Novel and Facile Route for the Synthesis of Tunable Boron Nitride Nanotubes Combining Atomic Layer Deposition and Annealing Processes for Water Purification

Weber Matthieu; Iatsunskyi Igor; Coy Emerson; Miele Philippe; Cornu David; Bechelany Mikhael

摘要

Abstract >The synthesis of tunable boron nitride (BN) nanotubes is the subject of intense research because of their potential applications in various fields, from smart textile materials to emerging environmental technologies. However, the preparation of these nanomaterials remains extremely challenging. Herein, proof‐of‐concept results on the scalable synthesis of boron nitride nanotubes with tunable dimensions are reported. Combining atomic layer deposition (ALD) of boron nitride on carbon nanofibers template supports and successive annealing steps at high temperature, BN nanotubes with controllable properties are prepared. The successive annealing steps enable the crystallization of BN and the combustion of the initial carbon supports. The self‐limiting nature of the ALD process allows for the scalable coating of large scale carbon fibers matrix. High‐resolution transmission electron microscopy measurements demonstrate the exquisite dimensions control at the nanoscale and the presence of crystalline BN. The proof‐of‐concept results presented allow for independent control of the inner and external diameter dimensions, opening up unique possibilities for the precise engineering of BN nanotubes properties. The nanotubes present good mechanical properties, are easy to handle, and the assessment of their sorption properties shows that they absorb up to 110 times their own weight in oils while repelling water, which opens prospects for water purification. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >可调谐氮化硼（BN）纳米管的合成是激烈研究的主题，因为它们在各种领域的潜在应用，从智能纺织材料到新兴的环境技术。然而，这些纳米材料的制备仍然非常具有挑战性。在此，概念证明结果对具有可调谐尺寸的氮化硼纳米管的可扩展合成的概念结果。将氮化硼的原子层沉积（ALD）与高温下的碳纳米纤维模板载体和连续退火步骤相结合，制备具有可控性质的BN纳米管。连续的退火步骤使得Bn的结晶和初始碳支撑件的燃烧能够结晶和燃烧。 ALD工艺的自限性质允许大规模碳纤维基质的可伸缩涂层。高分辨率透射电子显微镜测量显示在纳米级和结晶BN的存在下的精致尺寸控制。概念验证结果允许对内部和外径的独立控制，开辟了BN纳米管属性精确工程的独特可能性。纳米管呈现出良好的机械性能，易于处理，并对其吸附特性的评估表明，它们在排斥水的同时吸收高达110次的油脂，这使水净化前景。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2018年第16期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Weber Matthieu&option=202" target="_blank" rel="nofollow">Weber Matthieu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Iatsunskyi Igor&option=202" target="_blank" rel="nofollow">Iatsunskyi Igor;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Coy Emerson&option=202" target="_blank" rel="nofollow">Coy Emerson;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Miele Philippe&option=202" target="_blank" rel="nofollow">Miele Philippe;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cornu David&option=202" target="_blank" rel="nofollow">Cornu David;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bechelany Mikhael&option=202" target="_blank" rel="nofollow">Bechelany Mikhael;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Institut Européen des membranesENSCMMontpellier 34095 France;</p> <p>NanoBioMedical CentreAdam Mickiewicz University in PoznanUmultowska str. 85 61‐614 Poznan Poland;</p> <p>NanoBioMedical CentreAdam Mickiewicz University in PoznanUmultowska str. 85 61‐614 Poznan Poland;</p> <p>Institut Européen des membranesENSCMMontpellier 34095 France;</p> <p>Institut Européen des membranesENSCMMontpellier 34095 France;</p> <p>Institut Européen des membranesENSCMMontpellier 34095 France;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=atomic layer deposition&option=203" rel="nofollow">atomic layer deposition;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=boron nitride&option=203" rel="nofollow">boron nitride;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrospinning&option=203" rel="nofollow">electrospinning;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanotubes&option=203" rel="nofollow">nanotubes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=water purification&option=203" rel="nofollow">water purification;</a> </p> <div class="translation"> 机译：原子层沉积;氮化硼;静电纺丝;纳米管;水净化; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" 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Govindan Kutty,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zheng Liu&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zheng Liu </a> <span>2016</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过化学气相沉积可控合成原子层状六方氮化硼</span> </p> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/open-access_resources_thesis/01000130881466.html">Novel and Facile Route for the Synthesis of Tunable Boron Nitride Nanotubes Combining Atomic Layer Deposition and Annealing Processes for Water Purification</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Matthieu Weber&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Matthieu Weber,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Igor Iatsunskyi&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Igor Iatsunskyi,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Emerson Coy&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Emerson Coy,</a> <span>2018</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于合成可调谐氮化硼纳米管的新颖和容易途径，组合原子层沉积和退火工艺进行水净化</span> </p> </li> <li> <div> <b>8. </b><a class="enjiyixqcontent" href="/ntis-science-report_ad_thesis/02071204877.html">Longitudinal Splitting of Boron Nitride Nanotubes for the Facile Synthesis of High Quality Boron Nitride Nanoribbons.</a> <b>[R] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Erickson, K. J.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Erickson, K. J.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext= Gibb, A. L.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> Gibb, A. L.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext= Sinitskii, A.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> Sinitskii, A.,</a> <span>2011</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：氮化硼纳米管纵向裂解合成高质量氮化硼纳米带。</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-catalysis_thesis/0201280713726.html">新颖TiN/C3N4/CdS纳米管核/壳阵列的合成及其光电化学性能</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=艾长智&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 艾长智</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=童丽&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,童丽</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王志鹏&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王志鹏</a> <span> <a href="/journal-cn-28399/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 催化学报 </a> </span> <span> . 2020</span><span>,第010期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_advanced-technology-electrical-engineering-energy_thesis/0201230089342.html">用于六硼化镧阴极的可调节恒流源</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨中山&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 杨中山</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈坤仪&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陈坤仪</a> <span> <a href="/journal-cn-8474/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 电工电能新技术 </a> </span> <span> . 1991</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_china-powder-industry_thesis/0201214307468.html">球磨-退火法合成氮化硼纳米管及其表征</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=朱雁风&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 朱雁风</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=汪宙&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,汪宙</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘海洋&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘海洋</a> <span> <a href="/journal-cn-7732/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国粉体工业 </a> </span> <span> . 2017</span><span>,第006期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_journal-chemical-physics_thesis/0201296203523.html">毛刺状竹节结构氮化硼纳米管的合成与生长机理</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张弜&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 张弜</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈熹&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陈熹</a> <span> <a href="/journal-cn-12046/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 化学物理学报 </a> </span> <span> . 2014</span><span>,第5期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_guangzhou-chemical-industry_thesis/0201246565259.html">氮化硼纳米管的合成与表征</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘西文&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 刘西文</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=侯绍宇&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,侯绍宇</a> <span> <a href="/journal-cn-9125/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 广州化工 </a> </span> <span> . 2011</span><span>,第012期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-59982_thesis/020222846075.html">硼掺杂金刚石电极制备及用于航天器冷凝水净化处理</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Hao&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . Li Hao</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李浩&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李浩</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Zhongjian&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Li Zhongjian</a> <span> <a href="/conference-cn-59982/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第一届全国载人航天环境控制与生命保障技术研讨会 </a> <span> <span> . 2012</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314961608.html">两类新颖结构有机二氟化硼配合物的合成与其性能研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨曦&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 杨曦</a> <span> . 2010</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/061203301746.html">一种用于氢气存储的氮化硼纳米管及合成方法</a> <b>[P]</b> . <span> 中国专利： CN106517112B </span> <span> . 2019.05.07</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120108999396.html">一种用于氢气存储的氮化硼纳米管及合成方法</a> <b>[P]</b> . <span> 中国专利： CN106517112A </span> <span> . 2017-03-22</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130421781252.html">X-ray tube for medical diagnostic procedures, has shield formed in form of layer on surface arranged inside vacuum casing, where shield comprises carbon nanotubes and/or boron nitride nanotubes and/or carbon boron nitride nanotubes</a> <b>[P]</b> . <span> 外国专利：  DE102010022595A1 </span> <span> . 2011-12-01</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于医学诊断程序的X射线管具有布置在真空壳体内部的表面上的层状形式的屏蔽，其中屏蔽包括碳纳米管和/或氮化硼纳米管和/或碳氮化硼纳米管。 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130443206202.html">PROCESSES FOR FORMING BORON NITRIDE PRECURSOR AND FOR MANUFACTURING BORON NITRIDE NANOTUBE USING BORON NITRIDE PRECURSOR</a> <b>[P]</b> . <span> 外国专利：  JP2004161546A </span> <span> . 2004-06-10</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：氮化硼前驱物的形成工艺和利用氮化硼前驱物制造氮化硼纳米管的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130401299548.html">2. Al2O3 / Ni / Al2O3 nanotubes with high appearance rate and low polymerization probability, magnetic type and "core shell" type nanotubes, as well as collection methods including electric yarn, atomic layer deposition and subsequent pyrolysis process, can shorten the synthesis time and increase the yield.</a> <b>[P]</b> . <span> 外国专利：  CL2019003267A1 </span> <span> . 2020-06-05</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：2.具有高出现率和低聚合概率的Al2O3 / Ni / Al2O3纳米管，磁性型和“核壳”型纳米管以及包括电纱，原子层沉积和随后的热解过程在内的收集方法，可以缩短合成时间，并且提高产量。 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> 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