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Investigation of mesoporous carbon materials by magnetic solid phase extraction of selected phthalates from water samples

机译:磁性固相萃取水样中邻苯二甲酸酯对中孔碳材料的研究

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摘要

In the present work ordered mesoporous carbon materials soft templating-acidic (STA) were applied as adsorbents in magnetic solid phase extraction technique for isolation of selected phthalates from water samples. STA materials were obtained by soft-templating method in acidic environment. Nickel nanoparticles were added on the STA synthesis stage, thus the obtained material acquired magnetic properties. The analysis of phthalates after the extraction was carried out by gas chromatography-mass spectrometry method. Fast and easy procedure was elaborated, obtaining recoveries close to 90% for some phthalates.
机译:在目前的工作中,有序介孔碳材料软模板酸性(STA)被用作磁性固相萃取技术中的吸附剂,以从水样中分离出所选择的邻苯二甲酸盐。 STA材料是在酸性环境中通过软模板法获得的。在STA合成阶段添加镍纳米粒子,从而获得的材料获得了磁性。萃取后的邻苯二甲酸酯的分析通过气相色谱-质谱法进行。精心设计的快速简便的方法,使某些邻苯二甲酸酯的回收率接近90%。

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