Condition Screening for Sustainable Catalysis in Single‐Electron Steps by Cyclic Voltammetry: Additives and Solvents

Liedtke Theresa; Hilche Tobias; Klare Sven; Gans?uer Andreas

摘要

Abstract > Cyclic voltammetry‐based screening method for Cp <sub>2</sub> TiX‐catalyzed reactions is extended to the screening of solvents other than tetrahydrofuran for bulk electrolysis of the catalyst and radical arylation. It was found that CH <sub>3</sub> CN can be used as a solvent for both processes without additives. Furthermore, in tetrahydrofuran, squaramide L2 is more efficient than the previously reported supramolecular halide binder, Schreiner's thiourea L1 . The results extend the usefulness of the proposed time and resource‐efficient screening method for designing catalysis reactions in single‐electron steps. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 基于循环伏安法的CP筛选方法 <sub> 2 </ sub> Tix催化的反应延伸到筛选除催化剂的批量电解的四氢呋喃之外的溶剂和自由基芳基。发现ch <sub> 3 </ sub> CN可用作两种工艺的溶剂，没有添加剂。此外，在四氢呋喃中，Squaramide l2 </ b> 比以前报道的超分子卤化物粘合剂更效率，施莱纳的硫脲 l1 </ b> 。结果延长了所提出的时间和资源有效的筛选方法，用于在单电子步骤中设计催化反应的筛选方法。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16185/'>《ChemSusChem》</a> <b style="margin: 0 2px;">|</b><span>2019年第13期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liedtke Theresa&option=202" target="_blank" rel="nofollow">Liedtke Theresa;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hilche Tobias&option=202" target="_blank" rel="nofollow">Hilche Tobias;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Klare Sven&option=202" target="_blank" rel="nofollow">Klare Sven;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gans?uer Andreas&option=202" target="_blank" rel="nofollow">Gans?uer Andreas;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Kekulé-Institut für Organische Chemie und BiochemieUniversit?t BonnGerhard-Domagk-Stra?e 1 53121 Bonn Germany;</p> <p>Kekulé-Institut für Organische Chemie und BiochemieUniversit?t BonnGerhard-Domagk-Stra?e 1 53121 Bonn Germany;</p> <p>Kekulé-Institut für Organische Chemie und BiochemieUniversit?t BonnGerhard-Domagk-Stra?e 1 53121 Bonn Germany;</p> <p>Kekulé-Institut für Organische Chemie und BiochemieUniversit?t BonnGerhard-Domagk-Stra?e 1 53121 Bonn Germany;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=arylation&option=203" rel="nofollow">arylation;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=cyclic voltammetry&option=203" rel="nofollow">cyclic voltammetry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=epoxide&option=203" rel="nofollow">epoxide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=squaramide&option=203" rel="nofollow">squaramide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=titanium&option=203" rel="nofollow">titanium;</a> </p> <div class="translation"> 机译：芳族化;循环伏安法;环氧化物;鳞状;钛; 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href="/patent-detail/06120106234017.html">用于诊断、预防和/或护理特征为β-淀粉和/或淀粉样物质在人和/或动物器官和组织中异常沉积的人和/或动物病理的产物及它们的应用、和用于确定这种病理风险的筛选方法</a> <b>[P]</b> . <span> 中国专利： CN102037136A </span> <span> . 2011-04-27</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/061201207078.html">提高表面活性剂效率、抑制层状中间相、稳定单相区温度的方法以及借助添加剂和表面活性剂-油混合物降低含硅油的微乳状液中界面张力的方法</a> <b>[P]</b> . <span> 中国专利： CN101180347B </span> <span> . 2013.06.19</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130461357945.html">Plant watering water conditioning system - has cyclically operated mixing vessels and single stepwise conditioning line</a> <b>[P]</b> . <span> 外国专利：  DE4128019A1 </span> <span> . 1993-02-25</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：植物浇水水调节系统-具有循环操作的混合容器和单个逐步调节线 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130457877039.html">Cyclic voltammetry to measure the concentration of the plating bath additive components</a> <b>[P]</b> . <span> 外国专利：  JPH0820417B2 </span> <span> . 1996-03-04</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：循环伏安法测量镀浴添加剂成分的浓度 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130462174857.html">CYCLIC VOLTAMMETRY METHOD FOR MEASURING CONCENTRATION OF ADDITIVE COMPONENTS OF PLATING BATH</a> <b>[P]</b> . <span> 外国专利：  JPH05106100A </span> <span> . 1993-04-27</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：循环伏安法测定镀液中添加剂的含量。 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: 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