Substituent effect on supercapacitive performances of conducting polymer‐based redox electrodes: Poly(3′,4′‐bis(alkyloxy) 2,2′:5′,2″‐terthiophene) derivatives

Yi?it Deniz; Aykan Melis; Güllü Mustafa

摘要

ABSTRACT > This work reports the synthesis of novel poly(3′,4′‐bis(alkyloxy)terthiophene) derivatives (PTTOBu, PTTOHex, and PTTOOct) and their supercapacitor applications as redox‐active electrodes. The terthiophene‐based conducting polymers have been derivatized with different alkyl pendant groups (butyl‐, hexyl‐, and octyl‐) to explore the effect of alkyl chain length on the surface morphologies and pseudocapacitive properties. The electrochemical performance tests have revealed that the length of alkyl substituent created a remarkable impact over the surface morphologies and charge storage properties of polymer electrodes. PTTOBu, PTTOHex, and PTTOOct‐based electrodes have reached up to specific capacitances of 94.3, 227.3, and 443 F?g ?1 at 2.5 mA?cm ?2 constant current density, respectively, in a three‐electrode configuration. Besides, these redox‐active electrodes have delivered satisfactory energy densities of 13.5, 29.3, and 60.7 W?h?kg ?1 and power densities of 0.98, 1, and 1.1 kW?kg ?1 with good capacitance retentions after 10,000 charge/discharge cycles in symmetric solid‐state micro‐supercapacitor devices. ? 2017 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2018 , 56 , 480–495 </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”> <title type =“main”>抽象</ title> >本工作报告了新型多种多元的合成（ 3'，4'-双（烷氧基）萜烯）衍生物（Ptttobu，Pttohex和Pttooct）及其超级电容器应用作为氧化还原活性电极。基于三噻吩的导电聚合物已经用不同的烷基侧基（丁基，己基和辛基 - ）衍生化，以探讨烷基链长度对表面形态和假壳种性质的影响。电化学性能试验表明，烷基取代基的长度对聚合物电极的表面形态和电荷储存性能产生了显着的影响。 PTTTOBU，PTTOHEX和基于PTTOOC的电极已经达到了94.3,227.3和443fα1/ sup>在2.5 mAΔcm恒定电流下的特定电容密度分别在三电极配置中。此外，这些氧化还原主动电极具有13.5,29.3和60.7WΩ的令人满意的能量密度为13.5,29.3和60.7W≤1/ sup>和0.98,1和1.1 kW的功率密度？kg ？ 1 </ sup>在对称固态微型超级电容器装置10,000充电/放电循环后具有良好的电容保持。还是2017 Wiley期刊，Inc.J.Colom。 SCI。，A部分：polym。化学。 2018 </ b>， 56 </ i>，480-495 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35621/'>《Journal of Polymer Science, Part A. Polymer Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2018年第5期</span><b style="margin: 0 2px;">|</b><span>共16页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yi?it Deniz&option=202" target="_blank" rel="nofollow">Yi?it Deniz;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aykan Melis&option=202" target="_blank" rel="nofollow">Aykan Melis;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Güllü Mustafa&option=202" target="_blank" rel="nofollow">Güllü Mustafa;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of ChemistryAnkara UniversityBesevler 06100 Ankara Turkey;</p> <p>Department of ChemistryAnkara UniversityBesevler 06100 Ankara Turkey;</p> <p>Department of ChemistryAnkara UniversityBesevler 06100 Ankara Turkey;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1184.html" title="有机化学">有机化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=conducting materials&option=203" rel="nofollow">conducting materials;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=energy storage&option=203" rel="nofollow">energy storage;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=materials science&option=203" rel="nofollow">materials science;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polymers&option=203" rel="nofollow">polymers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=redox‐active electrodes&option=203" rel="nofollow">redox‐active electrodes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solid‐state devices&option=203" rel="nofollow">solid‐state devices;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=supercapacitors&option=203" rel="nofollow">supercapacitors;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=terthiophenes&option=203" rel="nofollow">terthiophenes;</a> </p> <div class="translation"> 机译：导电材料;储能;材料科学;聚合物;氧化还原活性电极;固态装置;超级电容器;萜烯; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704020726030.html">Substituent effect on supercapacitive performances of conducting polymer‐based redox electrodes: Poly(3′,4′‐bis(alkyloxy) 2,2′:5′,2″‐terthiophene) derivatives</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yi?it Deniz&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Yi?it Deniz,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Aykan Melis&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Aykan Melis,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Güllü Mustafa&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Güllü Mustafa </a> <a href="/journal-foreign-35621/" target="_blank" rel="nofollow" class="tuijian_authcolor">Journal of Polymer Science, Part A. 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class="enjiyixqcontent" href="/academic-journal-cn_chemical-journal-chinese-universities_thesis/0201231598156.html">取代基对二噻吩并噻吩衍生物的双光子吸收性质的影响</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=周树兰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 周树兰</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=赵显&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,赵显</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=孙学勤&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,孙学勤</a> <span> <a href="/journal-cn-10958/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 高等学校化学学报 </a> </span> <span> . 2006</span><span>,第010期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-1979_thesis/02022331447.html">烷氧基官能团化2-乙烯基噻吩聚合物制备场效应晶体管和全聚合物型太阳能电池</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=黄辉&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 黄辉</a> <span> <a href="/conference-cn-1979/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十四届中国光伏大会暨2014中国国际光伏展览会 </a> <span> <span> . 2014</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020311795046.html">聚烷氧基噻吩及聚噻吩/CdSe复合膜的制备与表征</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=黄鑫&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 黄鑫</a> <span> . 2007</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120104706375.html">含适宜形成中间相的基团的亚烷二氧基噻吩和聚(亚烷二氧基噻吩)</a> <b>[P]</b> . <span> 中国专利： CN1517357A </span> <span> . 2004-08-04</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120905458.html">具有聚亚烷氧基侧取代基的聚合物及其在个人护理方面的应用</a> <b>[P]</b> . <span> 中国专利： CN101232921B </span> <span> . 2012.04.04</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130417625338.html">Derivatives of bis (2,2 '-bitienylo)methane molecularly printed polymer formed by polymerization of derivatives of bis(2,2'-bitienylo)methane and the use of the polymer layer to selectively determine and release of adrenaline</a> <b>[P]</b> . <span> 外国专利：  PL217424B1 </span> <span> . 2014-07-31</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过双（2,2'-联苯胺基）甲烷衍生物的聚合反应形成的双（2,2'-联苯胺基）甲烷分子印刷聚合物的衍生物，以及使用聚合物层选择性地确定和释放肾上腺素 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130420248710.html">Derivatives of bis (2,2 '-bitienylo)methane molecularly printed polymer formed by polymerization of derivatives of bis(2,2'-bitienylo)methane and the use of the polymer layer to selectively determine and release of adrenaline</a> <b>[P]</b> . <span> 外国专利：  PL398219A1 </span> <span> . 2013-09-02</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过双（2,2'-联苯胺基）甲烷衍生物的聚合反应形成的双（2,2'-联苯胺基）甲烷分子印刷聚合物的衍生物，以及使用聚合物层选择性地确定和释放肾上腺素 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130457931239.html">Poly having an alkyl substituent (2,2'-bipyridine-5,5'-diyl) polymers, their preparation and use</a> <b>[P]</b> . <span> 外国专利：  JPH0826126B2 </span> <span> . 1996-03-13</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：具有烷基取代基（2,2'-联吡啶-5,5'-二基）聚合物的聚，其制备和用途 </span> </p> </li> </ul> </div> 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