SYNTHESIS AND ANTIBACTERIAL ACTIVITY OF Tb(III), Ho(III), Er(III) AND Yb(III) COMPLEXES OF CHRYSIN-4'-SULFONATE

JANUSZ PUSZ; EL?BIETA PIENI??EK; EL?BIETA WO?NICKA; EWA CISZKOWICZ; KATARZYNA LECKA-SZLACHTA; STANIS?AW WO?OWIEC; ?UKASZ BYCZY?SKI

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SYNTHESIS AND ANTIBACTERIAL ACTIVITY OF Tb(III), Ho(III), Er(III) AND Yb(III) COMPLEXES OF CHRYSIN-4'-SULFONATE

机译：Chrysin-4'-磺酸盐的Tb（III），HO（III），HO（III），ER（III）和YB（III）复合物的合成和抗菌活性

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New solid lanthanide(III) (Ln) compounds of Tb(III), Ho(III), Er(III) and Yb(III) with sodium salt chrysin-4'-sulfonate (Nachsa-4') were obtained. The compounds were obtained from M : Nachsa-4' = 1 : 3 aqueous solutions at 6.0 - 6.2 pH range. Solid products showed Ln(0H)(Nachsa-4')_2·nH_2O stoichiometry based on elemental analysis and thermogravimetric studies. The complexes were characterized in solution by UV/Vis and infrared as well as by the ~1H NMR spectroscopies. The anionic ligands were chelated to the central metal ion via 4C=0 and 5C-0 oxygen donors of Nachsa-4'. The ligand and the new complexes were tested in vitro to evaluate their activity against the bacteria Escherichia coli, Pseudomonas aeruginosa and Staphylococcus aureus.

机译：获得了与钠盐蛹-4'-磺酸钠（NACHSA-4'）的Tb（III），HO（III），HO（III），ER（III）和YB（III）的新的固体镧系（III）（III）化合物。将化合物从M：Nachsa-4'= 1：3水溶液中获得，在6.0-6.2 pH范围内。固体产品显示LN（0H）（NACHSA-4'）_ 2·NH_2O化学计量基于元素分析和热重分析研究。通过UV / Vis和红外和红外线以及〜1H NMR光谱在溶液中表征复合物。将阴离子配体通过4c = 0和5c-0的Nachsa-4'螯合到中央金属离子。在体外测试配体和新络合物，以评估它们对细菌大肠杆菌，假单胞菌铜绿假单胞菌和金黄色葡萄球菌的活性。

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《Acta Poloniae Pharmaceutica: Durg Research》 |2018年第3期|共11页
作者
JANUSZ PUSZ; EL?BIETA PIENI??EK; EL?BIETA WO?NICKA; EWA CISZKOWICZ; KATARZYNA LECKA-SZLACHTA; STANIS?AW WO?OWIEC; ?UKASZ BYCZY?SKI;
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Department of Inorganic and Analytical Chemistry Faculty of Chemistry Rzeszow University of;

Department of Inorganic and Analytical Chemistry Faculty of Chemistry Rzeszow University of;

Department of Inorganic and Analytical Chemistry Faculty of Chemistry Rzeszow University of;

Department of Biochemistry and Biotechnology Faculty of Chemistry Rzeszów University of Technology;

Department of Biochemistry and Biotechnology Faculty of Chemistry Rzeszów University of Technology;

Center for Innovative Research in Medical and Natural Sciences Faculty of Medicine University of;

Department of Polymers and Biopolymers Faculty of Chemistry Rzeszów University of Technology;

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正文语种 eng
中图分类药学;
关键词
sodium chrysin-4'-sulfonate; synthesis; complexes; spectroscopic properties; lanthanide;

机译：辣椒素-4'-磺酸钠;合成;复合物;光谱性质;镧系元素;

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专利

1. SYNTHESIS AND ANTIBACTERIAL ACTIVITY OF Tb(III), Ho(III), Er(III) AND Yb(III) COMPLEXES OF CHRYSIN-4'-SULFONATE [J] . JANUSZ PUSZ, EL?BIETA PIENI??EK, EL?BIETA WO?NICKA, Acta Poloniae Pharmaceutica: Durg Research . 2018,第3期

机译：Chrysin-4'-磺酸盐的Tb（III），HO（III），HO（III），ER（III）和YB（III）复合物的合成和抗菌活性
2. Visible and near-infrared intense luminescence from water-soluble lanthanide [Tb(III), Eu(III), Sm(III), Dy(III), Pr(III), Ho(III), Yb(III), Nd(III), Er(III)] complexes [J] . Quici S, Cavazzini M, Marzanni G, Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2005,第3期

机译：水溶性镧系元素[Tb（III），Eu（III），Sm（III），Dy（III），Pr（III），Ho（III），Yb（III），Nd（ III），Er（III）]配合物
3. Assembly of heterobimetallic Ni~(II)-Ln~(III) (Ln~(III) = Dy~(III), Tb~(III), Gd~(III), Ho~(III), Er~(III), Y~(III)) complexes using a ferrocene ligand: slow relaxation of the magnetization in Dy~(III), Tb~(III) and Ho~(III) analogues [J] . Amit Chakraborty, Prasenjit Bag, Eric Rivière, Dalton transactions: An international journal of inorganic chemistry . 2014,第23期

机译：异双金属Ni〜（II）-Ln〜（III）的组装（Ln〜（III）= Dy〜（III），Tb〜（III），Gd〜（III），Ho〜（III），Er〜（III）二茂铁配体形成的Y，（Y〜（III））配合物：Dy〜（III），Tb〜（III）和Ho〜（III）类似物中磁化的缓慢弛豫
4. Synthesis, Spectral Properties of Tb (III) Complexes with 2, 2'-Dithiosalicylic Acid [C] . Li-Hua Wang International Conference on Material Engineering, Architectural Engineering and Informatization . 2012

机译：合成，Tb（III）配合物的光谱特性，2,2'-二硫代甲酸
5. I. Synthesis and reactivity of chiral iridium(III) and rhodium(III) complexes. II. Platinum-catalyzed iridium-methyl and iridium-phenyl bond formation [D] . Smith, Stuart Edward 2008

机译：I.手性铱（III）和铑（III）配合物的合成和反应性。二。铂催化的铱甲基和铱苯基键的形成
6. Heterometallic Octanuclear NiII4LnIII4 (Ln = Y Gd Tb Dy Ho Er) ComplexesContaining NiII2LnIII2O4 Distorted Cubane Motifs: Synthesis Structure andMagnetic Properties [O] . Pankaj Kalita, Joydeb Goura, Juan Manuel Herrera, 2018

机译：杂金属八核NiII4LnIII4（Ln = YGdTbDyHoEr）配合物包含NiII2LnIII2O4扭曲的古巴图案：合成结构和磁性能
7. Heterometallic Octanuclear NiII4LnIII4 (Ln = Y, Gd, Tb, Dy, Ho, Er) Complexes Containing NiII2LnIII2O4 Distorted Cubane Motifs: Synthesis, Structure, and Magnetic Properties [O] . Pankaj Kalita, Joydeb Goura, Juan Manuel Herrera, 2018

机译：含NiI2LNIII2O4失真的Cubane基序的含NiI2LNII2O4扭曲，结构和磁性特性含有Nii2LNIII2O4的差异，HO，ER，OR）配合物：合成，结构和磁性性能，差异octanuii4（Ln = Y，Gd，Tb，Dy，HO，ER）配合物：合成，结构和磁性

SYNTHESIS AND ANTIBACTERIAL ACTIVITY OF Tb(III), Ho(III), Er(III) AND Yb(III) COMPLEXES OF CHRYSIN-4'-SULFONATE

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