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Microwave-assisted shape-controlled bulk synthesis of Ag and Fe nanorods in poly(ethylene glycol) solutions

机译:聚乙二醇溶液中微波辅助形状控制的Ag和Fe纳米棒的本体合成

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摘要

Bulk syntheses of silver (Ag) and iron (Fe) nanorods using poly(ethylene glycol) (PEG) under microwave irradiation conditions are reported. Favorable conditions to make Ag nanorods were established and can be extended to make. Fe nanorods with uniform size and shape. The nanorods formation depended upon the concentration of PEG used in the reaction with Ag salt. The obtained Ag and Fe nanorods were characterized using scanning electron microscopy, transmission electron microscopy, and UV-visible spectroscopy. Ag and Fe nanorods crystallized in face centered cubic symmetry. The method uses no surfactant or reducing agent and is greener in nature which could open a myriad of applications.
机译:报道了在微波辐射条件下使用聚乙二醇(PEG)大量合成银(Ag)和铁(Fe)纳米棒。建立了制备Ag纳米棒的有利条件,并且可以扩展制造条件。铁纳米棒具有均匀的尺寸和形状。纳米棒的形成取决于与银盐反应中使用的PEG的浓度。使用扫描电子显微镜,透射电子显微镜和UV-可见光谱对获得的Ag和Fe纳米棒进行表征。 Ag和Fe纳米棒以面心立方对称性结晶。该方法不使用表面活性剂或还原剂,并且本质上是绿色的,可以打开无数的应用领域。

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