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Study of Diels–Alder reactions between furan and maleimide model compounds and the preparation of a healable thermo‐reversible polyurethane

机译：呋喃和马来酰亚胺模型化合物之间的Diels-Alder反应及其愈合热可逆聚氨酯的制备

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ABSTRACT > A study of the reactions between various furan and maleimide model compounds and the effects of reaction conditions was performed, allowing for a proper design and preparation of a thermo‐reversible polyurethane (PU) material crosslinked via Diels–Alder (DA) bonds. Thus, a linear polyurethane containing furan groups along the main chain was synthesized and crosslinked with a bismaleimide by means of DA reaction. The obtained thermoset exhibited thermo‐reversibility as evidenced by DSC and FTIR microscopy, providing the material recyclability and scratch healability. Optical microscopy, SEM and tensile analysis of a scratched PU film revealed that efficient scratch healing was enabled by heating at 110 °C for 30 min and subsequently keeping at room temperature for 24 h, resulting in an approximately 80% recovery of the pristine mechanical strength. This material is a promising candidate for the development of self‐healing coatings. ? 2018 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2018 , 56 , 1806–1814 </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”> <title type =“main”>抽象</ title> >各种呋喃与进行马来酰亚胺模型化合物和反应条件的影响，允许通过Diels-Alder（DA）键交联的热可逆聚氨酯（PU）材料的适当设计和制备。因此，通过DA反应合成含有沿主链的呋喃基团的线性聚氨酯，并与双聚物交联。所获得的热固性可通过DSC和FTIR显微镜证明的热反转性，提供材料可回收性和划痕康复性。划痕PU膜的光学显微镜，SEM和拉伸分析显示，通过在110℃下加热30分钟并随后在室温下保持高效刮擦愈合，并在24小时内保持，导致原始机械强度的恢复约80％。这种材料是自我愈合涂料的开发的有希望的候选者。还是2018 Wiley期刊，Inc.J.Colom。 SCI。，A部分：polym。化学。 2018 </ b>， 56 </ i>，1806-1814 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35621/'>《Journal of Polymer Science, Part A. Polymer Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2018年第16期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Truong Thuy Thu&option=202" target="_blank" rel="nofollow">Truong Thuy Thu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nguyen Ha Tran&option=202" target="_blank" rel="nofollow">Nguyen Ha Tran;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Phan Man Ngoc&option=202" target="_blank" rel="nofollow">Phan Man Ngoc;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nguyen Le‐Thu T.&option=202" target="_blank" rel="nofollow">Nguyen Le‐Thu T.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Faculty of Materials TechnologyHo Chi Minh City University of Technology Vietnam National University (VNU–HCM) 268 Ly Thuong Kiet District 10Ho Chi Minh City Vietnam;</p> <p>Faculty of Materials TechnologyHo Chi Minh City University of Technology Vietnam National University (VNU–HCM) 268 Ly Thuong Kiet District 10Ho Chi Minh City Vietnam;</p> <p>Faculty of Materials TechnologyHo Chi Minh City University of Technology Vietnam National University (VNU–HCM) 268 Ly Thuong Kiet District 10Ho Chi Minh City Vietnam;</p> <p>Faculty of Materials TechnologyHo Chi Minh City University of Technology Vietnam National University (VNU–HCM) 268 Ly Thuong Kiet District 10Ho Chi Minh City Vietnam;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1184.html" title="有机化学">有机化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Diels–Alder&option=203" rel="nofollow">Diels–Alder;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=healable&option=203" rel="nofollow">healable;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polyurethane&option=203" rel="nofollow">polyurethane;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thermo‐reversible&option=203" rel="nofollow">thermo‐reversible;</a> </p> <div class="translation"> 机译：Diels-alder;可愈合;聚氨酯;热可逆; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704020726236.html">Study of Diels–Alder reactions between furan and maleimide model compounds and the preparation of a healable thermo‐reversible polyurethane</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Truong Thuy Thu&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Truong Thuy Thu,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nguyen Ha Tran&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Nguyen Ha Tran,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Phan Man Ngoc&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Phan Man Ngoc,</a> <a href="/journal-foreign-35621/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of Polymer Science, Part A. 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style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：-/-使用Diels-Alder / Retro Diels-Alder反应的热可逆自修复聚丙烯酸酯网络及其用途 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130405960672.html">-/- Thermoreversible self-healable polyacrylate networks using Diels-Alder/Retro Diels-Alder reaction and use thereof</a> <b>[P]</b> . <span> 外国专利：  KR20180114725A </span> <span> . 2018-10-19</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：-/-使用Diels-Alder / Retro Diels-Alder反应的热可逆自修复聚丙烯酸酯网络及其用途 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130418606252.html">( Hetero ) Diels - Alder reaction catalyst , and dihydropyran compounds using it and Diels - manufacturing method of Alder reaction adduct</a> <b>[P]</b> . <span> 外国专利：  JP5603041B2 </span> <span> . 2014-10-08</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：（杂）Diels-Alder反应催化剂，使用该催化剂的二氢吡喃化合物和Diels-Alder反应加合物的制备方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704020726236','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img 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