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Thermal and microwave dielectric properties of Cu/polyethylene oxide composite powder prepared by mechanical blending method

机译:机械混合法制备的Cu /聚环氧乙烷复合粉体的热和微波介电性能

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The copper/polyethylene oxide (Cu/PEO) powder composites are synthesized by varying the Cu concentration (by wt%) using mechanical blending method. The synthesized samples are characterized using various sophisticated tools viz. the X-ray diffraction (XRD), the Scanning Electron Microscopy (SEM), the Thermo Gravimetric Analysis (TGA) and the vector network analyzer (VNA) for the analysis of crystallinity, morphology, thermal stability and the microwave dielectric properties, respectively. The thermo gravimetric analysis result shows that the thermal stability of PEO matrix composite with Cu filler increases on increasing of the copper content. The effective dielectric properties of the resultant composites are measured in the X-band of microwave frequency using cavity perturbation technique. Two different rectangular cavities with a special arrangement of the sample holder are fabricated for testing of the dielectric properties of powdered composites. The variation in Cu-contenth as brought the significant change in the microwave dielectric properties of Cu/PEO composite e.g. the real and the imaginary parts of complex permittivity are found to be increasing from 2.1 to 6.1, and from 0.07 to 0.15, respectively with increasing the Cu content from 0 to 30 wt%. (C) 2015 The Society of Powder Technology Japan. Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights reserved.
机译:铜/聚环氧乙烷(Cu / PEO)粉末复合材料是通过使用机械混合方法改变铜浓度(按重量%)合成的。使用各种复杂的工具对合成的样品进行表征。 X射线衍射(XRD),扫描电子显微镜(SEM),热重分析(TGA)和矢量网络分析仪(VNA)分别用于分析结晶度,形态,热稳定性和微波介电性能。热重分析结果表明,含铜填料的PEO基复合材料的热稳定性随铜含量的增加而增加。使用腔室扰动技术在微波频率的X波段测量所得复合材料的有效介电性能。制作了两个不同的矩形腔,它们带有特殊布置的样品架,用于测试粉末状复合材料的介电性能。 Cu含量的变化带来了Cu / PEO复合材料例如Cu / PEO复合材料的微波介电性能的显着变化。发现随着Cu含量从0wt%增加到30wt%,复介电常数的实部和虚部分别从2.1增加到6.1,并且从0.07增加到0.15。 (C)2015年日本粉末技术学会。由Elsevier B.V.和日本粉末技术学会出版。版权所有。

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