Effect of Air‐Aging on the Electrochemical Characteristics of TiO        <sub xmlns='http://www.wiley.com/namespaces/wiley'>          x        </sub>          <i xmlns='http://www.wiley.com/namespaces/wiley'>xx                C        <sub xmlns='http://www.wiley.com/namespaces/wiley'>          y        </sub>          <i xmlns='http://www.wiley.com/namespaces/wiley'>yy                Films for Electrocatalysis Applications

Rüdiger Celine; Valero‐Vidal Carlos; Favaro Marco; Agnoli Stefano; Granozzi Gaetano; Kunze‐Liebh?user Julia

摘要

Abstract > We report on the electrochemical characteristics of pristine and air‐aged carbon‐modified titania electrodes in acidic electrolyte, which find applications as catalyst supports in electrocatalysis. Films with different chemical compositions (including TiO <sub>2</sub> , TiO <sub> x </sub> , TiO, TiC, C) are synthesized through a carbothermal treatment of compact anodic TiO <sub>2</sub> on Ti substrates at different temperatures, and are analyzed with X‐ray photoelectron spectroscopy. Their activity towards heterogeneous outer‐sphere electron transfer and their stability against passivation and corrosion under anodic polarization are investigated by means of electrochemical impedance spectroscopy. It is found that a high fraction of TiC in the pristine carburized films in combination with a thin TiO <sub>2</sub> surface layer yields high electron‐transfer kinetics even after aging for 9?months, and a high corrosion and passivation resistance until approximately 0.74V <sub>SHE</sub> . This finding is essential to the material‘s application as a catalyst support in general. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <标题类型=“main”>抽象</ title> > 我们报告了酸性电解质中原始和空气老化碳改性二氧化钛电极的电化学特性，其在电常放分析中发现应用作为催化剂载体。具有不同化学成分的薄膜（包括TiO <sub> 2 </ sub> ，TIO. <sub> x </ i> </ sub> ，TiO，Tic，C）通过紧凑型阳极TiO的碳水处理合成 <sub> 2 </ sub> 在不同温度下的Ti基材上，并用X射线光电子能谱分析。通过电化学阻抗光谱研究了它们对异质外球电子传递及其抗钝化和腐蚀的稳定性和腐蚀的稳定性。结果发现，原始渗碳膜中的高分化与薄TiO组合 <sub> 2 </ sub> 即使在老化9？个月后，表面层也会产生高电子转移动力学，以及高腐蚀和钝化阻力直至大约0.74V <sub>她</ sub> 。这一发现对于将材料的应用作为催化剂支持至关重要。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2017年第12期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rüdiger Celine&option=202" target="_blank" rel="nofollow">Rüdiger Celine;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Valero‐Vidal Carlos&option=202" target="_blank" rel="nofollow">Valero‐Vidal Carlos;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Favaro Marco&option=202" target="_blank" rel="nofollow">Favaro Marco;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Agnoli Stefano&option=202" target="_blank" rel="nofollow">Agnoli Stefano;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Granozzi Gaetano&option=202" target="_blank" rel="nofollow">Granozzi Gaetano;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kunze‐Liebh?user Julia&option=202" target="_blank" rel="nofollow">Kunze‐Liebh?user Julia;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Physik-DepartmentTechnische Universit?t MünchenJames-Franck-Str. 1 85748 Garching Germany;</p> <p>Physik-DepartmentTechnische Universit?t MünchenJames-Franck-Str. 1 85748 Garching Germany;</p> <p>Dipartimento di Scienze ChimicheUniversità di Padova Via Marzolo 1 35131 Padova Italy;</p> <p>Dipartimento di Scienze ChimicheUniversità di Padova Via Marzolo 1 35131 Padova Italy;</p> <p>Dipartimento di Scienze ChimicheUniversità di Padova Via Marzolo 1 35131 Padova Italy;</p> <p>Institut für Physikalische ChemieLeopold-Franzens-Universit?t InnsbruckInnrain 52c 6020 Innsbruck Austria;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=charge transfer&option=203" rel="nofollow">charge transfer;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrochemical impedance spectroscopy&option=203" rel="nofollow">electrochemical impedance spectroscopy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solid/liquid interface&option=203" rel="nofollow">solid/liquid interface;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=surface chemistry&option=203" rel="nofollow">surface chemistry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=titanium oxycarbide&option=203" rel="nofollow">titanium oxycarbide;</a> </p> <div class="translation"> 机译：电荷转移;电化学阻抗光谱;固体/液面界面;表面化学;氧化钛; 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MML：MROW> </ MML：MSUBSUP> </ MML ：MROW> </ MML：MATH>，和<MML：MATH ALTIMG =“SI2.GIF”overflow =“滚动”XMLNS：XOCS =“http://www.elsevier.com/xml/xocs/dtd”xmlns： xs =“http://www.w3.org/2001/xmlschema”xmlns：xsi =“http://www.w3.org/20 01 / XMLSchema-instance“xmlns =”http://www.elsevier.com/xml/ja/dtd“xmlns：ja =”http://www.elsevier.com/xml/ja/dtd“xmlns：mml = “http://www.w3.org/1998/math/mathml”xmlns：tb =“http://www.elsevier.com/xml/common/table/dtd”xmlns：sb =“http：// www .elsevier.com / xml / common / struct-bib / dtd“xmlns：ce =”http://www.elsevier.com/xml/common/dtd“xmlns：xlink =”http://www.w3.org / 1999 / xlink“xmlns：cals =”http://www.elsevier.com/xml/common/cals/dtd“> <mml：mrow> <mml：msubsup> <mml：mrow> <mml：mtext> d </ MML：MTEXT> </ MML：MROW> <MML：MROW> <MML：MN> 3 </ MML：MN> </ MML：MROW> <MML：MROW> <MML：MO> + </ MML： Mo> </ MML：MROW> </ MML：MSUBSUP> </ MML：MROW> </ MML：MATH>离子束照射</span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 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Effect of Air‐Aging on the Electrochemical Characteristics of TiO x xx C y yy Films for Electrocatalysis Applications

摘要

Effect of Air‐Aging on the Electrochemical Characteristics of TiO _x xx C _y yy Films for Electrocatalysis Applications