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A tungsten disulphide-polypyrrole composite-based humidity sensor at room temperature

机译:在室温下钨二硫吡吡硼复合材料基湿度传感器

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摘要

An electrically conductive polypyrrole-tungsten disulphide (PPy/WS2) composite was synthesized by a chemical polymerization technique. The composite was characterized by field emission scanning electron microscopy (FESEM), X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR) and energy dispersive X-ray spectroscopy (EDX). FESEM images showed the grainy morphology with permeable nature. XRD and FTIR characteristic peak analysis exhibited semi-crystalline behaviour and confirming the interfacial interaction of the as-synthesized composite. EDX confirmed the presence of carbon, nitrogen, oxygen, tungsten and sulphur in the composite. The humidity sensing property of the PPy/WS2-50% composite was tested and an approximate linear decrease in resistance was observed with an increase in relative humidity, along with a maximum sensing response of 97% and a response-recovery time of 52 and 58 s, respectively. The sensing ability of the composite was observed to be stable, when monitored for a period of two months.
机译:通过化学聚合技术合成导电聚吡咯 - 钨(PPY / WS2)复合物。该复合材料的特征是通过现场发射扫描电子显微镜(FESEM),X射线衍射(XRD),傅里叶变换红外光谱(FTIR)和能量分散X射线光谱(EDX)。 FeSEM图像显示颗粒状态,具有渗透性。 XRD和FTIR特征峰值分析显示出半结晶行为,并确认用合成复合材料的界面相互作用。 EDX证实了复合材料中存在碳,氮气,氧气,钨和硫。测试PPY / WS2-50%复合材料的湿度感应性能,并在相对湿度的增加,相对湿度的增加,观察到耐受性的近似线性降低,以及97%的最大感测响应和52和58的响应恢复时间分别。观察到复合材料的感测能力是稳定的,当监测为期两个月时。

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