Direct transformation of primary nitro compounds into nitriles with sodium-dithionite

TemelliB.; UnalerogluC.

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Direct transformation of primary nitro compounds into nitriles with sodium-dithionite

机译：用钠 - 二硫代钛矿将原发性硝基化合物直接转化为腈

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摘要

A new and practical direct transformation of primary nitro compounds into nitriles with sodium dithionite is described. The reaction is simple, convenient and eliminates the use of expensive and moisture-sensitive reagents.

机译：描述了用二硫代钠将原发性硝基化合物的新的和实际直接转化为二硫酸钠。反应简单，方便，消除了使用昂贵和湿度敏感的试剂。

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来源
《Synthesis: International Journal of Methods in Synthetic Organic Chemistry》 |2014年第10期|共6页
作者
TemelliB.; UnalerogluC.;
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作者单位

Hacettepe University Department of Chemistry 06800 Ankara Turkey;

Hacettepe University Department of Chemistry 06800 Ankara Turkey;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
nitriles; nitro compounds; radicals; sulfur; synthetic methods;

机译：腈;硝基化合物;自由基;硫;合成方法;

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1. Direct transformation of primary nitro compounds into nitriles with sodium-dithionite [J] . TemelliB., UnalerogluC. Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2014,第10期

机译：用连二亚硫酸钠将伯硝基化合物直接转化为腈
2. FACILE SYNTHESIS OF NITRILES FROM PRIMARY NITRO COMPOUNDS VIA NITROLIC ACIDS AND THEIR ESTERS [J] . Chang RK., Kim K. Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 1996,第43期

机译：通过硝酸和酯类从初级硝基化合物轻松合成腈
3. Chemoselective reduction of nitro and nitrile compounds using an Fe3O4-MWCNTs@PEI-Ag nanocomposite as a reusable catalyst [J] . Ansari Sara, Khorshidi Alireza, Shariati Shahab RSC Advances . 2020,第6期

机译：使用Fe3O4-MWCNTS硝基纳米复合物作为可再用催化剂的硝基和腈化合物的化学选择性减少
4. Direct Transformations of Tetrafluoroethylene into Useful Synthetic Intermediates for Organofluorine Compounds [C] . Kotaro Kikushima, Masato Ohashi, Sensuke Ogoshi 日本化学会春季年会講演予稿集 . 2018

机译：四氟乙烯转化为有机氟化合物有用的合成中间体
5. CARBOHYDRAZIDE AS A SOLID REDUCING AGENT FOR REACTION GAS CHROMATOGRAPHY (DETERMINATION OF AZO, NITRO AND SULFONATE COMPOUNDS). PART I: REACTIONGAS CHROMATOGRAPHY OF AZO COMPOUNDS BY CARBOHYDRAZIDE REDUCTION AND GAS CHROMATOGRAPHY OF THE RESULTANT COMPOUNDS. PART II: ANALYSIS OF AROMATIC NITRO COMPOUNDS AND AROMATIC SULFONATES BY CARBOHYDRAZIDE REDUCTION AND GAS CHROMATOGRAPHY OF THE RESULTANT COMPOUNDS. [D] . RAHN, PETER CHARLES. 1973

机译：碳酰肼作为一种固体还原剂，用于气相色谱法（测定偶氮，硝基和磺酸盐化合物）。第一部分：偶氮化合物通过碳酰肼还原反应的气相色谱法和所得化合物的气相色谱法。第二部分：用碳酰肼还原法和气相色谱法分析芳香族硝基化合物和芳香族硫酸酯。
6. Magnetically Separable and Recyclable Fe3O4-Supported Ag Nanocatalysts for Reduction of Nitro Compounds and Selective Hydration of Nitriles to Amides in Water [O] . Hyunje Woo, Kyoungho Lee, Sungkyun Park, 2014

机译：磁性可分离和可回收利用的Fe3O4负载的Ag纳米催化剂用于还原硝基化合物以及将腈选择性水合为水中的酰胺
7. Chemoselective reduction of nitro and nitrile compounds using an Fe3O4-MWCNTs@PEI-Ag nanocomposite as a reusable catalyst [O] . Sara Ansari, Alireza Khorshidi, Shahab Shariati 2020

机译：使用Fe3O4-MWCNTS硝基纳米复合物作为可再用催化剂的硝基和腈化合物的化学选择性减少
8. Detection of Hydroxylated Nitro Aromatic and Hydroxylated Nitro Polycyclic Aromatic Compounds in an Ambient Air Particulate Extract Using Bioassay-Directed Fractionation [R] . Nishioka, M. G. , Howard, C. C. , Contos, D. A. , 1988

机译：生物测定定向分离检测环境空气颗粒提取物中羟基化硝基芳香和羟基化硝基多环芳烃

Direct transformation of primary nitro compounds into nitriles with sodium-dithionite

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