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Development and testing of superfluid-cooled 900 MHz NMR magnet

机译:超流体冷却的900 MHz NMR磁体的开发和测试

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摘要

As the preliminary step for the 1 GHz NMR spectrometer, a 900 MHz class NMR magnet was fabricated and was successfully operated in December 1999. The magnet is made of 15 percent Sn-bronze-processed (Nb, Ti)_3Sn, Ta-reinforced (Nb, Ti)_3Sn, and NbTi conductors. All the coils are cooled with pressurized superfluid helium. The magnet generated a field of 21.20 T in a driven mode and then operated in a persistent mode at 21.17 T corresponding to a proton NMR frequency of 901.2 MHz. During the magnet excitation for 24 h, the superfluid bath temperature was kept constant to below 1.6 K using an automatic control system. After several excitation tests, the magnet was quenched and the rupture disk of the magnet vessel was broken. The size of the cold safety valve and the structure of the rupture disk have been checked and modified. Before the reassembly of the magnet cryostat, the modified superfluid cooler for cooling the magnet bath was tested.
机译:作为1 GHz NMR光谱仪的预备步骤,制造了900 MHz级NMR磁体,并于1999年12月成功运行。该磁体由15%锡青铜处理的(Nb,Ti)_3Sn,Ta增强( Nb,Ti)_3Sn和NbTi导体。所有盘管均用加压超流体氦冷却。磁体在驱动模式下产生21.20 T的磁场,然后在21.17 T的持久模式下运行,对应于901.2 MHz的质子NMR频率。在磁铁励磁24小时的过程中,使用自动控制系统将超流体浴的温度恒定保持在1.6 K以下。经过几次励磁测试后,将磁体淬火,并破坏了磁容器的破裂盘。检查并修改了冷安全阀的尺寸和防爆膜的结构。在重新组装磁体低温恒温器之前,已经对用于冷却磁体熔池的改进型超流体冷却器进行了测试。

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