首页> 外文期刊>Chemphyschem: A European journal of chemical physics and physical chemistry >3D ^{1414 N/ ^{11 H Double Quantum/ ^{11 H Single Quantum Correlation Solid‐State NMR for Probing the Parallel and Anti‐Parallel Beta‐Sheet Arrangement of Oligo‐Peptides at Natural Abundance}}}

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3D ^{1414 N/ ^{11 H Double Quantum/ ^{11 H Single Quantum Correlation Solid‐State NMR for Probing the Parallel and Anti‐Parallel Beta‐Sheet Arrangement of Oligo‐Peptides at Natural Abundance}}}

机译：3D 14 14 n / 1 1 h双量子/ 1 1 h单量子相关固态nmr用于探测并联和反平行在天然丰度下的寡肽的β-薄片排列

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Abstract > The beta (β)‐sheet structures of oligopeptides and polypeptides can be formed in anti‐parallel (AP) and parallel (P) forms, which is an important feature to understand such structures. In principle, P‐ and AP‐β‐sheet structures can be identified by the presence (AP) or absence (P) of inter‐strand 1 H <sub>NH</sub> / 1 H <sub>NH</sub> correlations on a diagonal in the corresponding 2D 1 H double quantum (DQ)/ 1 H single quantum (SQ) spectrum due to the different inter‐strand 1 H <sub>NH</sub> / 1 H <sub>NH</sub> distances between the two arrangements. However, the 1 H <sub>NH</sub> / 1 H <sub>NH</sub> peaks overlap with the 1 H <sub>NH3</sub> + / 1 H <sub>NH3</sub> + peaks, which always give cross‐peaks regardless of the β‐sheet arrangement. The 1 H <sub>NH3</sub> + / 1 H <sub>NH3</sub> + peaks disturb the observation of the presence/absence of 1 H <sub>NH</sub> / 1 H <sub>NH</sub> correlations and the assignment of 1 H <sub>NH</sub> and 1 H <sub>NH3</sub> + is not always available. Here, 3D 14 N/ 1 </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“main”XML：Lang =“en”> <标题类型=“main”>摘录</标题> >寡肽和多肽的β（β） - 曲调结构可以在反平行中形成（AP）和平行（P）形式，这是理解此类结构的重要特征。原则上，可以通过链间间 1 </ sup> h <sub </ sub> / <sup的存在（ap）或缺席（p）鉴定p-和ap-β-片状结构。 > 1 </ sup> h <sub> nh </ sub>在相应的2d 1 </ sup> h双量子（dq）/ 1 </ sup> h单量子（ SQ）谱引起的不同链间 1 </ sup> h <sub> nh </ sub> / 1 </ sup> h <sub> nh </ sub>两者之间的距离。但是， 1 </ sup> h <sub> nh </ sub> / 1 </ sup> h <sub> nh </ sub>峰值与 1 重叠h <sub> nh3 </ sub> + </ sup> / 1 </ sup> h <sub> nh3 </ sub> + </ sup>峰值，始终交叉 - 峰值无论β-纸条排列如何。 1 </ sup> h <sub> nh3 </ sub> + </ sup> / 1 </ sup> h <sub> nh3 </ sub> + </ Sup>峰值干扰 1 h <sub> nh </ sub> / 1 </ sup> h <sub> nh </ sub>相关性的存在/不存在的观察 1 </ sup> h <sub> nh </ sub>和 1 </ sup> h <sub> nh3 </ sub> + </ sup>并不总是可用的分配。这里，3D 14 </ sup> n / 1 </ sup> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16300/'>《Chemphyschem: A European journal of chemical physics and physical chemistry》</a> <b style="margin: 0 2px;">|</b><span>2018年第15期</span><b style="margin: 0 2px;">|</b><span>共5页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hong You‐lee&option=202" target="_blank" rel="nofollow">Hong You‐lee;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Asakura Tetsuo&option=202" target="_blank" rel="nofollow">Asakura Tetsuo;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nishiyama Yusuke&option=202" target="_blank" rel="nofollow">Nishiyama Yusuke;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>RIKEN CLST-JEOL Collaboration CenterYokohama Kanagawa 230-0045 Japan;</p> <p>Department of BiotechnologyTokyo University of Agriculture and TechnologyKoganei Tokyo 184-8588 Japan;</p> <p>RIKEN CLST-JEOL Collaboration CenterYokohama Kanagawa 230-0045 Japan;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=amino acids&option=203" rel="nofollow">amino acids;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=β-sheets&option=203" rel="nofollow">β-sheets;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hydrogen bonds&option=203" rel="nofollow">hydrogen bonds;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=NMR spectroscopy&option=203" rel="nofollow">NMR spectroscopy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=peptides&option=203" rel="nofollow">peptides;</a> </p> <div class="translation"> 机译：氨基酸;β-薄膜;氢键;NMR光谱;肽; 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3D 1414 N/ 11 H Double Quantum/ 11 H Single Quantum Correlation Solid‐State NMR for Probing the Parallel and Anti‐Parallel Beta‐Sheet Arrangement of Oligo‐Peptides at Natural Abundance

摘要

3D ^{1414 N/ ^{11 H Double Quantum/ ^{11 H Single Quantum Correlation Solid‐State NMR for Probing the Parallel and Anti‐Parallel Beta‐Sheet Arrangement of Oligo‐Peptides at Natural Abundance}}}