodization potential, electrolyte composition, anodization duration and cell temperature as well as by the geometry of the samples. This finding opens new perspectives in testing medical devices to all researchers. Scientists will may able to use the “real” prosthesis, exactly the same that are used in clinical practice, coating them with nanotubes. It will be easier to analyse the devices response using samples formed by “real” prosthesis, which could be tested in living bodies.
机译:我们证明,使用非常简单的实验装置,就可以在复杂几何形状的样品(例如通常用作牙科植入物的钛螺钉)上创建TiO_2纳米管阵列的均匀分布。通过恒电位阳极氧化工艺在H_3PO_4和HF水溶液中合成了TiO_2纳米管阵列。在阳极氧化过程中,将钛植入物用作工作电极,将铂片用作对电极,为了对整个螺钉进行阳极氧化,使用了旋转装置。多孔层的形态由阳极氧化电势,电解质组成,阳极氧化持续时间和电池温度以及样品的几何形状控制。这一发现为所有研究人员打开了测试医疗设备的新视野。科学家将能够使用与临床实践完全相同的“真实”假体,并在其上涂上纳米管。使用由“假体”假体形成的样本来分析设备的响应将更加容易,这些样本可以在活体内进行测试。

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