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The research for low-temperature rheological properties and structural characteristics of high-viscosity modified asphalt

机译:高粘度改性沥青的低温流变性能及结构特征研究

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High-viscosity modified (HVM) asphalt was prepared by the addition of styrene-butadiene-styrene, furfural exact oil (FEO, plasticizer), sulphur (crosslinker). The low-temperature rheological properties of HVM asphalt were investigated by using bending beam rheometer, and different analysis ways including Fourier transform infrared (FTIR) analysis, thermal analysis, (1)hydrogen nuclear magnetic resonance ((NMR)-N-1) analysis, elemental analysis, optical microscopy were used to investigate the structural characteristics of modified asphalts and FEO. Rheological tests demonstrated the effect of each modifier on low-temperature rheological performances of asphalt and displayed the structural characteristics of each binder to some extent. FTIR analysis indicated the effect of ageing and modifier on the distribution of functional groups of modified asphalt before and after ageing. Morphology observation showed the distribution of polymer in asphalt with different modifications or ageing. The thermal analysis showed the effect of each modifier on thermal behaviour of asphalt before and after ageing and confirmed the result of FTIR analysis and morphology observation further. Besides, the constituents of base asphalt and plasticizer were also investigated and compared further by adopting elemental analysis, and (HNMR)-H-1 and FTIR tests.
机译:通过添加苯乙烯 - 丁二烯 - 苯乙烯,糠醛精确油(FeO,增塑剂),硫(交联剂)制备高粘度改性(HVM)沥青。通过使用弯曲梁流变仪研究HVM沥青的低温流变性能,以及包括傅里叶变换红外(FTIR)分析,热分析,(1)氢核磁共振((NMR)-N-1)分析的不同分析方式,元素分析,光学显微镜用于研究改性沥青和Feo的结构特征。流变试验证明了每种改性剂对沥青的低温流变性能的影响,并在一定程度上显示每个粘合剂的结构特征。 FTIR分析表明老化和改性剂对衰老前后改性沥青官能团分布的影响。形态学观察显示沥青中聚合物的分布,不同的修饰或老化。热分析显示了每种改性剂对老化前后沥青的热行为的影响,并确认了FTIR分析和形态学观察的结果。此外,还通过采用元素分析和(HNMR)-H-1和FTIR测试进一步研究并比较碱基沥青和增塑剂的成分。

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