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Dy/chitosan: a highly efficient and recyclable heterogeneous nano catalyst for the synthesis of hexahydropyrimidines in aqueous media

机译:DY /壳聚糖:一种高效且可回收的非均相纳米催化剂,用于在含水介质中合成六氢嘧啶

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摘要

A chitosan supported Dy(III) nanocatalyst was synthesised by a simple procedure. It was used as a catalyst for one pot, three component synthesis of hexahydropyrimidine derivatives. All the reactions were completed in a short time period at room temperature and the products were obtained in high to excellent yields. The catalyst was characterized by FT-IR, XRD, SEM-EDX, TEM and ICP-AES analyses. The stability of the catalyst was evaluated by TG analysis. Use of water, ambient conditions, recyclability and high TOF of the catalyst make this protocol a sustainable alternative to existing protocols.
机译:通过简单的程序合成壳聚糖支持的Dy(III)纳米催化剂。 它用作一个罐的催化剂,三种组分合成六氢嘧啶衍生物。 所有反应在室温下在短时间内完成,并将产物高至优异的产率。 催化剂的特征在于FT-IR,XRD,SEM-EDX,TEM和ICP-AES分析。 通过TG分析评价催化剂的稳定性。 使用水,环境条件,催化剂的高度TOF使本协议成为现有协议的可持续替代方案。

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  • 来源
    《RSC Advances》 |2015年第63期|共10页
  • 作者单位

    Aligarh Muslim Univ Dept Chem Aligarh 202002 Uttar Pradesh India;

    Aligarh Muslim Univ Dept Chem Aligarh 202002 Uttar Pradesh India;

    Aligarh Muslim Univ Dept Chem Aligarh 202002 Uttar Pradesh India;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 化学;
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