Monodispersed, Highly Interactive Facet (111)‐Oriented Pd Nanograins by ALD onto Free‐Standing and Flexible Electrospun Polymeric Nanofibrous Webs for Catalytic Application

Ranjith Kugalur Shanmugam; Celebioglu Asli; Eren Hamit; Biyikli Necmi; Uyar Tamer

摘要

Abstract > An atomic layer deposition (ALD) of monodispersed palladium (Pd) nanograins (≈2 nm) onto electrospun polymeric nanofibers (NF) is presented. By ALD, monodispersed Pd nanograins with (111) exposed facets are decorated on the surface of the free‐standing flexible nanofibrous webs (NW). The Pd nanograin‐decorated free‐standing NW exhibit catalytic reduction of 4‐nitrophenol to 4‐aminophenol. Even under low loading capacity (≈20 μg mg ?1 ), Pd nanograins manifest effective catalytic performance which can be referred to direct exposure of Pd single crystalline highly interactive (111) plains with high surface area on the NW. The Pd nanograins and the interactive sites along with the high surface area NW yield effective catalytic reduction of 4‐nitrophenol to 4‐aminophenol with the catalytic reduction rate of 0.0531 min ?1 . Pd nanograins display thermally tunable effective catalytic reduction properties with activation energy ( E <sub>a</sub> ) of 1.705 J mol ?1 on varying the reaction temperature from 12 to 42 °C. Moreover, Pd nanograin‐decorated NW are exhibited the effective reusable behavior with stable structural integrity even after repeated catalytic reactions. The approach of this study opens up synthesis and surface decoration of metal nanostructures onto NF through ALD with controlled size and facet orientation for designing reusable and free‐standing flexible catalytic nanofibrous materials. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 呈现了将单分散钯（Pd）纳米（≈2nm）的原子层沉积（Ald）呈现在电纺成聚合物纳米纤维（NF）上。通过ALD，具有（111）曝光刻面的单分散的PD纳米簇装饰在独立式柔性纳米纤维网（NW）的表面上装饰。 PD纳米格勒装饰的独立式NW表现出4-硝基苯酚至4-氨基酚的催化还原。即使在低负载能力下（≈0μgmg ？1 </ sup> ），PD纳米甲型表现出有效的催化性能，其可以被称为直接暴露于NW上具有高表面积的Pd单晶高度相互作用（111）平原。 Pd纳米甲酸和互动位点以及高表面积NW产生4-硝基苯酚对4-氨基苯酚的有效催化还原率为0.0531分钟？1 </ sup> 。 PD纳米纳米用活化能量显示热可调的有效催化还原性能（ e </ i> <sub> a </ sub> ）1.705 J Mol ？1 </ sup> 改变12至42℃的反应温度。此外，甚至在重复催化反应后，Pd Nanograin装饰的NW也具有稳定的结构完整性的有效可重复使用的行为。该研究的方法使金属纳米结构的合成和表面装饰在NF通过ALD上，具有控制尺寸和面向方向，用于设计可重复使用和独立的柔性催化纳米纤维材料。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2017年第24期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ranjith Kugalur Shanmugam&option=202" target="_blank" rel="nofollow">Ranjith Kugalur Shanmugam;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Celebioglu Asli&option=202" target="_blank" rel="nofollow">Celebioglu Asli;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Eren Hamit&option=202" target="_blank" rel="nofollow">Eren Hamit;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Biyikli Necmi&option=202" target="_blank" rel="nofollow">Biyikli Necmi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Uyar Tamer&option=202" target="_blank" rel="nofollow">Uyar Tamer;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Institute of Materials Science and Nanotechnology and UNAM–National Nanotechnology Research CenterBilkent UniversityAnkara 06800 Turkey;</p> <p>Institute of Materials Science and Nanotechnology and UNAM–National Nanotechnology Research CenterBilkent UniversityAnkara 06800 Turkey;</p> <p>Institute of Materials Science and Nanotechnology and UNAM–National Nanotechnology Research CenterBilkent UniversityAnkara 06800 Turkey;</p> <p>Electrical and Computer EngineeringUniversity of ConnecticutStorrs CT 06269‐4157 USA;</p> <p>Institute of Materials Science and Nanotechnology and UNAM–National Nanotechnology Research CenterBilkent UniversityAnkara 06800 Turkey;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=atomic layer deposition&option=203" rel="nofollow">atomic layer deposition;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrospinning&option=203" rel="nofollow">electrospinning;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=metal catalyst&option=203" rel="nofollow">metal catalyst;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pd nanograins&option=203" rel="nofollow">Pd nanograins;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polymeric nanofibers&option=203" rel="nofollow">polymeric nanofibers;</a> </p> <div class="translation"> 机译：原子层沉积;静电纺丝;金属催化剂;Pd纳米注塑;聚合物纳米纤维; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022434640.html">Nanofibrous Catalysts: Monodispersed, Highly Interactive Facet (111)‐Oriented Pd Nanograins by ALD onto Free‐Standing and Flexible Electrospun Polymeric Nanofibrous Webs for Catalytic Application (Adv. 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