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Synthesis and characterization of mesoporous composite silica monolith

机译:介孔复合二氧化硅整体料的合成与表征

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Coumarin4 (Cou4) was loaded into mesoporous silicon SBA-15 monolith channels by a simple postgraft-ing method at room temperature. The obtained Cou4/SBA-15 composite monolith was compared with the blank SBA-15 monolith. The investigation of X-ray diffraction, transmission electron microscopy (TEM), UV-vis and photoluminescence (PL) reveals the existence of cou4 in the channels of SBA-15 monolith. In addition, a red-shift and strong fluorescence in PL spectrum was observed from the composite monolith compared with that of Cou4 in C2H5OH solution. This is good for the new application of optical materials.
机译:通过简单的后接枝方法在室温下将香豆素4(Cou4)装入中孔硅SBA-15整体通道中。将获得的Cou4 / SBA-15复合整料与空白SBA-15整料进行比较。 X射线衍射,透射电子显微镜(TEM),紫外可见光和光致发光(PL)的研究揭示了cou4在SBA-15整体通道中的存在。此外,与C4H5OH溶液中的Cou4相比,复合整料在PL光谱中观察到红移和强荧光。这对于光学材料的新应用是有好处的。

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