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首页> 外文期刊>Chemistry, an Asian journal >Rational Design of [ 1313 C,D 1414 ] TertTert ‐butylbenzene as a Scaffold Structure for Designing Long‐lived Hyperpolarized 1313 C Probes
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Rational Design of [ 1313 C,D 1414 ] TertTert ‐butylbenzene as a Scaffold Structure for Designing Long‐lived Hyperpolarized 1313 C Probes

机译：理性设计[ 13 13 光盘 14 14 ] tert tert - 丁基苯作为用于设计长寿命的超极化的支架结构 13 13 C探针

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Abstract > Dynamic nuclear polarization (DNP) is a technique to polarize the nuclear spin population. As a result of the hyperpolarization, the NMR sensitivity of the nuclei in molecules can be dramatically enhanced. Recent application of the hyperpolarization technique has led to advances in biochemical and molecular studies. A major problem is the short lifetime of the polarized nuclear spin state. Generally, in solution, the polarized nuclear spin state decays to a thermal spin equilibrium, resulting in loss of the enhanced NMR signal. This decay is correlated directly with the spin‐lattice relaxation time T <sub>1</sub> . Here we report [ 13 C,D <sub>14</sub> ] tert ‐butylbenzene as a new scaffold structure for designing hyperpolarized 13 C probes. Thanks to the minimized spin‐lattice relaxation ( T <sub>1</sub> ) pathways, its water‐soluble derivative showed a remarkably long 13 C T <sub>1</sub> value and long retention of the hyperpolarized spin state. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <标题类型=“main”>抽象</ title> > 动态核偏振（DNP）是一种偏振核旋转群体的技术。由于超极化，可以显着增强分子中核的NMR敏感性。最近的超极化技术的应用导致生化和分子研究进展。主要问题是偏振核旋转状态的短寿命。通常，在溶液中，偏振核自旋状态衰减到热旋转平衡，导致增强的NMR信号损失。这种衰减与旋转格子松弛时间直接相关 t </ i> <sub> 1 </ sub> 。在这里我们报告[ 13 </ sup> 光盘 <sub> 14 </ sub> ] tert </ i> - 丁基苯作为用于设计超极化的新支架结构 13 </ sup> C探针。由于最小化的旋转晶格放松（ t </ i> <sub> 1 </ sub> ）途径，其水溶性衍生物显示出显着长的 13 </ sup> C t </ i> <sub> 1 </ sub> 超极化旋转状态的价值和长期保留。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16161/'>《Chemistry, an Asian journal》</a> <b style="margin: 0 2px;">|</b><span>2018年第3期</span><b style="margin: 0 2px;">|</b><span>共4页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Imakura Yuki&option=202" target="_blank" rel="nofollow">Imakura Yuki;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nonaka Hiroshi&option=202" target="_blank" rel="nofollow">Nonaka Hiroshi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Takakusagi Yoichi&option=202" target="_blank" rel="nofollow">Takakusagi Yoichi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ichikawa Kazuhiro&option=202" target="_blank" rel="nofollow">Ichikawa Kazuhiro;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Maptue Nesmine R.&option=202" target="_blank" rel="nofollow">Maptue Nesmine R.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Funk Alexander M.&option=202" target="_blank" rel="nofollow">Funk Alexander M.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Khemtong Chalermchai&option=202" target="_blank" rel="nofollow">Khemtong Chalermchai;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sando Shinsuke&option=202" target="_blank" rel="nofollow">Sando Shinsuke;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Chemistry and Biotechnology Graduate School of EngineeringThe University of Tokyo7-3-1 Hongo Bunkyo-ku Tokyo 113-8656 Japan;</p> <p>Department of Chemistry and Biotechnology Graduate School of EngineeringThe University of Tokyo7-3-1 Hongo Bunkyo-ku Tokyo 113-8656 Japan;</p> <p>Incubation Center for Advanced Medical ScienceKyushu University3-1-1 Maidashi Higashi-ku Fukuoka 812-8582 Japan;</p> <p>Incubation Center for Advanced Medical ScienceKyushu University3-1-1 Maidashi Higashi-ku Fukuoka 812-8582 Japan;</p> <p>Advanced Imaging Research CenterUniversity of Texas Southwestern Medical Center5323 Harry Hines Boulevard Dallas Texas 75390 USA;</p> <p>Advanced Imaging Research CenterUniversity of Texas Southwestern Medical Center5323 Harry Hines Boulevard Dallas Texas 75390 USA;</p> <p>Advanced Imaging Research CenterUniversity of Texas Southwestern Medical Center5323 Harry Hines Boulevard Dallas Texas 75390 USA;</p> <p>Department of Chemistry and Biotechnology Graduate School of EngineeringThe University of Tokyo7-3-1 Hongo Bunkyo-ku Tokyo 113-8656 Japan;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=chemical probe&option=203" rel="nofollow">chemical probe;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=dynamic nuclear polarization&option=203" rel="nofollow">dynamic nuclear polarization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hyperpolarization&option=203" rel="nofollow">hyperpolarization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nuclear magnetic resonance&option=203" rel="nofollow">nuclear magnetic resonance;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=spin-lattice relaxation time&option=203" rel="nofollow">spin-lattice relaxation time;</a> </p> <div class="translation"> 机译：化学探针;动态核极化;超极化;核磁共振;旋转晶格松弛时间; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022086715.html">Rational Design of [ <sup 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