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Biosynthesis and Characterization of Copper Nanoparticles Using a Bioflocculant Extracted from Alcaligenis faecalis HCB2

机译:使用Alcaligenis Faecalis HCB2中萃取的生物絮凝剂的生物合成和表征铜纳米粒子

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摘要

Bioflocculant from Alcaligenis faecalis HCB2 was used in the eco-friendly synthesis of the copper nanoparticles. Nanoparticles were characterized using a scanning electron microscope (SEM), transmission electron microscopy (TEM), UV-visible spectroscopy, thermo gravimetric analysis(TGA) and Fourier Transform Infrared Spectroscopy (FT-IR). The transmission electron microscopy images showed close to spherical shapes with an average particle size of ~53 nm. Energy-dispersive X-ray spectroscopy analysis confirmed the presence of the Cu nanopartilces and also the otherelements such as O, C, P, Ca, Cl, Na, K, Mg, and S originated from the bioflocculant. FT-IR results showed the presence of the –OH and –NH2 groups, aliphatic bonds, amide and Cu–O bonds. Powder X-ray diffraction peaks confirmed the presence of (111) and (220) planesof fcc structure at 2 of 33° and 47° respectively with no other impurity peaks.
机译:来自Alcaligenis Faecalis HCB2的生物絮凝剂用于Eco友好的铜纳米粒子的合成。 使用扫描电子显微镜(SEM),透射电子显微镜(TEM),UV可见光谱,热重量分析(TGA)和傅里叶变换红外光谱(FT-IR)进行纳米颗粒。 透射电子显微镜图像显示靠近球形形状,平均粒径为约53nm。 能量分散X射线光谱分析证实了Cu纳米颗粒的存在,以及诸如O,C,P,Ca,Cl,Na,K,Mg的子项的存在源自生物絮凝剂。 FT-IR结果显示了-OH和-NH2基团的存在,脂族键,酰胺和Cu-O键。 粉末X射线衍射峰确认在33°和47°的23°和47°的FCC结构中确认存在(111)和(220)普林,没有其他杂质峰。

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