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Sulfur‐Deficient TiS2‐x for Promoted Polysulfide Redox Conversion in Lithium‐Sulfur Batteries

机译：硫缺陷的TIS2-X用于促进锂 - 硫电池中的多硫化物氧化还原转化率

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Abstract > Sulfur‐deficient TiS <sub>2–x</sub> is prepared through high temperature vacuum annealing. Electron spin resonance (ESR) and X‐ray photoelectron spectroscopy (XPS) data confirm the presence of sulfur vacancies in TiS <sub>2–x</sub> . Effective polysulfide adsorption and promotion to polysulfide redox conversion was proven by adsorption simulation experiments and electrochemical measurements. Thus, TiS <sub>2–x</sub> is used as cathode promoter for Li?S half‐cells to improve the overall electrochemical performance. As expected, the TiS <sub>2–x</sub> /S electrode shows a high and stable capacity of 751?mAh?g ?1 even after 500 cycles and a fade rate as low as 0.04?% per cycle at 1?C. Besides, the high sulfur loading of the electrode of 4?mg?cm ?2 also displays an admirable cycling performance of 963?mAh?g ?1 with a capacity retention up to 91.7?% over 50 cycles at 0.2?C. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 硫缺陷TIS <sub> 2-x </ sub> 通过高温真空退火制备。电子自旋共振（ESR）和X射线光电子体光谱（XPS）数据确认了TIS中的硫空位 <sub> 2-x </ sub> 。通过吸附模拟实验和电化学测量证明了对多硫化钠氧化还原转化率的有效多硫化物吸附和促进。因此，TIS. <sub> 2-x </ sub> 用作Li·S半电池的阴极促进剂，以提高整体电化学性能。正如预期的那样，TIS <sub> 2-x </ sub> / S电极显示出751的高且稳定的容量为751？MAH？G ？1 </ sup> 即使在500次循环和淡出率低至0.04°/ 0.04的衰减率为1Ω·c。此外，电极的高硫加载为4？mg？cm ？2 </ sup> 还展示了963的令人钦佩的循环性能？Mah？G ？1 </ sup> 容量保留高达91.7℃超过50周期，0.2？c。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16042/'>《ChemElectroChem》</a> <b style="margin: 0 2px;">|</b><span>2019年第8期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhao Yingyue&option=202" target="_blank" rel="nofollow">Zhao Yingyue;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cai Wenlong&option=202" target="_blank" rel="nofollow">Cai Wenlong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fang Yuting&option=202" target="_blank" rel="nofollow">Fang Yuting;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ao Huaisheng&option=202" target="_blank" rel="nofollow">Ao Huaisheng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhu Yongchun&option=202" target="_blank" rel="nofollow">Zhu Yongchun;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Qian Yitai&option=202" target="_blank" rel="nofollow">Qian Yitai;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Hefei National Laboratory for Physical Science at Microscale Department of Chemistry and Department of Materials Science and EngineeringUniversity of Science and Technology of China96 JinZhai Road Hefei 230026 P. R. China;</p> <p>Hefei National Laboratory for Physical Science at Microscale Department of Chemistry and Department of Materials Science and EngineeringUniversity of Science and Technology of China96 JinZhai Road Hefei 230026 P. R. China;</p> <p>Hefei National Laboratory for Physical Science at Microscale Department of Chemistry and Department of Materials Science and EngineeringUniversity of Science and Technology of China96 JinZhai Road Hefei 230026 P. R. China;</p> <p>Hefei National Laboratory for Physical Science at Microscale Department of Chemistry and Department of Materials Science and EngineeringUniversity of Science and Technology of China96 JinZhai Road Hefei 230026 P. R. China;</p> <p>Hefei National Laboratory for Physical Science at Microscale Department of Chemistry and Department of Materials Science and EngineeringUniversity of Science and Technology of China96 JinZhai Road Hefei 230026 P. R. China;</p> <p>Hefei National Laboratory for Physical Science at Microscale Department of Chemistry and Department of Materials Science and EngineeringUniversity of Science and Technology of China96 JinZhai Road Hefei 230026 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=effective polysulfide adsorption&option=203" rel="nofollow">effective polysulfide adsorption;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=fast polysulfide redox conversion&option=203" rel="nofollow">fast polysulfide redox conversion;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=lithium-sulfur batteries&option=203" rel="nofollow">lithium-sulfur batteries;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=sulfur deficiency&option=203" rel="nofollow">sulfur deficiency;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=sulfur vacancies&option=203" rel="nofollow">sulfur vacancies;</a> </p> <div class="translation"> 机译：有效的多硫化物吸附;快速多硫化物氧化还原转化;锂 - 硫磺电池;硫缺乏;硫磺空缺; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022061024.html">Sulfur‐Deficient TiS2‐x for Promoted Polysulfide Redox Conversion in Lithium‐Sulfur Batteries</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhao Yingyue&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zhao Yingyue,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cai Wenlong&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Cai Wenlong,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fang Yuting&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Fang Yuting,</a> <a href="/journal-foreign-16042/" target="_blank" rel="nofollow" class="tuijian_authcolor">ChemElectroChem .</a> <span>2019</span><span>,第8期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：硫缺陷的TIS2-X用于促进锂 - 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. <span> 中国专利： CN111712948A </span> <span> . 2020-09-25</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/061202688920.html">在锂‑硫或硅‑硫电池中作为粘结剂的单锂离子导体</a> <b>[P]</b> . <span> 中国专利： CN104051737B </span> <span> . 2017.12.26</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130501112917.html">ELECTRODE AND ELECTRODE MATERIAL COMPRISING SULFUR-LIMONENE POLYSULFIDE FOR LITHIUM-SULFUR BATTERIES</a> <b>[P]</b> . <span> 外国专利：  US2021376322A1 </span> <span> . 2021-12-02</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包含用于锂 - 硫磺电池的硫 - 柠檬烯多硫化物的电极和电极材料 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130403432058.html">ELECTRODE AND ELECTRODE MATERIAL COMPRISING SULFUR-LIMONENE POLYSULFIDE FOR LITHIUM-SULFUR BATTERIES</a> <b>[P]</b> . <span> 外国专利：  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