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首页> 外文期刊>Journal of Molecular Structure >Microwave assisted rapid green synthesis of gold nanoparticles using Annona squamosa L peel extract for the efficient catalytic reduction of organic pollutants
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Microwave assisted rapid green synthesis of gold nanoparticles using Annona squamosa L peel extract for the efficient catalytic reduction of organic pollutants

机译:微波炉辅助使用斜鳞粒子的快速绿色合成金纳米粒子 l剥皮提取物,用于有机污染物的有效催化还原

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摘要

Here we demonstrate a rapid green synthetic approach for the production of gold nanoparticles (AuNPs) using microwave irradiation, in whichAnnona squamosaL (AS) fruit waste extract served as a sole agent for both reduction and stabilization. Synthetic conditions were optimized by monitoring the changes surface plasmon resonance (SPR) peak, zeta potential and DLS size distribution. TEM results revealed that under optimized synthetic conditions monodispersed and spherical nanoparticles with average diameter of 5?±?2?nm could be achieved. The possible mechanism involved in the formation of AuNPs was interpreted by FTIR. The formed AuNPs dispersion remained stable to environmental conditions like temperature, ionic strength and pH of the medium and exhibited high shelf life. Further they exhibited admirable catalytic activity for the efficient reduction of Congo red & Methylene Blue and 4-Nitrophenol in the presence of NaBH4, which is stable even after five cycles of reaction.
机译:在这里,我们展示了使用微波辐射生产金纳米颗粒(AUNP)的快速绿色综合方法,在anaNonaNaNa and(As)果实废物提取物中作为唯一的药物,用于减少和稳定。 通过监测变化表面等离子体共振(SPR)峰,Zeta电位和DLS尺寸分布来优化合成条件。 TEM结果表明,在优化的合成条件下,可以实现平均直径为5Ω·2Ω·2μm的单分散的合成条件和平均直径的球形纳米颗粒。 FTIR解释了患有AUNPS形成的可能机制。 形成的AUNPS分散体保持稳定,与温度,离子强度和培养基的pH一样稳定,并且表现出高保质期。 此外,它们表现出令人钦佩的催化活性,以便在NaBH4的存在下有效减少刚果红色和4-硝基苯酚,即使在五个反应循环后也稳定。

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